DE102005020781A1 - Zirkondioxid und Aluminiumoxid enthaltender Schlicker und daraus erhältlicher Formkörper - Google Patents
Zirkondioxid und Aluminiumoxid enthaltender Schlicker und daraus erhältlicher Formkörper Download PDFInfo
- Publication number
- DE102005020781A1 DE102005020781A1 DE102005020781A DE102005020781A DE102005020781A1 DE 102005020781 A1 DE102005020781 A1 DE 102005020781A1 DE 102005020781 A DE102005020781 A DE 102005020781A DE 102005020781 A DE102005020781 A DE 102005020781A DE 102005020781 A1 DE102005020781 A1 DE 102005020781A1
- Authority
- DE
- Germany
- Prior art keywords
- zirconia
- alumina
- slip
- powder
- slip according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 title claims abstract description 107
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 title claims abstract description 43
- 238000000465 moulding Methods 0.000 title claims description 10
- 239000000843 powder Substances 0.000 claims abstract description 45
- 239000002245 particle Substances 0.000 claims abstract description 39
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000002002 slurry Substances 0.000 claims abstract description 14
- 238000002441 X-ray diffraction Methods 0.000 claims abstract description 6
- 239000007787 solid Substances 0.000 claims abstract description 5
- 238000010586 diagram Methods 0.000 claims abstract description 4
- 229910002076 stabilized zirconia Inorganic materials 0.000 claims abstract description 3
- 239000006185 dispersion Substances 0.000 claims description 27
- 239000012071 phase Substances 0.000 claims description 14
- 239000000654 additive Substances 0.000 claims description 12
- 238000002360 preparation method Methods 0.000 claims description 12
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000011148 porous material Substances 0.000 claims description 4
- 239000004035 construction material Substances 0.000 claims description 3
- 239000007791 liquid phase Substances 0.000 claims description 3
- 210000000988 bone and bone Anatomy 0.000 claims description 2
- 239000007943 implant Substances 0.000 claims description 2
- 239000004094 surface-active agent Substances 0.000 claims 1
- 238000009826 distribution Methods 0.000 description 9
- 239000000203 mixture Substances 0.000 description 6
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 6
- 238000012360 testing method Methods 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000001257 hydrogen Substances 0.000 description 4
- 229910052739 hydrogen Inorganic materials 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000003607 modifier Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 125000000524 functional group Chemical group 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000011164 primary particle Substances 0.000 description 3
- 229910052726 zirconium Inorganic materials 0.000 description 3
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 description 2
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000002902 bimodal effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 230000009918 complex formation Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003822 epoxy resin Substances 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- CJNBYAVZURUTKZ-UHFFFAOYSA-N hafnium(iv) oxide Chemical compound O=[Hf]=O CJNBYAVZURUTKZ-UHFFFAOYSA-N 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000011505 plaster Substances 0.000 description 2
- 229920000647 polyepoxide Polymers 0.000 description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 230000000087 stabilizing effect Effects 0.000 description 2
- WGTYBPLFGIVFAS-UHFFFAOYSA-M tetramethylammonium hydroxide Chemical compound [OH-].C[N+](C)(C)C WGTYBPLFGIVFAS-UHFFFAOYSA-M 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- OAYXUHPQHDHDDZ-UHFFFAOYSA-N 2-(2-butoxyethoxy)ethanol Chemical compound CCCCOCCOCCO OAYXUHPQHDHDDZ-UHFFFAOYSA-N 0.000 description 1
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical group CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- DFPAKSUCGFBDDF-UHFFFAOYSA-N Nicotinamide Chemical group NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 description 1
