DE102017104872A1 - ATR Spektrometer und Verfahren zum Analysieren der chemischen Zusammensetzung einer Probe - Google Patents
ATR Spektrometer und Verfahren zum Analysieren der chemischen Zusammensetzung einer Probe Download PDFInfo
- Publication number
- DE102017104872A1 DE102017104872A1 DE102017104872.3A DE102017104872A DE102017104872A1 DE 102017104872 A1 DE102017104872 A1 DE 102017104872A1 DE 102017104872 A DE102017104872 A DE 102017104872A DE 102017104872 A1 DE102017104872 A1 DE 102017104872A1
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- Germany
- Prior art keywords
- infrared light
- light detectors
- atr
- wavelength
- sample
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
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- 239000000126 substance Substances 0.000 title claims abstract description 13
- 238000000034 method Methods 0.000 title claims description 12
- 238000001228 spectrum Methods 0.000 claims abstract description 65
- 239000011159 matrix material Substances 0.000 claims abstract description 46
- 239000013078 crystal Substances 0.000 claims abstract description 39
- 230000003993 interaction Effects 0.000 claims abstract description 8
- 239000000523 sample Substances 0.000 claims description 52
- 230000001419 dependent effect Effects 0.000 claims description 35
- 230000008033 biological extinction Effects 0.000 claims description 17
- 230000003595 spectral effect Effects 0.000 claims description 16
- 238000010521 absorption reaction Methods 0.000 claims description 14
- 238000005033 Fourier transform infrared spectroscopy Methods 0.000 claims description 5
- 230000005540 biological transmission Effects 0.000 claims description 5
- 239000013074 reference sample Substances 0.000 claims description 5
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 claims description 3
- 238000002835 absorbance Methods 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 8
- 238000000862 absorption spectrum Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 238000004566 IR spectroscopy Methods 0.000 description 3
- 238000012569 chemometric method Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000010238 partial least squares regression Methods 0.000 description 2
- 230000003466 anti-cipated effect Effects 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 230000002123 temporal effect Effects 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/28—Investigating the spectrum
- G01J3/2803—Investigating the spectrum using photoelectric array detector
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/28—Investigating the spectrum
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/28—Investigating the spectrum
- G01J3/30—Measuring the intensity of spectral lines directly on the spectrum itself
- G01J3/36—Investigating two or more bands of a spectrum by separate detectors
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/28—Investigating the spectrum
- G01J3/42—Absorption spectrometry; Double beam spectrometry; Flicker spectrometry; Reflection spectrometry
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/27—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands using photo-electric detection ; circuits for computing concentration
- G01N21/274—Calibration, base line adjustment, drift correction
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/55—Specular reflectivity
- G01N21/552—Attenuated total reflection
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/28—Investigating the spectrum
- G01J2003/2866—Markers; Calibrating of scan
- G01J2003/2869—Background correcting
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/02—Details
- G01J3/0205—Optical elements not provided otherwise, e.g. optical manifolds, diffusers, windows
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3563—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing solids; Preparation of samples therefor
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3577—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing liquids, e.g. polluted water
Landscapes
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- General Physics & Mathematics (AREA)
- Biochemistry (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Mathematical Physics (AREA)
- Theoretical Computer Science (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102017104872.3A DE102017104872A1 (de) | 2017-03-08 | 2017-03-08 | ATR Spektrometer und Verfahren zum Analysieren der chemischen Zusammensetzung einer Probe |
| PCT/EP2018/055319 WO2018162398A1 (en) | 2017-03-08 | 2018-03-05 | Atr spectrometer and method for analysing the chemical composition of a sample |
| JP2019548903A JP7241021B2 (ja) | 2017-03-08 | 2018-03-05 | Atr分光計及びサンプルの化学組成を分析する方法 |
| US16/491,068 US11248958B2 (en) | 2017-03-08 | 2018-03-05 | ATR spectrometer and method for analysing the chemical composition of a sample |
