CS256118B1 - Polymer sorbent for colloidal and sensory stabilization of drinks and method of its production - Google Patents
Polymer sorbent for colloidal and sensory stabilization of drinks and method of its production Download PDFInfo
- Publication number
- CS256118B1 CS256118B1 CS861117A CS111786A CS256118B1 CS 256118 B1 CS256118 B1 CS 256118B1 CS 861117 A CS861117 A CS 861117A CS 111786 A CS111786 A CS 111786A CS 256118 B1 CS256118 B1 CS 256118B1
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- caprolactam
- polymerization
- sodium
- sorbent
- mixture
- Prior art date
Links
- 239000002594 sorbent Substances 0.000 title claims description 44
- 238000000034 method Methods 0.000 title claims description 17
- 229920000642 polymer Polymers 0.000 title claims description 13
- 230000001953 sensory effect Effects 0.000 title claims description 11
- 230000006641 stabilisation Effects 0.000 title claims description 4
- 238000011105 stabilization Methods 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title description 10
- 235000013361 beverage Nutrition 0.000 claims description 49
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 claims description 32
- 239000000126 substance Substances 0.000 claims description 19
- 238000006116 polymerization reaction Methods 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 17
- 239000011148 porous material Substances 0.000 claims description 14
- 239000000047 product Substances 0.000 claims description 13
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 11
- 239000003999 initiator Substances 0.000 claims description 11
- 235000013405 beer Nutrition 0.000 claims description 8
- 239000012190 activator Substances 0.000 claims description 7
- 239000002131 composite material Substances 0.000 claims description 7
- QISSLHPKTCLLDL-UHFFFAOYSA-N N-Acetylcaprolactam Chemical compound CC(=O)N1CCCCCC1=O QISSLHPKTCLLDL-UHFFFAOYSA-N 0.000 claims description 6
- 229920001577 copolymer Polymers 0.000 claims description 6
- -1 sodium tetra-6-caprolactam aluminum aluminum Chemical compound 0.000 claims description 6
- 235000015096 spirit Nutrition 0.000 claims description 5
- 239000000725 suspension Substances 0.000 claims description 5
- 235000014101 wine Nutrition 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- 235000013399 edible fruits Nutrition 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 239000012467 final product Substances 0.000 claims description 3
- 239000004615 ingredient Substances 0.000 claims description 3
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 claims description 2
- 150000004645 aluminates Chemical class 0.000 claims description 2
- DUQXROGNHFUZBI-UHFFFAOYSA-N azepan-2-one;sodium Chemical compound [Na].O=C1CCCCCN1 DUQXROGNHFUZBI-UHFFFAOYSA-N 0.000 claims description 2
- 125000004122 cyclic group Chemical group 0.000 claims description 2
- 239000012948 isocyanate Substances 0.000 claims description 2
- 150000002513 isocyanates Chemical class 0.000 claims description 2
- 239000012312 sodium hydride Substances 0.000 claims description 2
- 229910000104 sodium hydride Inorganic materials 0.000 claims description 2
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 2
- 235000013311 vegetables Nutrition 0.000 claims description 2
- KRMWJYDLDZJRNK-UHFFFAOYSA-N 2-oxo-n-phenylazepane-1-carboxamide Chemical compound C1CCCCC(=O)N1C(=O)NC1=CC=CC=C1 KRMWJYDLDZJRNK-UHFFFAOYSA-N 0.000 claims 1
- 230000000977 initiatory effect Effects 0.000 claims 1
- DGTNSSLYPYDJGL-UHFFFAOYSA-N phenyl isocyanate Chemical compound O=C=NC1=CC=CC=C1 DGTNSSLYPYDJGL-UHFFFAOYSA-N 0.000 claims 1
- 239000003381 stabilizer Substances 0.000 description 10
- 150000008442 polyphenolic compounds Chemical class 0.000 description 9
- 235000013824 polyphenols Nutrition 0.000 description 9
- 230000037048 polymerization activity Effects 0.000 description 6
