DE102005046250B4 - Anlage zur Abtrennung von organischen Übergangsmetallkomplexkatalysatoren - Google Patents

Anlage zur Abtrennung von organischen Übergangsmetallkomplexkatalysatoren Download PDF

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Publication number
DE102005046250B4
DE102005046250B4 DE102005046250.2A DE102005046250A DE102005046250B4 DE 102005046250 B4 DE102005046250 B4 DE 102005046250B4 DE 102005046250 A DE102005046250 A DE 102005046250A DE 102005046250 B4 DE102005046250 B4 DE 102005046250B4
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Prior art keywords
membrane
hydroformylation
separation step
plant according
reaction mixture
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Expired - Fee Related
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DE102005046250.2A
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German (de)
English (en)
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DE102005046250A1 (de
Inventor
Dr. Dipl.Chem. Wiese Klaus-Diether
Dr. Baumgarten Goetz
Dr. Kuppinger Franz-Felix
Dr. Dipl.-Chem. Möller Oliver
Dr. Dipl.-Chem. Ortmann Dagmara
Dr. Dipl.-Chem. Borgmann Cornelia
Dr. Dipl.-Chem. Büschken Wilfried
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Evonik Operations GmbH
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Evonik Operations GmbH
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Application filed by Evonik Operations GmbH filed Critical Evonik Operations GmbH
Priority to DE102005046250.2A priority Critical patent/DE102005046250B4/de
Priority to US12/088,041 priority patent/US8226829B2/en
Priority to KR1020087007298A priority patent/KR101337117B1/ko
Priority to ES06778422T priority patent/ES2320698T3/es
Priority to DE502006002616T priority patent/DE502006002616D1/de
Priority to CN2006800358000A priority patent/CN101272860B/zh
Priority to AT06778422T priority patent/ATE419917T1/de
Priority to EP06778422A priority patent/EP1931472B1/de
Priority to PCT/EP2006/066181 priority patent/WO2007036424A1/de
Priority to PL06778422T priority patent/PL1931472T3/pl
Priority to JP2008532709A priority patent/JP5091142B2/ja
Priority to TW095134974A priority patent/TWI418396B/zh
Publication of DE102005046250A1 publication Critical patent/DE102005046250A1/de
Publication of DE102005046250B4 publication Critical patent/DE102005046250B4/de
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/027—Nanofiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/22—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/26—Further operations combined with membrane separation processes
    • B01D2311/2653—Degassing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2313/00—Details relating to membrane modules or apparatus
    • B01D2313/14—Specific spacers
    • B01D2313/143—Specific spacers on the feed side
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/30—Chemical resistance
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/38—Hydrophobic membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/32—Addition reactions to C=C or C-C triple bonds
    • B01J2231/321—Hydroformylation, metalformylation, carbonylation or hydroaminomethylation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/822—Rhodium
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Supply & Treatment (AREA)
  • Nanotechnology (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
DE102005046250.2A 2005-09-27 2005-09-27 Anlage zur Abtrennung von organischen Übergangsmetallkomplexkatalysatoren Expired - Fee Related DE102005046250B4 (de)

Priority Applications (12)

Application Number Priority Date Filing Date Title
DE102005046250.2A DE102005046250B4 (de) 2005-09-27 2005-09-27 Anlage zur Abtrennung von organischen Übergangsmetallkomplexkatalysatoren
AT06778422T ATE419917T1 (de) 2005-09-27 2006-09-08 Verfahren zur abtrennung von organischen übergangsmetallkomplexkatalysatoren
PCT/EP2006/066181 WO2007036424A1 (de) 2005-09-27 2006-09-08 Verfahren zur abtrennung von organischen übergangsmetallkomplexkatalysatoren
ES06778422T ES2320698T3 (es) 2005-09-27 2006-09-08 Procedimiento para la separacion de catalizadores complejos organicos de metales de transicion.
DE502006002616T DE502006002616D1 (de) 2005-09-27 2006-09-08 Verfahren zur abtrennung von organischen übergangsmetallkomplexkatalysatoren
CN2006800358000A CN101272860B (zh) 2005-09-27 2006-09-08 有机过渡金属络合催化剂的分离方法
US12/088,041 US8226829B2 (en) 2005-09-27 2006-09-08 Method for separating organic transition metal complex catalysts
EP06778422A EP1931472B1 (de) 2005-09-27 2006-09-08 Verfahren zur abtrennung von organischen übergangsmetallkomplexkatalysatoren
KR1020087007298A KR101337117B1 (ko) 2005-09-27 2006-09-08 유기 전이금속 착물 촉매를 분리하는 방법
PL06778422T PL1931472T3 (pl) 2005-09-27 2006-09-08 Sposób oddzielania organicznych katalizatorów kompleksowych z metalem przejściowym
JP2008532709A JP5091142B2 (ja) 2005-09-27 2006-09-08 有機遷移金属錯体触媒を分離する方法
TW095134974A TWI418396B (zh) 2005-09-27 2006-09-21 分離有機過渡金屬錯合物觸媒的方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102005046250.2A DE102005046250B4 (de) 2005-09-27 2005-09-27 Anlage zur Abtrennung von organischen Übergangsmetallkomplexkatalysatoren

