DE105797C - - Google Patents
Info
- Publication number
- DE105797C DE105797C DENDAT105797D DE105797DA DE105797C DE 105797 C DE105797 C DE 105797C DE NDAT105797 D DENDAT105797 D DE NDAT105797D DE 105797D A DE105797D A DE 105797DA DE 105797 C DE105797 C DE 105797C
- Authority
- DE
- Germany
- Prior art keywords
- toluidine
- xylidine
- formaldehyde
- parts
- anhydroformaldehyde
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 27
- RZXMPPFPUUCRFN-UHFFFAOYSA-N p-toluidine Chemical compound CC1=CC=C(N)C=C1 RZXMPPFPUUCRFN-UHFFFAOYSA-N 0.000 claims description 26
- AFBPFSWMIHJQDM-UHFFFAOYSA-N N-methyl-N-phenylamine Natural products CNC1=CC=CC=C1 AFBPFSWMIHJQDM-UHFFFAOYSA-N 0.000 claims description 13
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 6
- UAJWDYLSRSNGFH-UHFFFAOYSA-N 1,3,5-tris(4-methylphenyl)-1,3,5-triazinane Chemical compound C1=CC(C)=CC=C1N1CN(C=2C=CC(C)=CC=2)CN(C=2C=CC(C)=CC=2)C1 UAJWDYLSRSNGFH-UHFFFAOYSA-N 0.000 claims description 5
- 150000001412 amines Chemical class 0.000 claims description 5
- 239000007859 condensation product Substances 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- CZZZABOKJQXEBO-UHFFFAOYSA-N 2,4-dimethylaniline Chemical group CC1=CC=C(N)C(C)=C1 CZZZABOKJQXEBO-UHFFFAOYSA-N 0.000 claims 6
- LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 claims 4
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 3
- 238000010438 heat treatment Methods 0.000 claims 3
- JQKBUTDZZRGQDR-UHFFFAOYSA-N hydron;4-methylaniline;chloride Chemical compound Cl.CC1=CC=C(N)C=C1 JQKBUTDZZRGQDR-UHFFFAOYSA-N 0.000 claims 3
- 238000000034 method Methods 0.000 claims 3
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- -1 acetone compound Chemical class 0.000 claims 2
- 230000008018 melting Effects 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 claims 1
- CSCPPACGZOOCGX-UHFFFAOYSA-N acetone Substances CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 239000000155 melt Substances 0.000 claims 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 claims 1
- 229910052757 nitrogen Inorganic materials 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 150000003142 primary aromatic amines Chemical class 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 150000004992 toluidines Chemical group 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- NKDDWNXOKDWJAK-UHFFFAOYSA-N dimethoxymethane Chemical compound COCOC NKDDWNXOKDWJAK-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE105797C true DE105797C (enrdf_load_stackoverflow) |
Family
ID=376045
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT105797D Active DE105797C (enrdf_load_stackoverflow) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE105797C (enrdf_load_stackoverflow) |
-
0
- DE DENDAT105797D patent/DE105797C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE105797C (enrdf_load_stackoverflow) | ||
| DE3001752A1 (de) | Verfahren zur herstellung von 8(alpha)-substituierten 6-methylergolinen | |
| DE107718C (enrdf_load_stackoverflow) | ||
| DE922467C (de) | Verfahren zur Herstellung von N-Derivaten des Phenothiazins | |
| DE495337C (de) | Verfahren zur Darstellung organischer Basen | |
| DE134979C (de) | Verfahren zur darstellung von benzylphtalimiden | |
| DE105199C (enrdf_load_stackoverflow) | ||
| DE113723C (enrdf_load_stackoverflow) | ||
| DE104230C (enrdf_load_stackoverflow) | ||
| DE71320C (de) | Verfahren zur Darstellung von Auramin. (3 | |
| DE108064C (enrdf_load_stackoverflow) | ||
| DE184808C (enrdf_load_stackoverflow) | ||
| DE495451C (de) | Verfahren zur Gewinnung von N-substituierten, aromatischen Aminen aus den bei der Doebnerschen Synthese in 2-Stellung substituierter Chinolin-4-carbonsaeuren anfallendenharzigen Rueckstaenden | |
| DE634275C (de) | Verfahren zur Darstellung von N-Arylglukaminen | |
| DE1670543C (de) | Substituierte 2 Morpholino 4 piperazi no 6 amino s triazine | |
| DE280971C (enrdf_load_stackoverflow) | ||
| DE123260C (enrdf_load_stackoverflow) | ||
| DE175024C (enrdf_load_stackoverflow) | ||
| DE200203C (enrdf_load_stackoverflow) | ||
| AT240358B (de) | Verfahren zur Herstellung von 1, 5-disubstituierten Tetrazolen | |
| DE815043C (de) | Verfahren zur Herstellung von Derivaten des 1-(p-Oxyphenyl)-2-amino-propanols-(1) | |
| DE96852C (enrdf_load_stackoverflow) | ||
| DE2316320A1 (de) | Verfahren zur herstellung von 5-amino-2-(beta-cyanoaethyl)-5-cyclohexen-1-on | |
| DE1233411B (de) | Verfahren zur Herstellung von 3, 4-Dihydropyranyl-2-methyl-aminen | |
| DE184850A (enrdf_load_stackoverflow) |