CS250235B2 - Method of glass articles polishing - Google Patents
Method of glass articles polishing Download PDFInfo
- Publication number
- CS250235B2 CS250235B2 CS837499A CS749983A CS250235B2 CS 250235 B2 CS250235 B2 CS 250235B2 CS 837499 A CS837499 A CS 837499A CS 749983 A CS749983 A CS 749983A CS 250235 B2 CS250235 B2 CS 250235B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- polishing
- acid
- bath
- concentration
- sulfuric acid
- Prior art date
Links
- 238000005498 polishing Methods 0.000 title claims description 133
- 239000011521 glass Substances 0.000 title claims description 39
- 238000000034 method Methods 0.000 title claims description 30
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 90
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 60
- 239000002253 acid Substances 0.000 claims description 28
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 23
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 18
- 238000010494 dissociation reaction Methods 0.000 claims description 17
- 230000005593 dissociations Effects 0.000 claims description 17
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 14
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- 239000011780 sodium chloride Substances 0.000 claims description 9
- 150000007524 organic acids Chemical class 0.000 claims description 8
- 230000001590 oxidative effect Effects 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 7
- 235000006408 oxalic acid Nutrition 0.000 claims description 7
- 239000001103 potassium chloride Substances 0.000 claims description 7
- 235000011164 potassium chloride Nutrition 0.000 claims description 7
- 235000002906 tartaric acid Nutrition 0.000 claims description 6
- 239000011975 tartaric acid Substances 0.000 claims description 6
- 230000007423 decrease Effects 0.000 claims description 5
- 230000007547 defect Effects 0.000 claims description 5
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 3
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 3
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims description 2
- 230000002045 lasting effect Effects 0.000 claims 1
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 claims 1
- 150000003839 salts Chemical class 0.000 description 15
- -1 fluoride ions Chemical class 0.000 description 13
- 150000007513 acids Chemical class 0.000 description 11
- 238000011282 treatment Methods 0.000 description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 238000007654 immersion Methods 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- 239000007795 chemical reaction product Substances 0.000 description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 4
- 229910001413 alkali metal ion Inorganic materials 0.000 description 4
- HTUMBQDCCIXGCV-UHFFFAOYSA-N lead oxide Chemical compound [O-2].[Pb+2] HTUMBQDCCIXGCV-UHFFFAOYSA-N 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 229910001420 alkaline earth metal ion Inorganic materials 0.000 description 3
- 239000000292 calcium oxide Substances 0.000 description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005530 etching Methods 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000007517 polishing process Methods 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 150000001991 dicarboxylic acids Chemical class 0.000 description 2
- 229910000464 lead oxide Inorganic materials 0.000 description 2
- 150000002763 monocarboxylic acids Chemical class 0.000 description 2
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
- 229910001414 potassium ion Inorganic materials 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 229910001415 sodium ion Inorganic materials 0.000 description 2
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000012080 ambient air Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- QXDMQSPYEZFLGF-UHFFFAOYSA-L calcium oxalate Chemical compound [Ca+2].[O-]C(=O)C([O-])=O QXDMQSPYEZFLGF-UHFFFAOYSA-L 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 1