- -1 SH groups Chemical group 0.000 description 1
- 229910008051 Si-OH Inorganic materials 0.000 description 1
- 229910006358 Si—OH Inorganic materials 0.000 description 1
- 238000003917 TEM image Methods 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- OBETXYAYXDNJHR-UHFFFAOYSA-N alpha-ethylcaproic acid Natural products CCCCC(CC)C(O)=O OBETXYAYXDNJHR-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 150000008064 anhydrides Chemical group 0.000 description 1
- 125000002843 carboxylic acid group Chemical group 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000002296 dynamic light scattering Methods 0.000 description 1
- 125000003700 epoxy group Chemical group 0.000 description 1
- 125000004185 ester group Chemical group 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000003966 growth inhibitor Substances 0.000 description 1
- 239000012456 homogeneous solution Substances 0.000 description 1
- XFXPMWWXUTWYJX-UHFFFAOYSA-N isonitrile group Chemical group N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 238000013001 point bending Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- XPGAWFIWCWKDDL-UHFFFAOYSA-N propan-1-olate;zirconium(4+) Chemical compound [Zr+4].CCC[O-].CCC[O-].CCC[O-].CCC[O-] XPGAWFIWCWKDDL-UHFFFAOYSA-N 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 125000001302 tertiary amino group Chemical group 0.000 description 1
- 150000005622 tetraalkylammonium hydroxides Chemical class 0.000 description 1
- 229940073455 tetraethylammonium hydroxide Drugs 0.000 description 1
- LRGJRHZIDJQFCL-UHFFFAOYSA-M tetraethylazanium;hydroxide Chemical compound [OH-].CC[N+](CC)(CC)CC LRGJRHZIDJQFCL-UHFFFAOYSA-M 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
- C04B35/111—Fine ceramics
- C04B35/117—Composites
- C04B35/119—Composites with zirconium oxide
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Composite Materials (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Compositions Of Oxide Ceramics (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005020781A DE102005020781A1 (de) | 2005-05-04 | 2005-05-04 | Zirkondioxid und Aluminiumoxid enthaltender Schlicker und daraus erhältlicher Formkörper |
| US11/913,412 US7700034B2 (en) | 2005-05-04 | 2006-04-27 | Slip containing zirconium dioxide and aluminum oxide and shaped body obtainable therefrom |
| PCT/EP2006/061864 WO2006117318A1 (en) | 2005-05-04 | 2006-04-27 | Slip containing zirconium dioxide and aluminium oxide and shaped body obtainable therefrom |
| JP2008509417A JP2008540305A (ja) | 2005-05-04 | 2006-04-27 | 二酸化ジルコニウム及び酸化アルミニウムを有するスリップ、並びにそれらから得られる成形体 |
| EP06754875A EP1896378A1 (en) | 2005-05-04 | 2006-04-27 | Slip containing zirconium dioxide and aluminium oxide and shaped body obtainable therefrom |
| CN200680014926XA CN101171208B (zh) | 2005-05-04 | 2006-04-27 | 含二氧化锆和氧化铝的泥釉及由此得到的成形体 |
| TW095115757A TWI333940B (en) | 2005-05-04 | 2006-05-03 | Slip containing zirconium dioxide and aluminium oxide and shaped body obtainable therefrom |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005020781A DE102005020781A1 (de) | 2005-05-04 | 2005-05-04 | Zirkondioxid und Aluminiumoxid enthaltender Schlicker und daraus erhältlicher Formkörper |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE102005020781A1 true DE102005020781A1 (de) | 2006-11-09 |
Family
ID=36685923
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE102005020781A Withdrawn DE102005020781A1 (de) | 2005-05-04 | 2005-05-04 | Zirkondioxid und Aluminiumoxid enthaltender Schlicker und daraus erhältlicher Formkörper |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7700034B2 (https=) |
| EP (1) | EP1896378A1 (https=) |
| JP (1) | JP2008540305A (https=) |
| CN (1) | CN101171208B (https=) |
| DE (1) | DE102005020781A1 (https=) |
| TW (1) | TWI333940B (https=) |
| WO (1) | WO2006117318A1 (https=) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102008044906A1 (de) * | 2008-08-29 | 2010-03-04 | Ibu-Tec Advanced Materials Ag | Verfahren zur Herstellung eines feinteiligen Pulverwerkstoffs sowie ein solcher Pulverwerkstoff |
| EP2248614B1 (de) * | 2009-04-30 | 2011-11-16 | Evonik Degussa GmbH | Dispersion, Schlicker und Verfahren zur Herstellung einer Gießform für den Präzisionsguss unter Verwendung des Schlickers |
| AU2010340892B2 (en) * | 2009-12-16 | 2014-10-09 | Ceramtec Gmbh | Ceramic composite material consisting of aluminium oxide and zirconium oxide as main constituents |
| US9434651B2 (en) | 2012-05-26 | 2016-09-06 | James R. Glidewell Dental Ceramics, Inc. | Method of fabricating high light transmission zirconia blanks for milling into natural appearance dental appliances |
| JP5954830B2 (ja) * | 2013-03-04 | 2016-07-20 | 株式会社ソディック | 表面改質方法 |
| CN104692431B (zh) * | 2015-03-24 | 2016-03-30 | 哈尔滨工业大学 | 一种亚微米级晶体结构与粒径可控的球形α-Al2O3/t-ZrO2复相粉体的制备方法 |
| JP6973734B2 (ja) * | 2017-11-29 | 2021-12-01 | 昭和電工株式会社 | アルミナ質焼結体用組成物及びその製造方法、並びにアルミナ質焼結体の製造方法 |
| CN110078480B (zh) * | 2019-04-18 | 2022-01-28 | 常州华森医疗器械股份有限公司 | 一种人工关节用陶瓷复合材料及其制备方法 |
| US11731312B2 (en) | 2020-01-29 | 2023-08-22 | James R. Glidewell Dental Ceramics, Inc. | Casting apparatus, cast zirconia ceramic bodies and methods for making the same |
| CN117467199B (zh) * | 2023-10-30 | 2026-04-14 | 信维电子科技(益阳)有限公司 | 一种隔离粉末、隔离粉末的制备方法及应用方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3630754A (en) * | 1969-05-07 | 1971-12-28 | Truman Benjamin Wayne | Milling of cereal grains and processing of products derived therefrom |
| US4298385A (en) * | 1976-11-03 | 1981-11-03 | Max-Planck-Gesellschaft Zur Forderung Wissenschaften E.V. | High-strength ceramic bodies |
| AU573631B2 (en) * | 1983-10-17 | 1988-06-16 | Tosoh Corporation | High strength zirconia type sintered body |
| JPS60131860A (ja) * | 1983-12-19 | 1985-07-13 | 呉羽化学工業株式会社 | アルミナ・ジルコニアセラミツク粉体とその製造方法 |
| US4525464A (en) * | 1984-06-12 | 1985-06-25 | Max-Planck-Gesellschaft Zur Forderung Der Wissenschaften | Ceramic body of zirconium dioxide (ZrO2) and method for its preparation |
| CA1259080A (en) * | 1985-09-06 | 1989-09-05 | Nobuo Kimura | High density alumina zirconia ceramics and a process for production thereof |
| AT389882B (de) * | 1986-06-03 | 1990-02-12 | Treibacher Chemische Werke Ag | Verfahren zur herstellung eines mikrokristallinen schleifmaterials |
| JPS63103859A (ja) * | 1986-10-22 | 1988-05-09 | 岩尾磁器工業株式会社 | アルミナ−ジルコニア焼結体の製造方法 |
| US5183610A (en) * | 1987-07-22 | 1993-02-02 | Cooper Indusries, Inc. | Alumina-zirconia ceramic |
| DE4411862A1 (de) * | 1994-04-06 | 1995-10-12 | Inst Neue Mat Gemein Gmbh | Verfahren zur Herstellung homogener Mehrkomponenten-Dispersionen und davon abgeleiteter Produkte |
| DE4445205A1 (de) * | 1994-12-17 | 1996-06-20 | Degussa | Zirkondioxidpulver, Verfahren zu seiner Herstellung und Verwendung |
| JP2001240460A (ja) * | 1999-12-24 | 2001-09-04 | Sumitomo Chem Co Ltd | アルミナ・ジルコニア複合焼結体およびその製造方法 |
-
2005
- 2005-05-04 DE DE102005020781A patent/DE102005020781A1/de not_active Withdrawn
-
2006
- 2006-04-27 CN CN200680014926XA patent/CN101171208B/zh not_active Expired - Fee Related
- 2006-04-27 WO PCT/EP2006/061864 patent/WO2006117318A1/en not_active Ceased
- 2006-04-27 US US11/913,412 patent/US7700034B2/en not_active Expired - Fee Related
- 2006-04-27 JP JP2008509417A patent/JP2008540305A/ja active Pending
- 2006-04-27 EP EP06754875A patent/EP1896378A1/en not_active Withdrawn
- 2006-05-03 TW TW095115757A patent/TWI333940B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| US20080258358A1 (en) | 2008-10-23 |
| TWI333940B (en) | 2010-12-01 |
| WO2006117318A1 (en) | 2006-11-09 |
| CN101171208B (zh) | 2010-12-22 |
| TW200710062A (en) | 2007-03-16 |
| US7700034B2 (en) | 2010-04-20 |
| JP2008540305A (ja) | 2008-11-20 |
| CN101171208A (zh) | 2008-04-30 |
| EP1896378A1 (en) | 2008-03-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8127 | New person/name/address of the applicant |
Owner name: DEGUSSA GMBH, 40474 DUESSELDORF, DE |
|
| 8127 | New person/name/address of the applicant |
Owner name: EVONIK DEGUSSA GMBH, 40474 DUESSELDORF, DE |
|
| 8181 | Inventor (new situation) |
Inventor name: OSWALD, MONIKA, DR., 63454 HANAU, DE Inventor name: NIKOLAY, DIETER, 56745 BELL, DE Inventor name: KOLLENBERG, WOLFGANG, PROF., 50321 BRUEHL, DE Inventor name: DELLER, KLAUS, DR., 63512 HAINBURG, DE |
|
| R119 | Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee |
Effective date: 20111201 |