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DE102005046250A1 DE102005046250A1 (de) 2007-03-29
DE102005046250B4 true DE102005046250B4 (de) 2020-10-08

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DE102005046250.2A Expired - Fee Related DE102005046250B4 (de) 2005-09-27 2005-09-27 Anlage zur Abtrennung von organischen Übergangsmetallkomplexkatalysatoren
DE502006002616T Active DE502006002616D1 (de) 2005-09-27 2006-09-08 Verfahren zur abtrennung von organischen übergangsmetallkomplexkatalysatoren

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DE502006002616T Active DE502006002616D1 (de) 2005-09-27 2006-09-08 Verfahren zur abtrennung von organischen übergangsmetallkomplexkatalysatoren

Country Status (11)

Country Link
US (1) US8226829B2 (https=)
EP (1) EP1931472B1 (https=)
JP (1) JP5091142B2 (https=)
KR (1) KR101337117B1 (https=)
CN (1) CN101272860B (https=)
AT (1) ATE419917T1 (https=)
DE (2) DE102005046250B4 (https=)
ES (1) ES2320698T3 (https=)
PL (1) PL1931472T3 (https=)
TW (1) TWI418396B (https=)
WO (1) WO2007036424A1 (https=)

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DE102007054885A1 (de) * 2007-11-15 2009-05-20 Evonik Degussa Gmbh Verfahren zur Fraktionierung oxidischer Nanopartikel durch Querstrom-Membranfiltration
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DE102008002188A1 (de) 2008-06-03 2009-12-10 Evonik Oxeno Gmbh Verfahren zur Abtrennung von 1-Buten aus C4-haltigen Kohlenwasserstoffströmen durch Hydroformylierung
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DE102013203117A1 (de) * 2013-02-26 2014-08-28 Evonik Industries Ag Optimierte Trenntechnik zur Aufarbeitung von homogen katalysierten Hydroformylierungsmischungen
DE102013208759A1 (de) * 2013-05-13 2014-11-13 Evonik Industries Ag Abtrennung von Homogenkatalysatoren mittels einer geregelten Membrantrenneinheit
DE102013215004A1 (de) * 2013-07-31 2015-02-05 Evonik Industries Ag Membrankaskade mit sinkender Trenntemperatur
DE102013221708A1 (de) 2013-10-25 2015-04-30 Evonik Industries Ag Strahlschlaufenreaktor mit Nanofiltration und Gasseparator
DE102014002103B4 (de) 2014-02-15 2020-10-22 Oxea Gmbh Verfahren zur Regenerierung gebrauchter Hydroformylierungskatalysatoren
US10155200B2 (en) * 2015-02-18 2018-12-18 Evonik Degussa Gmbh Separation off of a homogeneous catalyst from a reaction mixture with the help of organophilic nanofiltration
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CN113996340B (zh) * 2021-11-16 2023-12-19 万华化学集团股份有限公司 一种用于氢甲酰化反应的新型催化剂体系及氢甲酰化反应方法
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Publication number Publication date
DE102005046250A1 (de) 2007-03-29
ATE419917T1 (de) 2009-01-15
PL1931472T3 (pl) 2009-06-30
JP2009513320A (ja) 2009-04-02
US8226829B2 (en) 2012-07-24
DE502006002616D1 (de) 2009-02-26
KR101337117B1 (ko) 2013-12-05
TW200719947A (en) 2007-06-01
JP5091142B2 (ja) 2012-12-05
EP1931472A1 (de) 2008-06-18
TWI418396B (zh) 2013-12-11
US20080251456A1 (en) 2008-10-16
ES2320698T3 (es) 2009-05-27
WO2007036424A1 (de) 2007-04-05
CN101272860A (zh) 2008-09-24
CN101272860B (zh) 2010-11-17
KR20080053476A (ko) 2008-06-13
EP1931472B1 (de) 2009-01-07

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