- 229940117975 chromium trioxide Drugs 0.000 description 1
- WGLPBDUCMAPZCE-UHFFFAOYSA-N chromium trioxide Inorganic materials O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 1
- GAMDZJFZMJECOS-UHFFFAOYSA-N chromium(6+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Cr+6] GAMDZJFZMJECOS-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 230000029142 excretion Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 1
- 239000006066 glass batch Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 150000001261 hydroxy acids Chemical class 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- KYKNRZGSIGMXFH-ZVGUSBNCSA-M potassium bitartrate Chemical compound [K+].OC(=O)[C@H](O)[C@@H](O)C([O-])=O KYKNRZGSIGMXFH-ZVGUSBNCSA-M 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- 239000001472 potassium tartrate Substances 0.000 description 1
- 229940111695 potassium tartrate Drugs 0.000 description 1
- 235000011005 potassium tartrates Nutrition 0.000 description 1
- 239000005401 pressed glass Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000009938 salting Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- HIFJUMGIHIZEPX-UHFFFAOYSA-N sulfuric acid;sulfur trioxide Chemical compound O=S(=O)=O.OS(O)(=O)=O HIFJUMGIHIZEPX-UHFFFAOYSA-N 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
- C03C15/02—Surface treatment of glass, not in the form of fibres or filaments, by etching for making a smooth surface
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
- C03C15/02—Surface treatment of glass, not in the form of fibres or filaments, by etching for making a smooth surface
- C03C15/025—Surface treatment of glass, not in the form of fibres or filaments, by etching for making a smooth surface for polishing crystal glass, i.e. lead glass
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3238011 | 1982-10-13 | ||
| DE3322875 | 1983-06-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS250235B2 true CS250235B2 (en) | 1987-04-16 |
Family
ID=25805099
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS837499A CS250235B2 (en) | 1982-10-13 | 1983-10-12 | Method of glass articles polishing |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4555304A (es) |
| EP (1) | EP0106301B1 (es) |
| CS (1) | CS250235B2 (es) |
| DD (1) | DD212725A5 (es) |
| DE (1) | DE3368915D1 (es) |
| ES (1) | ES8500612A1 (es) |
| IE (1) | IE56029B1 (es) |
| PT (1) | PT77479B (es) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2188925B (en) * | 1986-04-08 | 1990-05-09 | Glaverbel | Matted glass and process of manufacturing same |
| GB2188924B (en) * | 1986-04-08 | 1990-05-09 | Glaverbel | Matted glass, process of producing matted glass, photo-voltaic cell incorporating a glass sheet, and process of manufacturing such a cell |
| USH532H (en) | 1986-10-20 | 1988-10-04 | The United States Of America As Represented By The Secretary Of The Army | Method of chemically polishing fused quartz |
| US5120605A (en) * | 1988-09-23 | 1992-06-09 | Zuel Company, Inc. | Anti-reflective glass surface |
| US4944986A (en) * | 1988-09-23 | 1990-07-31 | Zuel Company | Anti-reflective glass surface |
| US5258131A (en) * | 1990-04-13 | 1993-11-02 | Austen-Chase Industries Inc. | Products for treating asbestos |
| DE4217057A1 (de) * | 1992-05-22 | 1993-11-25 | Saelzle Erich | Verfahren zur Verminderung der Blei- und/oder Bariumemission von Blei und/oder Barium enthaltenden Kristallglasgegenständen bei Berührung mit einer flüssigen Phase |
| US5851366A (en) * | 1994-07-19 | 1998-12-22 | Corning Incorporated | Adhering metal to glass |
| US5792327A (en) * | 1994-07-19 | 1998-08-11 | Corning Incorporated | Adhering metal to glass |
| US5741358A (en) * | 1996-09-27 | 1998-04-21 | W. R. Grace & Co.-Conn. | Corrosion inhibiting composition for treating asbestos containing materials |
| US5753032A (en) * | 1996-09-27 | 1998-05-19 | W. R. Grace & Co.-Conn. | Composition and method to remove asbestos |
| US5753034A (en) * | 1996-09-27 | 1998-05-19 | W. R. Grace & Co. -Conn. | Composition and method to remove asbestos |
