DD158228A5 - Pyrogen hergestellte kieselsaeure und verfahren zu ihrer herstellung - Google Patents
Pyrogen hergestellte kieselsaeure und verfahren zu ihrer herstellung Download PDFInfo
- Publication number
- DD158228A5 DD158228A5 DD81229359A DD22935981A DD158228A5 DD 158228 A5 DD158228 A5 DD 158228A5 DD 81229359 A DD81229359 A DD 81229359A DD 22935981 A DD22935981 A DD 22935981A DD 158228 A5 DD158228 A5 DD 158228A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- silica
- mixture
- mpas
- siloxane
- hexamethyldisiloxane
- Prior art date
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 64
- 239000000377 silicon dioxide Substances 0.000 title claims abstract description 25
- 238000000034 method Methods 0.000 title claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 21
- UQEAIHBTYFGYIE-UHFFFAOYSA-N hexamethyldisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)C UQEAIHBTYFGYIE-UHFFFAOYSA-N 0.000 claims abstract description 13
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000005049 silicon tetrachloride Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 7
- JLUFWMXJHAVVNN-UHFFFAOYSA-N methyltrichlorosilane Chemical compound C[Si](Cl)(Cl)Cl JLUFWMXJHAVVNN-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000001257 hydrogen Substances 0.000 claims description 12
- 229910052739 hydrogen Inorganic materials 0.000 claims description 12
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 11
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 claims description 10
- 101000588924 Anthopleura elegantissima Delta-actitoxin-Ael1a Proteins 0.000 claims description 5
- -1 siloxanes Chemical class 0.000 claims description 5
- 239000005055 methyl trichlorosilane Substances 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 229920006305 unsaturated polyester Polymers 0.000 claims description 3
- 239000004215 Carbon black (E152) Substances 0.000 claims description 2
- 229930195733 hydrocarbon Natural products 0.000 claims description 2
- 150000002430 hydrocarbons Chemical class 0.000 claims description 2
- 239000007858 starting material Substances 0.000 claims description 2
- 230000001698 pyrogenic effect Effects 0.000 abstract description 3
- 230000008719 thickening Effects 0.000 description 17
- 229910021485 fumed silica Inorganic materials 0.000 description 15
- 230000000694 effects Effects 0.000 description 11
- 238000012360 testing method Methods 0.000 description 10
- 239000000047 product Substances 0.000 description 8
- 238000001816 cooling Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000007795 chemical reaction product Substances 0.000 description 5
- 239000003973 paint Substances 0.000 description 5
- 239000004033 plastic Substances 0.000 description 5
- 239000000606 toothpaste Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 229940034610 toothpaste Drugs 0.000 description 4
- 229920006337 unsaturated polyester resin Polymers 0.000 description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
- 239000000460 chlorine Substances 0.000 description 3
- 229910052801 chlorine Inorganic materials 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 239000006072 paste Substances 0.000 description 3
- 229920001225 polyester resin Polymers 0.000 description 3
- 239000004645 polyester resin Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000012188 paraffin wax Substances 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- DDJSWKLBKSLAAZ-UHFFFAOYSA-N cyclotetrasiloxane Chemical compound O1[SiH2]O[SiH2]O[SiH2]O[SiH2]1 DDJSWKLBKSLAAZ-UHFFFAOYSA-N 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 239000000551 dentifrice Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000003475 lamination Methods 0.000 description 1
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 1
- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 125000002467 phosphate group Chemical group [H]OP(=O)(O[H])O[*] 0.000 description 1
- CKRORYDHXIRZCH-UHFFFAOYSA-N phosphoric acid;dihydrate Chemical compound O.O.OP(O)(O)=O CKRORYDHXIRZCH-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 125000005624 silicic acid group Chemical class 0.000 description 1
- XUIMIQQOPSSXEZ-AKLPVKDBSA-N silicon-31 atom Chemical compound [31Si] XUIMIQQOPSSXEZ-AKLPVKDBSA-N 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/181—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process
- C01B33/183—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process by oxidation or hydrolysis in the vapour phase of silicon compounds such as halides, trichlorosilane, monosilane
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Medicinal Chemistry (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Silicon Compounds (AREA)
- Cosmetics (AREA)
- Saccharide Compounds (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3016010A DE3016010C2 (de) | 1980-04-25 | 1980-04-25 | Verfahren zur pyrogenen Herstellung von Kieselsäure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD158228A5 true DD158228A5 (de) | 1983-01-05 |
Family
ID=6100961
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD81229359A DD158228A5 (de) | 1980-04-25 | 1981-04-21 | Pyrogen hergestellte kieselsaeure und verfahren zu ihrer herstellung |
Country Status (7)
| Country | Link |
|---|---|
| EP (2) | EP0092024B1 (enExample) |
| JP (2) | JPS56164009A (enExample) |
| AT (1) | ATE14562T1 (enExample) |
| BR (1) | BR8102491A (enExample) |
| DD (1) | DD158228A5 (enExample) |
| DE (2) | DE3016010C2 (enExample) |
| SU (1) | SU1421256A3 (enExample) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4386117A (en) * | 1981-11-20 | 1983-05-31 | Gordon Roy G | Coating process using alkoxy substituted silicon-bearing reactant |
| GB8905966D0 (en) * | 1989-03-15 | 1989-04-26 | Tsl Group Plc | Improved vitreous silica products |
| US5152819A (en) * | 1990-08-16 | 1992-10-06 | Corning Incorporated | Method of making fused silica |
| CN1211264A (zh) | 1996-12-16 | 1999-03-17 | 康宁股份有限公司 | 制造锗掺杂的二氧化硅用的原料及制造方法 |
| US6487879B1 (en) | 1997-03-07 | 2002-12-03 | Corning Incorporated | Method of making titania-doped fused silica |
| RU2154126C1 (ru) * | 1999-06-01 | 2000-08-10 | Дагестанский государственный университет | Способ получения пероксомонокремниевой кислоты |
| DE19936478A1 (de) * | 1999-08-03 | 2001-02-15 | Degussa | Sinterwerkstoffe |
| EP1122212B1 (en) * | 1999-11-11 | 2003-07-09 | Degussa AG | Composite carbon clack-fumed silica nanostructured particles |
| DE10302914B4 (de) * | 2003-01-24 | 2005-12-29 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zur Herstellung von synthetischem Quarzglas |
| DE10326049A1 (de) * | 2003-06-10 | 2004-12-30 | Degussa Ag | Flammenhydrolytisch hergestelltes Siliciumdioxid, Verfahren zu seiner Herstellung und Verwendung |
| US7824644B2 (en) | 2005-05-19 | 2010-11-02 | Tokuyama Corporation | Particulate silica |
| DE102011121356A1 (de) | 2011-12-19 | 2013-06-20 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zur Herstellung von synthetischem Quarzglas |
| WO2015003873A1 (de) | 2013-07-11 | 2015-01-15 | Evonik Industries Ag | Verfahren zur herstellung von kieselsäure mit variabler verdickung |