| EP18712092.8A EP3593118B1 (en) | 2017-03-08 | 2018-03-05 | Atr spectrometer and method for analysing the chemical composition of a sample |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102017104872.3A DE102017104872A1 (de) | 2017-03-08 | 2017-03-08 | ATR Spektrometer und Verfahren zum Analysieren der chemischen Zusammensetzung einer Probe |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE102017104872A1 true DE102017104872A1 (de) | 2018-09-13 |
Family
ID=61691925
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE102017104872.3A Withdrawn DE102017104872A1 (de) | 2017-03-08 | 2017-03-08 | ATR Spektrometer und Verfahren zum Analysieren der chemischen Zusammensetzung einer Probe |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US11248958B2 (https=) |
| EP (1) | EP3593118B1 (https=) |
| JP (1) | JP7241021B2 (https=) |
| DE (1) | DE102017104872A1 (https=) |
| WO (1) | WO2018162398A1 (https=) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115993342A (zh) | 2021-10-15 | 2023-04-21 | 谱钜科技股份有限公司 | 药物扫描与辨识系统及其使用方法 |
| TWI809530B (zh) * | 2021-10-15 | 2023-07-21 | 譜鉅科技股份有限公司 | 藥物掃描與辨識系統及其使用方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030176775A1 (en) | 1998-10-13 | 2003-09-18 | Medoptix, Inc. | Cleaning kit for an infrared glucose measurement system |
| DE102013005372A1 (de) | 2013-03-28 | 2014-10-02 | Spectrolytic GmbH | Vorrichtung zur spektroskopischen Messwerterfassung von physikalischen und/oder chemischen Parametern eines Messobjektes |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59171837A (ja) | 1983-03-19 | 1984-09-28 | Japan Spectroscopic Co | 赤外分光装置による透過率測定におけるデ−タ補正方法 |
| US5460973A (en) * | 1994-12-20 | 1995-10-24 | Ceramoptec Industries Inc. | Method for continuous determination of volatile impurities in contaminated medium |
| US5731581A (en) * | 1995-03-13 | 1998-03-24 | Ohmeda Inc. | Apparatus for automatic identification of gas samples |
| JP4127195B2 (ja) | 2003-11-21 | 2008-07-30 | コニカミノルタセンシング株式会社 | 分光強度測定装置およびその校正方法ならびに分光反射特性測定装置およびその校正方法 |
| JP2008197043A (ja) | 2007-02-15 | 2008-08-28 | Yokogawa Electric Corp | 光信号測定装置 |
| EP2133478A3 (en) * | 2008-02-27 | 2011-10-05 | Jsm Healthcare Inc | Apparatus for analyzing components of urine by using atr and method thereof |
| DE102008054056A1 (de) * | 2008-10-31 | 2010-05-06 | Carl Zeiss Microimaging Gmbh | Spektrometrische Anordnung und Verfahren zum Ermitteln eines Temperaturwerts für einen Detektor eines Spektrometers |
| DE102009027134A1 (de) * | 2009-06-24 | 2010-12-30 | Robert Bosch Gmbh | Spektroskopischer Sensor und Messverfahren zur Bestimmung mindestens einer Konzentration |
| AT512291B1 (de) * | 2012-02-20 | 2013-07-15 | Anton Paar Gmbh | Verfahren und vorrichtung zur bestimmung des co2-gehalts in einer flüssigkeit |
| WO2015050791A1 (en) | 2013-10-04 | 2015-04-09 | The Research Foundation For The State University Of New York | Spectroscopy for gunshot residue analysis |
| DE102013114244B3 (de) | 2013-12-17 | 2015-01-22 | Pyreos Ltd. | ATR-Infrarotspektrometer |
| US9182280B1 (en) | 2014-08-08 | 2015-11-10 | Thermo Scientific Portable Analytical Instruments Inc. | Method for reducing frequency of taking background/reference spectra in FTIR or FTIR-ATR spectroscopy and handheld measurement device embodying same |
| GB2530098B (en) * | 2014-09-15 | 2017-02-22 | Schlumberger Holdings | Mid-infrared acid sensor |
| DE102014115502A1 (de) | 2014-10-24 | 2016-04-28 | Pyreos Ltd. | Hautmessgerät und Armbanduhr |
| US10066990B2 (en) * | 2015-07-09 | 2018-09-04 | Verifood, Ltd. | Spatially variable filter systems and methods |
-
2017
- 2017-03-08 DE DE102017104872.3A patent/DE102017104872A1/de not_active Withdrawn
-
2018
- 2018-03-05 EP EP18712092.8A patent/EP3593118B1/en active Active
- 2018-03-05 WO PCT/EP2018/055319 patent/WO2018162398A1/en not_active Ceased
- 2018-03-05 US US16/491,068 patent/US11248958B2/en active Active
- 2018-03-05 JP JP2019548903A patent/JP7241021B2/ja active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030176775A1 (en) | 1998-10-13 | 2003-09-18 | Medoptix, Inc. | Cleaning kit for an infrared glucose measurement system |
| DE102013005372A1 (de) | 2013-03-28 | 2014-10-02 | Spectrolytic GmbH | Vorrichtung zur spektroskopischen Messwerterfassung von physikalischen und/oder chemischen Parametern eines Messobjektes |
Also Published As
| Publication number | Publication date |
|---|---|
| JP7241021B2 (ja) | 2023-03-16 |
| WO2018162398A1 (en) | 2018-09-13 |
| EP3593118A1 (en) | 2020-01-15 |
| US11248958B2 (en) | 2022-02-15 |
| EP3593118B1 (en) | 2024-10-30 |
| JP2020513216A (ja) | 2020-05-07 |
| US20200011735A1 (en) | 2020-01-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| R012 | Request for examination validly filed | ||
| R016 | Response to examination communication | ||
| R082 | Change of representative |
Representative=s name: MEWBURN ELLIS LLP, DE |
|
| R119 | Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee |