DE102008021084A1 - Verwendung eines Katalysators auf Edelmetallbasis zur Verringerung des Teergehalts in Gasen aus Vergasungsprozessen - Google Patents

Verwendung eines Katalysators auf Edelmetallbasis zur Verringerung des Teergehalts in Gasen aus Vergasungsprozessen Download PDF

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Publication number
DE102008021084A1
DE102008021084A1 DE102008021084A DE102008021084A DE102008021084A1 DE 102008021084 A1 DE102008021084 A1 DE 102008021084A1 DE 102008021084 A DE102008021084 A DE 102008021084A DE 102008021084 A DE102008021084 A DE 102008021084A DE 102008021084 A1 DE102008021084 A1 DE 102008021084A1
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Germany
Prior art keywords
noble metal
containing catalyst
gasification
tar
catalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
DE102008021084A
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German (de)
English (en)
Inventor
Georg Anfang
Norbert Modl
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Clariant Produkte Deutschland GmbH
Original Assignee
Sued Chemie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sued Chemie AG filed Critical Sued Chemie AG
Priority to DE102008021084A priority Critical patent/DE102008021084A1/de
Priority to JP2011506645A priority patent/JP2011518930A/ja
Priority to US12/989,655 priority patent/US20110101278A1/en
Priority to PCT/EP2009/054429 priority patent/WO2009132959A2/de
Priority to EP09738003.4A priority patent/EP2274094B1/de
Publication of DE102008021084A1 publication Critical patent/DE102008021084A1/de
Ceased legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56—Platinum group metals
    • B01J23/63—Platinum group metals with rare earths or actinides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/83—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with rare earths or actinides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/892—Nickel and noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/024—Multiple impregnation or coating
    • B01J37/0242—Coating followed by impregnation
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J3/00—Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
    • C10J3/72—Other features
    • C10J3/82—Gas withdrawal means
    • C10J3/84—Gas withdrawal means with means for removing dust or tar from the gas
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00—Purifying combustible gases containing carbon monoxide
    • C10K1/34—Purifying combustible gases containing carbon monoxide by catalytic conversion of impurities to more readily removable materials
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K3/00—Modifying the chemical composition of combustible gases containing carbon monoxide to produce an improved fuel, e.g. one of different calorific value, which may be free from carbon monoxide
    • C10K3/02—Modifying the chemical composition of combustible gases containing carbon monoxide to produce an improved fuel, e.g. one of different calorific value, which may be free from carbon monoxide by catalytic treatment
    • C10K3/023—Reducing the tar content
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/46—Ruthenium, rhodium, osmium or iridium
    • B01J23/462—Ruthenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56—Platinum group metals
    • B01J23/64—Platinum group metals with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/656—Manganese, technetium or rhenium
    • B01J23/6567—Rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0205—Impregnation in several steps
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J2300/00—Details of gasification processes
    • C10J2300/09—Details of the feed, e.g. feeding of spent catalyst, inert gas or halogens
    • C10J2300/0913—Carbonaceous raw material
    • C10J2300/0916—Biomass
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J2300/00—Details of gasification processes
    • C10J2300/16—Integration of gasification processes with another plant or parts within the plant
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/32—Hydrogen storage
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Combustion & Propulsion (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Catalysts (AREA)
  • Industrial Gases (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE102008021084A 2008-04-28 2008-04-28 Verwendung eines Katalysators auf Edelmetallbasis zur Verringerung des Teergehalts in Gasen aus Vergasungsprozessen Ceased DE102008021084A1 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
DE102008021084A DE102008021084A1 (de) 2008-04-28 2008-04-28 Verwendung eines Katalysators auf Edelmetallbasis zur Verringerung des Teergehalts in Gasen aus Vergasungsprozessen
JP2011506645A JP2011518930A (ja) 2008-04-28 2009-04-15 ガス化プロセスに由来するガス中のタール含有量を減少させるための貴金属系触媒の使用
US12/989,655 US20110101278A1 (en) 2008-04-28 2009-04-15 Use of a catalyst based on noble metal for reducing the tar content in gases resulting from gasification processes
PCT/EP2009/054429 WO2009132959A2 (de) 2008-04-28 2009-04-15 Verwendung eines katalysators auf edelmetallbasis zur verringerung des teergehalts in gasen aus vergasungsprozessen
EP09738003.4A EP2274094B1 (de) 2008-04-28 2009-04-15 Verwendung eines katalysators auf edelmetallbasis zur verringerung des teergehalts in gasen aus vergasungsprozessen

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102008021084A DE102008021084A1 (de) 2008-04-28 2008-04-28 Verwendung eines Katalysators auf Edelmetallbasis zur Verringerung des Teergehalts in Gasen aus Vergasungsprozessen

Publications (1)

Publication Number Publication Date
DE102008021084A1 true DE102008021084A1 (de) 2009-10-29

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Family Applications (1)

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DE102008021084A Ceased DE102008021084A1 (de) 2008-04-28 2008-04-28 Verwendung eines Katalysators auf Edelmetallbasis zur Verringerung des Teergehalts in Gasen aus Vergasungsprozessen

Country Status (5)

Country Link
US (1) US20110101278A1 (enExample)
EP (1) EP2274094B1 (enExample)
JP (1) JP2011518930A (enExample)
DE (1) DE102008021084A1 (enExample)
WO (1) WO2009132959A2 (enExample)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010007588A1 (de) * 2010-02-05 2011-08-11 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V., 80686 Herstellungsverfahren für ein Synthesegas aus einer Biomasse
DE102011105353A1 (de) 2011-06-22 2012-12-27 Süd-Chemie AG Multifunktionaler Katalysator zur simultanen Entfernung/Umwandlung von teerartigen und schwefelhaltigen Kohlenwasserstoffen
EP2542654A4 (en) * 2010-03-03 2014-12-03 Neste Oil Oyj METHOD FOR REFORMING GASING GAS

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102012111900A1 (de) 2012-12-06 2014-06-26 Krones Ag Vorrichtung und Verfahren zum Cracken von Gasen

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050255995A1 (en) * 2004-05-14 2005-11-17 Gas Technology Institute Method for producing catalytically-active materials
DE102004024672A1 (de) 2004-05-18 2005-12-15 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Vorrichtung und Verfahren zur Erzeugung eines teerfreien Schwachgases durch Vergasung von Biomasse
WO2007044009A1 (en) * 2005-10-07 2007-04-19 Midwest Research Institute Attrition resistant fluidizable reforming catalyst
WO2007116121A1 (en) 2006-04-10 2007-10-18 Valtion Teknillinen Tutkimuskeskus Multiple stage method of reforming a gas containing tarry impurities employing a zirconium-based catalyst

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JP2005112956A (ja) * 2003-10-06 2005-04-28 Nippon Steel Corp バイオマスのガス化方法
KR100569120B1 (ko) * 2004-08-05 2006-04-10 한국에너지기술연구원 바이오메스 정제연료의 저온 촉매가스화 장치 및가스제조방법
US7704486B2 (en) * 2005-02-16 2010-04-27 Basf Corporation Precious metal water-gas shift catalyst with oxide support modified with rare earth elements
RU2438968C2 (ru) * 2005-12-21 2012-01-10 Вайрент, Инк. Катализатор и способ риформинга кислородсодержащих соединений
DE102008021081A1 (de) * 2008-04-28 2009-10-29 Süd-Chemie AG Verfahren zur katalytischen Verringerung des Teergehalts in Gasen aus Vergasungsprozessen unter Verwendung eines Katalysators auf Edelmetallbasis

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Publication number Priority date Publication date Assignee Title
US20050255995A1 (en) * 2004-05-14 2005-11-17 Gas Technology Institute Method for producing catalytically-active materials
DE102004024672A1 (de) 2004-05-18 2005-12-15 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Vorrichtung und Verfahren zur Erzeugung eines teerfreien Schwachgases durch Vergasung von Biomasse
WO2007044009A1 (en) * 2005-10-07 2007-04-19 Midwest Research Institute Attrition resistant fluidizable reforming catalyst
WO2007116121A1 (en) 2006-04-10 2007-10-18 Valtion Teknillinen Tutkimuskeskus Multiple stage method of reforming a gas containing tarry impurities employing a zirconium-based catalyst