| EP3002262B1 (de) | 2014-10-01 | 2018-06-27 | Heraeus Quarzglas GmbH & Co. KG | Verfahren zur Herstellung von synthetischem Quarzglas mittels einer polymerisierbaren Polyalkylsiloxanverbindung |
| EP3034476A1 (de) | 2014-12-16 | 2016-06-22 | Heraeus Quarzglas GmbH & Co. KG | Verfahren zur herstellung von synthetischem quarzglas unter verwendung einer reinigungsvorrichtung |
| EP3059212A1 (de) | 2015-02-18 | 2016-08-24 | Heraeus Quarzglas GmbH & Co. KG | Verfahren und vorrichtung zur herstellung von quarzglas aus einer polymerisierbaren polyalkylsiloxanverbindung mit membranfilter als reinigungsvorrichtung |
| EP3428135A1 (de) | 2017-07-14 | 2019-01-16 | Evonik Degussa GmbH | Wärmedämm-materialien auf basis hochverdickender kieselsäuren |
| CN116715244B (zh) * | 2023-06-14 | 2024-06-11 | 扬州大学 | 一种高纯二氧化硅的合成方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2399687A (en) * | 1942-05-29 | 1946-05-07 | Goodrich Co B F | Preparation of finely-divided silicon dioxide |
| US3086851A (en) * | 1957-10-10 | 1963-04-23 | Degussa | Burner for production of finely divided oxides |
| DE1933291C3 (de) * | 1969-07-01 | 1978-12-14 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Hochdisperses weißes Siliciumdioxid |
| GB1348372A (en) * | 1970-02-16 | 1974-03-13 | Ici Ltd | Foam-compatible powder compositions |
| DE2123233C3 (de) * | 1971-05-11 | 1977-10-13 | Degussa | Feinteiliges grossoberflaechiges siliciumdioxid |
| US3772427A (en) * | 1971-06-14 | 1973-11-13 | Gen Electric | Combustion process for producing high surface area silica |
| BE790704A (fr) * | 1971-10-28 | 1973-02-15 | Degussa | Procede pour la fabrication d'oxydes finement |
| DE2344388B2 (de) * | 1973-09-03 | 1978-06-22 | Elektroschmelzwerk Kempten Gmbh, 8000 Muenchen | Verfahren zum Herstellen von hydrophobem Siliciumdioxyd |
| DE2403783C2 (de) * | 1974-01-26 | 1982-10-21 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung hydrophobierter pyrogener Kieselsäure |
| DE2620737C2 (de) * | 1976-05-11 | 1982-07-29 | Wacker-Chemie GmbH, 8000 München | Verfahren zum Herstellen von hochdispersem Siliciumdioxid |
| DE2904199A1 (de) * | 1979-02-05 | 1980-08-07 | Degussa | Verfahren zur gelenkten herstellung von kieselsaeure mittels flammenhydrolyse |
| DE2909815C2 (de) | 1979-03-13 | 1984-11-22 | Wacker-Chemie GmbH, 8000 München | Verfahren zur Herstellung von hochdispersem Siliciumdioxid |
-
1980
- 1980-04-25 DE DE3016010A patent/DE3016010C2/de not_active Expired
-
1981
- 1981-01-21 EP EP83100856A patent/EP0092024B1/de not_active Expired
- 1981-01-21 EP EP81100412A patent/EP0038900B1/de not_active Expired
- 1981-01-21 AT AT83100856T patent/ATE14562T1/de not_active IP Right Cessation
- 1981-01-21 DE DE8181100412T patent/DE3162719D1/de not_active Expired
- 1981-03-02 SU SU813252703A patent/SU1421256A3/ru active
- 1981-04-21 JP JP5925781A patent/JPS56164009A/ja active Granted
- 1981-04-21 DD DD81229359A patent/DD158228A5/de unknown
- 1981-04-24 BR BR8102491A patent/BR8102491A/pt unknown
-
1984
- 1984-10-25 JP JP59223136A patent/JPS60127215A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| DE3016010A1 (de) | 1981-10-29 |
| JPS56164009A (en) | 1981-12-16 |
| EP0092024A1 (de) | 1983-10-26 |
| EP0038900A1 (de) | 1981-11-04 |
| JPH0131456B2 (enExample) | 1989-06-26 |
| JPS6116733B2 (enExample) | 1986-05-01 |
| EP0092024B1 (de) | 1985-07-31 |
| JPS60127215A (ja) | 1985-07-06 |
| BR8102491A (pt) | 1982-01-05 |
| DE3016010C2 (de) | 1985-01-10 |
| SU1421256A3 (ru) | 1988-08-30 |
| DE3162719D1 (en) | 1984-04-26 |
| ATE14562T1 (de) | 1985-08-15 |
| EP0038900B1 (de) | 1984-03-21 |
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