| US5753035A (en) * | 1996-09-27 | 1998-05-19 | W. R. Grace & Co.-Conn. | Composition and method to remove asbestos |
| US5753031A (en) * | 1996-09-27 | 1998-05-19 | W. R. Grace & Co.-Conn. | Composition and method to remove asbestos |
| US5753033A (en) * | 1996-09-27 | 1998-05-19 | W. R. Grace & Co.-Conn. | Composition and method to remove asbestos |
| US5743841A (en) * | 1996-09-27 | 1998-04-28 | W. R. Grace & Co.-Conn. | Foam composition for treating asbestos-containing materials and method of using same |
| KR100248113B1 (ko) * | 1997-01-21 | 2000-03-15 | 이기원 | 전자 표시 장치 및 기판용 세정 및 식각 조성물 |
| US6284721B1 (en) | 1997-01-21 | 2001-09-04 | Ki Won Lee | Cleaning and etching compositions |
| KR20010048192A (ko) * | 1999-11-25 | 2001-06-15 | 황정남 | 유리에서 나트륨 원소 제거 방법 |
| AU2001253308A1 (en) * | 2000-04-11 | 2001-10-23 | Cabot Microelectronics Corporation | System for the preferential removal of silicon oxide |
| JP4367816B2 (ja) * | 2000-05-19 | 2009-11-18 | 信越石英株式会社 | 石英ガラスの表面処理方法 |
| JP5197902B2 (ja) * | 2001-08-31 | 2013-05-15 | ステラケミファ株式会社 | 多成分を有するガラス基板用の微細加工表面処理液 |
| US6929861B2 (en) | 2002-03-05 | 2005-08-16 | Zuel Company, Inc. | Anti-reflective glass surface with improved cleanability |
| DE10228116A1 (de) | 2002-06-24 | 2004-01-29 | Sälzle, Erich, Dr. | Verfahren zum Polieren von Glasgegenständen |
| US9926225B2 (en) | 2011-12-30 | 2018-03-27 | Corning Incorporated | Media and methods for etching glass |
| WO2013181213A1 (en) * | 2012-05-31 | 2013-12-05 | Corning Incorporated | Systems and methods for acid-treating glass articles |
| CN113105123A (zh) * | 2021-04-08 | 2021-07-13 | 惠州市清洋实业有限公司 | 一种Micro LED显示屏的抛光处理方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1777321A (en) * | 1928-09-24 | 1930-10-07 | Meth Isaac | Glass-polishing solution and method of polishing glass |
| US2372535A (en) * | 1941-10-31 | 1945-03-27 | Alncin Inc | Curved glass surface and method and means for manufacturing same |
| US2328533A (en) * | 1941-12-26 | 1943-08-31 | Alncin Inc | Glass article and method of manufacture thereof |
| DE1185780B (de) * | 1962-11-10 | 1965-01-21 | Erich Saelzle Dipl Chem Dr | Verfahren zum Polieren von Gegenstaenden aus Kristall- oder Bleikristallglas |
| BE639724A (es) * | 1963-11-09 | |||
| DE1496666C3 (de) * | 1965-05-26 | 1974-04-04 | Erich Dipl.-Chem.Dr. 8000 Muenchen Saelzle | Verfahren zum Polieren von Glasgegenständen in einem Flußsäure und Schwefelsäure enthaltenden Polierbad |
| BE779363A (nl) * | 1972-02-15 | 1972-08-16 | Demeulemeester Rosanne Echtgen | Bereidingen voor het wegnemen van irisatie op glas. |
| US4040897A (en) * | 1975-05-05 | 1977-08-09 | Signetics Corporation | Etchants for glass films on metal substrates |
| DE2949383C2 (de) * | 1979-12-07 | 1982-01-21 | Sälzle, Erich, Dr., 8000 München | Verfahren zur Schwefelsäure-Flußsäure-Polieren von Glasgegenständen |
| US4395304A (en) * | 1982-05-11 | 1983-07-26 | Rca Corporation | Selective etching of phosphosilicate glass |
-
1983
- 1983-09-26 ES ES525932A patent/ES8500612A1/es not_active Expired
- 1983-09-29 US US06/537,209 patent/US4555304A/en not_active Expired - Lifetime
- 1983-10-10 EP EP83110094A patent/EP0106301B1/de not_active Expired
- 1983-10-10 DE DE8383110094T patent/DE3368915D1/de not_active Expired
- 1983-10-10 DD DD83255543A patent/DD212725A5/de not_active IP Right Cessation
- 1983-10-11 PT PT77479A patent/PT77479B/pt active IP Right Revival
- 1983-10-12 CS CS837499A patent/CS250235B2/cs unknown
- 1983-10-12 IE IE2401/83A patent/IE56029B1/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| IE832401L (en) | 1984-04-13 |
| EP0106301B1 (de) | 1987-01-07 |
| PT77479B (en) | 1986-02-12 |
| EP0106301A1 (de) | 1984-04-25 |
| IE56029B1 (en) | 1991-03-27 |
| DD212725A5 (de) | 1984-08-22 |
| ES525932A0 (es) | 1984-11-16 |
| DE3368915D1 (en) | 1987-02-12 |
| US4555304A (en) | 1985-11-26 |
| PT77479A (en) | 1983-11-01 |
| ES8500612A1 (es) | 1984-11-16 |
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