DE1216464B - Verfahren zur Herstellung eines Rutil-Titandioxid-Pigments mit verbesserter fotochemischer Stabilitaet - Google Patents
Verfahren zur Herstellung eines Rutil-Titandioxid-Pigments mit verbesserter fotochemischer StabilitaetInfo
- Publication number
- DE1216464B DE1216464B DEP36197A DEP0036197A DE1216464B DE 1216464 B DE1216464 B DE 1216464B DE P36197 A DEP36197 A DE P36197A DE P0036197 A DEP0036197 A DE P0036197A DE 1216464 B DE1216464 B DE 1216464B
- Authority
- DE
- Germany
- Prior art keywords
- antimony
- titanium dioxide
- arsenic
- precipitation
- salt solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 title claims description 25
- 239000000049 pigment Substances 0.000 title claims description 18
- 238000000034 method Methods 0.000 title claims description 16
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 9
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims description 9
- 239000012266 salt solution Substances 0.000 claims description 9
- 229910052785 arsenic Inorganic materials 0.000 claims description 8
- 229910052787 antimony Inorganic materials 0.000 claims description 7
- 238000001556 precipitation Methods 0.000 claims description 7
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims description 6
- 229920000877 Melamine resin Polymers 0.000 claims description 5
- 239000000725 suspension Substances 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 4
- 239000002244 precipitate Substances 0.000 claims description 4
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- ZDINGUUTWDGGFF-UHFFFAOYSA-N antimony(5+) Chemical class [Sb+5] ZDINGUUTWDGGFF-UHFFFAOYSA-N 0.000 claims description 2
- GOLCXWYRSKYTSP-UHFFFAOYSA-N arsenic trioxide Inorganic materials O1[As]2O[As]1O2 GOLCXWYRSKYTSP-UHFFFAOYSA-N 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000000227 grinding Methods 0.000 claims description 2
- 150000001463 antimony compounds Chemical class 0.000 claims 2
- IKWTVSLWAPBBKU-UHFFFAOYSA-N a1010_sial Chemical compound O=[As]O[As]=O IKWTVSLWAPBBKU-UHFFFAOYSA-N 0.000 claims 1
- 238000013019 agitation Methods 0.000 claims 1
- 239000003513 alkali Substances 0.000 claims 1
- 150000001495 arsenic compounds Chemical class 0.000 claims 1
- 229960002594 arsenic trioxide Drugs 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 229910010413 TiO 2 Inorganic materials 0.000 description 25
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 229910004298 SiO 2 Inorganic materials 0.000 description 7
- 229910052782 aluminium Inorganic materials 0.000 description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 5
- 238000000137 annealing Methods 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 239000004408 titanium dioxide Substances 0.000 description 5
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 description 4
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical class O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 229910052718 tin Inorganic materials 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- HJTAZXHBEBIQQX-UHFFFAOYSA-N 1,5-bis(chloromethyl)naphthalene Chemical compound C1=CC=C2C(CCl)=CC=CC2=C1CCl HJTAZXHBEBIQQX-UHFFFAOYSA-N 0.000 description 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 150000000703 Cerium Chemical class 0.000 description 1
- 229910052684 Cerium Inorganic materials 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 1
- 239000004640 Melamine resin Substances 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 206010034960 Photophobia Diseases 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 150000001462 antimony Chemical class 0.000 description 1
- FAWGZAFXDJGWBB-UHFFFAOYSA-N antimony(3+) Chemical class [Sb+3] FAWGZAFXDJGWBB-UHFFFAOYSA-N 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- JBDSSBMEKXHSJF-UHFFFAOYSA-N cyclopentanecarboxylic acid Chemical compound OC(=O)C1CCCC1 JBDSSBMEKXHSJF-UHFFFAOYSA-N 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 150000004677 hydrates Chemical class 0.000 description 1
- 238000010902 jet-milling Methods 0.000 description 1
- 208000013469 light sensitivity Diseases 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- AKMXMQQXGXKHAN-UHFFFAOYSA-N titanium;hydrate Chemical compound O.[Ti] AKMXMQQXGXKHAN-UHFFFAOYSA-N 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 238000001238 wet grinding Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/36—Compounds of titanium
- C09C1/3607—Titanium dioxide
- C09C1/3653—Treatment with inorganic compounds
- C09C1/3661—Coating