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Caballero, Miguel A., Corella, Jose, Aznar, Maria-Pilar and Gil, Javier., Biomass Gasification with Air in Fluidized Bed. Hot Gas Cleanup with Selected Commercial and Full-Size Nickel-Based Catalysts, 2000, 1143-1154
Corella, J., Caballero, M. A., Aznar, M. P. and Gil, J., Biomass gasification with air in fluidized bed: hot gas cleanup and upgrading with steam-reforming catalysts of big size, 1999, 933-938
Corella, Jose, Orio, Alberto and Aznar, Pilar, Biomass Gasification with Air in Fluidized Bed: Reforming of the Gas Composition with Commercial Steam Reforming Catalysts, Ind. Eng. Chem. Res., 1998, 4617-4624
Corella, Jose, Orio, Alberto and Toledo, Jose-Manuel., Biomass Gasification with Air in a Fluidized Bed: Exhaustive Tar Elimination with Commercial Steam Reforming Catalysts, Energy Fuels, 1999, 702-709
Delgado, Jesus, Aznar, Maria P. and Corella, Jose., Biomass Gasification with Steam in Fluidized Bed: Effectiveness of CaO, MgO, and CaO-MgO for Hot Raw Gas Cleaning, Ind. Eng. Chem. Res., 1997, 1535-1543
Delgado, Jesus, Aznar, Maria P. and Corella, Jose., Calcined Dolomite, Magnesite, and Calcite for Cleaning Hot Gas from a Fluidized Bed Biomass Gasifier with Steam: Life and Usefulness, Ind. Eng. Chem. Res., 1996, 3637-3643
Devi L., Nair S. A., Pemen A. J. M. et al., Tar Removal from Biomass Gasification Processes, Biomass and Bioenergy: New Research, 2006, pp. 249-274
Handbook of Heterogeneous Catalysis 4 - Environmental Catalysis, Seiten 1575-1583
Jess, A. (1996) beschreibt in "Mechanisms and kinetics of thermal reactions of aromatic hydrocarbons from pyrolysis of solid fuels", Fuel 75, 1441-1448
Neeft, J. P. A., Knowef, H. A. M., Onaji, P. (1999) weisen in "Behaviour of tar in biomass gasification systems. Tar related Problems and their solutions." Novem, The Netherlands, Report No. 9919
SAXENA,R.C.: Thermo-chemical routes for hydrogen rich gas from biomass: a review. In: Renewable and Sustainable Energy Reviews,2008,S.1909-1927 $S.1918-1924$ *
SAXENA,R.C.: Thermo-chemical routes for hydrogen rich gas from biomass: a review. In: Renewable and Sustainable Energy Reviews,2008,S.1909-1927 S.1918-1924 TOMSHIGE,K.: Catalytic performance of Ni/CeO/A2Omodified with noble metals in steam gasification of biomass. In: Catalysis Today,2008,S.146-155 ges.Artikel
TOMSHIGE,K.: Catalytic performance of Ni/CeO/A2Omodified with noble metals in steam gasification of biomass. In: Catalysis Today,2008,S.146-155 $ges.Artikel$ *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010007588A1 (de) * 2010-02-05 2011-08-11 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V., 80686 Herstellungsverfahren für ein Synthesegas aus einer Biomasse
EP2542654A4 (en) * 2010-03-03 2014-12-03 Neste Oil Oyj METHOD FOR REFORMING GASING GAS
DE102011105353A1 (de) 2011-06-22 2012-12-27 Süd-Chemie AG Multifunktionaler Katalysator zur simultanen Entfernung/Umwandlung von teerartigen und schwefelhaltigen Kohlenwasserstoffen
WO2012175625A1 (de) 2011-06-22 2012-12-27 Süd-Chemie AG Simultane entfernung/umwandlung von teerartigen und schwefelhaltigen kohlenwasserstoffen

Also Published As

Publication number Publication date
WO2009132959A2 (de) 2009-11-05
JP2011518930A (ja) 2011-06-30
EP2274094B1 (de) 2018-10-03
EP2274094A2 (de) 2011-01-19
WO2009132959A3 (de) 2010-08-05
US20110101278A1 (en) 2011-05-05

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