- 239000000155 melt Substances 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Substances OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 239000011541 reaction mixture Substances 0.000 description 4
- 239000013049 sediment Substances 0.000 description 4
- SLXKOJJOQWFEFD-UHFFFAOYSA-N 6-aminohexanoic acid Chemical compound NCCCCCC(O)=O SLXKOJJOQWFEFD-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 239000000284 extract Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 230000000087 stabilizing effect Effects 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 239000004952 Polyamide Substances 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 2
- 229960002684 aminocaproic acid Drugs 0.000 description 2
- 235000012216 bentonite Nutrition 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 235000021440 light beer Nutrition 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 229920002647 polyamide Polymers 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- IYQDFYHVZJUZNL-UHFFFAOYSA-N 2-oxo-N-phenylazepane-3-carboxamide Chemical compound C1(=CC=CC=C1)NC(=O)C1C(=O)NCCCC1 IYQDFYHVZJUZNL-UHFFFAOYSA-N 0.000 description 1
- QPJCYJIZFCJYIR-UHFFFAOYSA-N 4-propylazetidin-2-one Chemical compound CCCC1CC(=O)N1 QPJCYJIZFCJYIR-UHFFFAOYSA-N 0.000 description 1
- PXRKCOCTEMYUEG-UHFFFAOYSA-N 5-aminoisoindole-1,3-dione Chemical compound NC1=CC=C2C(=O)NC(=O)C2=C1 PXRKCOCTEMYUEG-UHFFFAOYSA-N 0.000 description 1
- 235000008694 Humulus lupulus Nutrition 0.000 description 1
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 description 1
- RNJCXDJXPXWMDK-UHFFFAOYSA-N [AlH3].COCCO[Na] Chemical compound [AlH3].COCCO[Na] RNJCXDJXPXWMDK-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 1
- 235000015197 apple juice Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 229920001400 block copolymer Polymers 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000029142 excretion Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000012676 herbal extract Substances 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 239000000017 hydrogel Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229920002959 polymer blend Polymers 0.000 description 1
- 229920001184 polypeptide Polymers 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 229910001388 sodium aluminate Inorganic materials 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000002459 sustained effect Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 235000020097 white wine Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/40—Polyamides containing oxygen in the form of ether groups
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/80—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by adsorption
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
- C12H1/04—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material
- C12H1/0416—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of organic added material
- C12H1/0424—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of organic added material with the aid of a polymer
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Biochemistry (AREA)
- Nutrition Science (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Non-Alcoholic Beverages (AREA)
Priority Applications (11)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CS861117A CS256118B1 (en) | 1986-02-18 | 1986-02-18 | Polymer sorbent for colloidal and sensory stabilization of drinks and method of its production |
DK071787A DK71787A (da) | 1986-02-18 | 1987-02-12 | Polymer sorptionsmidler til kolloidisk og sensorisk stabilisering af vaesker og fremgangsmaade til fremstilling heraf |
CH543/87A CH672134A5 (enrdf_load_stackoverflow) | 1986-02-18 | 1987-02-13 | |
DE19873704822 DE3704822A1 (de) | 1986-02-18 | 1987-02-16 | Polymeres sorbens zur kolloidalen und sensorischen stabilisation von getraenken und verfahren zu seiner herstellung |
DD87299944A DD266464A3 (de) | 1986-02-18 | 1987-02-16 | Polymeres sorptionsmittel zur kolloiden und organoleptischen stabilisierung von getraenken und verfahren zu seiner herstellung |
NL8700368A NL8700368A (nl) | 1986-02-18 | 1987-02-16 | Polymeer absorptiemateriaal, werkwijze voor het bereiden van een dergelijk absorptiemateriaal en werkwijze voor het stabiliseren van dranken. |
BG78501A BG48105A1 (en) | 1986-02-18 | 1987-02-16 | Polymer sorbent for colloidic and organoleptic stabilizing of drinks and method its production |
IT19411/87A IT1202562B (it) | 1986-02-18 | 1987-02-17 | Assorbente polimerico per la stabilizzazione colloidale e organolettica di bevande e metodo per la sua fabbricazione |
FR8702108A FR2595709B3 (fr) | 1986-02-18 | 1987-02-18 | Agent d'absorption polymere pour la stabilisation colloidale et sensorielle de boissons, et procede pour sa fabrication |
GB8703732A GB2188329B (en) | 1986-02-18 | 1987-02-18 | Polymeric sorbent for colloidal and sensoric stabilisation of beverages and method for manufacture thereof |
BE8700139A BE1000056A7 (fr) | 1986-02-18 | 1987-02-18 | Sorbant polymere pour stabilisation colloidale et organoleptique des boissons, et procede pour sa fabrication. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CS861117A CS256118B1 (en) | 1986-02-18 | 1986-02-18 | Polymer sorbent for colloidal and sensory stabilization of drinks and method of its production |
Publications (2)
Publication Number | Publication Date |
---|---|
CS111786A1 CS111786A1 (en) | 1987-08-13 |
CS256118B1 true CS256118B1 (en) | 1988-04-15 |
Family
ID=5344726
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CS861117A CS256118B1 (en) | 1986-02-18 | 1986-02-18 | Polymer sorbent for colloidal and sensory stabilization of drinks and method of its production |
Country Status (11)
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5030710A (en) * | 1990-04-10 | 1991-07-09 | Texaco Chemical Company | Nylon-6 modified with low molecular weight polyethylene glycol diamines |
DE19501646A1 (de) * | 1995-01-20 | 1996-07-25 | Schwartz G Gmbh & Co Kg | Verfahren zur Herstellung von Formteilen mittels Polymerisation von Lactamen in Formen |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2030007C3 (de) * | 1970-06-18 | 1979-05-17 | Basf Ag, 6700 Ludwigshafen | Fäden oder Fasern aus Polyamiden |
GB2164945B (en) * | 1984-09-28 | 1988-11-09 | Vysoka Skola Chem Tech | Sorbent for stabilizing colloidal and organoleptic properties of beverages containing organic components and a method of its preparations |
-
1986
- 1986-02-18 CS CS861117A patent/CS256118B1/cs unknown
-
1987
- 1987-02-12 DK DK071787A patent/DK71787A/da not_active Application Discontinuation
- 1987-02-13 CH CH543/87A patent/CH672134A5/de not_active IP Right Cessation
- 1987-02-16 DD DD87299944A patent/DD266464A3/xx unknown
- 1987-02-16 DE DE19873704822 patent/DE3704822A1/de not_active Withdrawn
- 1987-02-16 BG BG78501A patent/BG48105A1/xx unknown
- 1987-02-16 NL NL8700368A patent/NL8700368A/nl not_active Application Discontinuation
- 1987-02-17 IT IT19411/87A patent/IT1202562B/it active
- 1987-02-18 GB GB8703732A patent/GB2188329B/en not_active Expired
- 1987-02-18 BE BE8700139A patent/BE1000056A7/fr active
- 1987-02-18 FR FR8702108A patent/FR2595709B3/fr not_active Expired
Also Published As
Publication number | Publication date |
---|---|
CS111786A1 (en) | 1987-08-13 |
IT1202562B (it) | 1989-02-09 |
GB2188329A (en) | 1987-09-30 |
GB2188329B (en) | 1989-11-08 |
DE3704822A1 (de) | 1987-08-20 |
IT8719411A0 (it) | 1987-02-17 |
DK71787D0 (da) | 1987-02-12 |
DK71787A (da) | 1987-08-19 |
CH672134A5 (enrdf_load_stackoverflow) | 1989-10-31 |
DD266464A3 (de) | 1989-04-05 |
BG48105A1 (en) | 1990-12-14 |
FR2595709B3 (fr) | 1988-02-26 |
FR2595709A3 (fr) | 1987-09-18 |
BE1000056A7 (fr) | 1987-12-29 |
NL8700368A (nl) | 1987-09-16 |
GB8703732D0 (en) | 1987-03-25 |
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