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP36197A DE1216464B (de) | 1965-03-03 | 1965-03-03 | Verfahren zur Herstellung eines Rutil-Titandioxid-Pigments mit verbesserter fotochemischer Stabilitaet |
| FR50638A FR1469827A (fr) | 1965-03-03 | 1966-02-22 | Procédé de préparation d'un pigment d'oxyde de titane rutile possédant une stabilité photochimique améliorée |
| FI47766A FI44260B (enrdf_load_stackoverflow) | 1965-03-03 | 1966-02-25 | |
| BE677079D BE677079A (enrdf_load_stackoverflow) | 1965-03-03 | 1966-02-25 | |
| GB874266A GB1080637A (en) | 1965-03-03 | 1966-02-28 | Improvements in or relating to rutile pigments |
| NL6602690A NL148354B (nl) | 1965-03-03 | 1966-03-02 | Werkwijze voor het bereiden van een fotochemisch stabiel rutiel-titaandioxydepigment, alsmede gevormd laminaatpapier, waarin het rutiel-titaandioxydepigment, verkregen volgens deze werkwijze, verwerkt is. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP36197A DE1216464B (de) | 1965-03-03 | 1965-03-03 | Verfahren zur Herstellung eines Rutil-Titandioxid-Pigments mit verbesserter fotochemischer Stabilitaet |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1216464B true DE1216464B (de) | 1966-05-12 |
Family
ID=7374617
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEP36197A Pending DE1216464B (de) | 1965-03-03 | 1965-03-03 | Verfahren zur Herstellung eines Rutil-Titandioxid-Pigments mit verbesserter fotochemischer Stabilitaet |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE677079A (enrdf_load_stackoverflow) |
| DE (1) | DE1216464B (enrdf_load_stackoverflow) |
| FI (1) | FI44260B (enrdf_load_stackoverflow) |
| GB (1) | GB1080637A (enrdf_load_stackoverflow) |
| NL (1) | NL148354B (enrdf_load_stackoverflow) |
-
1965
- 1965-03-03 DE DEP36197A patent/DE1216464B/de active Pending
-
1966
- 1966-02-25 BE BE677079D patent/BE677079A/xx unknown
- 1966-02-25 FI FI47766A patent/FI44260B/fi active
- 1966-02-28 GB GB874266A patent/GB1080637A/en not_active Expired
- 1966-03-02 NL NL6602690A patent/NL148354B/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| NL6602690A (enrdf_load_stackoverflow) | 1966-09-05 |
| FI44260B (enrdf_load_stackoverflow) | 1971-06-30 |
| GB1080637A (en) | 1967-08-23 |
| BE677079A (enrdf_load_stackoverflow) | 1966-07-18 |
| NL148354B (nl) | 1976-01-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE69308351T2 (de) | Titandioxidpigment und Herstellungsverfahren | |
| DE2244298C3 (de) | Perlglanzpigmente und Verfahren zu ihrer Herstellung | |
| DE69104759T2 (de) | Verfahren zum Überziehen von metalloxydischen Pigmenten und erhaltene Pigmente. | |
| DE2634661C2 (enrdf_load_stackoverflow) | ||
| DE2523682C2 (enrdf_load_stackoverflow) | ||
| EP0187331B1 (de) | Verfahren zur Herstellung heller farbreiner Eisenoxidrotpigmente | |
| DE2951805A1 (de) | Metallphosphat-beschichtete titandioxid-pigmente, verfahren zu ihrer herstellung und ihre verwendung | |
| DE2741615A1 (de) | Verbessertes monoklines wismutvanadatpigment | |
| CH495413A (de) | Verfahren zur Herstellung eines Rutil-Pigments mit hoher Kreidungsresistenz und Glanzhaltung | |
| DE3145620A1 (de) | Titandioxidpigment und verfahren zu seiner herstellung | |
| EP0075197B1 (de) | Flockungsstabile Mischphasenpigmente mit Rutilstruktur, Verfahren zu ihrer Herstellung sowie ihre Verwendung | |
| DE2629953A1 (de) | Verfahren zur behandlung von titandioxid-pigment | |
| DE1202422B (de) | Titandioxydpigmente | |
| DE1213557B (de) | Verfahren zum Erhoehen der Lichtbestaendigkeit von Rutilpigmenten in Melamin- und Harnstoff-Formaldehydharzen | |
| DE2605651C2 (de) | Verfahren zur Herstellung von verbesserten Chrom-Rutilpigmenten | |
| DE2223524C2 (de) | Verfahren zur Herstellung eines beschichteten Titandioxid-Pigmentes | |
| EP0315849A1 (de) | Verfahren zur Herstellung von Bismutoxidchlorid-Perlglanzpigmenten | |
| DE2629954C2 (enrdf_load_stackoverflow) | ||
| DE1592957A1 (de) | Verfahren zur Herstellung von Titandioxydpigmenten fuer die Papierindustrie | |
| DE1216464B (de) | Verfahren zur Herstellung eines Rutil-Titandioxid-Pigments mit verbesserter fotochemischer Stabilitaet | |
| DE1592934A1 (de) | Titandioxydpigmente und Verfahren zu ihrer Herstellung | |
| DE2234519A1 (de) | Verfahren zur herstellung von oberflaechenueberzogenen oxidteilchen | |
| DE1803637C3 (de) | Verfahren zur Herstellung von Eisenoxid-Pigmenten | |
| DE1592937B2 (de) | Verfahren zur farbverbesserung von rutilpigmenten | |
| DE2314593A1 (de) | Verfahren zur herstellung von molybdatorangepigmenten mit rotem farbton |