DE106510C - - Google Patents
Info
- Publication number
- DE106510C DE106510C DENDAT106510D DE106510DA DE106510C DE 106510 C DE106510 C DE 106510C DE NDAT106510 D DENDAT106510 D DE NDAT106510D DE 106510D A DE106510D A DE 106510DA DE 106510 C DE106510 C DE 106510C
- Authority
- DE
- Germany
- Prior art keywords
- acid
- melting point
- dinitrochlorobenzoic
- chlorobenzoic
- chlorobenzoic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 8
- CNTZGSBMOTYCOV-UHFFFAOYSA-N 2-chloro-3,4-dinitrobenzoic acid Chemical compound OC(=O)C1=CC=C([N+]([O-])=O)C([N+]([O-])=O)=C1Cl CNTZGSBMOTYCOV-UHFFFAOYSA-N 0.000 claims description 7
- 238000002844 melting Methods 0.000 claims description 6
- 230000008018 melting Effects 0.000 claims description 6
- IKCLCGXPQILATA-UHFFFAOYSA-N 2-chlorobenzoic acid Chemical compound OC(=O)C1=CC=CC=C1Cl IKCLCGXPQILATA-UHFFFAOYSA-N 0.000 claims description 5
- JRQDVRIQJJPHEQ-UHFFFAOYSA-N 3970-35-2 Chemical compound OC(=O)C1=CC=CC([N+]([O-])=O)=C1Cl JRQDVRIQJJPHEQ-UHFFFAOYSA-N 0.000 claims description 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 2
- 229910017604 nitric acid Inorganic materials 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000013067 intermediate product Substances 0.000 claims 1
- 150000002823 nitrates Chemical class 0.000 claims 1
- 238000006396 nitration reaction Methods 0.000 claims 1
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000004323 potassium nitrate Substances 0.000 description 3
- 235000010333 potassium nitrate Nutrition 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 229960000583 acetic acid Drugs 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- -1 dinitro compound Chemical class 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000004682 monohydrates Chemical class 0.000 description 1
- 238000005121 nitriding Methods 0.000 description 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE106510C true DE106510C (cs) |
Family
ID=376675
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT106510D Active DE106510C (cs) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE106510C (cs) |
-
0
- DE DENDAT106510D patent/DE106510C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE106510C (cs) | ||
| DE637318C (de) | Verfahren zur Herstellung von Nitroverbindungen substituierter Benzotrifluoride | |
| DE2513801A1 (de) | Neue fluorierte indazolderivate und verfahren zu ihrer herstellung | |
| DE3880281T2 (de) | 5-Nitro-4,6-bis-(3-nitro-1H-1,2,4-triazol-1-yl)pyrimidin, Verfahren zu seiner Herstellung und dieses enthaltender Sprengstoff. | |
| DE104495C (cs) | ||
| DE69707007T2 (de) | Nitrierungsverfahren | |
| DE92010C (cs) | ||
| DE116759C (cs) | ||
| DE249721C (cs) | ||
| DE264012C (cs) | ||
| DE206638C (cs) | ||
| DE415023C (de) | Verfahren zur Darstellung von Diacylessigsaeurearyliden | |
| DE112179C (cs) | ||
| DE2033644C3 (de) | Verfahren zur Herstellung von 5,6, 7,7a-Tetrahydro-1 ß -hydroxy-5-oxo-4-indancarbonsäuren bzw. deren Aethern und Estern | |
| DE1643607A1 (de) | Verfahren zum Sulfonieren aromatischer Nitroverbindungen | |
| DE885704C (de) | Verfahren zur Herstellung von ª‡-Halogen-p-nitroacetophenon | |
| DE79250C (de) | Verfahren zur Darstellung von Säurederivaten von m-Amidoalkyldiamidobenzhydrolen | |
| DE507417C (de) | Verfahren zur Darstellung von Trinitro-p-halogenbenzoyl-o-benzoesaeuren | |
| Avery et al. | The Nitration of β-p-TOLYGLUTARIC Acid. | |
| DE512228C (de) | Verfahren zur Darstellung von 2-Halogen-5-nitro-1, 4-benzoldicarbonsaeuren | |
| DE767510C (de) | Verfahren zur Herstellung von 1, 3, 5-Trichlor-2, 4, 6-Trinitrobenzol | |
| DE63485C (de) | Verfahren zur Darstellung von p-Phenetol- und p Anisolcarbamid | |
| DE269746C (cs) | ||
| AT167275B (de) | Verfahren zur Herstellung von Sulfonamiden der Thiazolreihe | |
| DE163516C (cs) |