CS244802B2 - Copper catalysed reaction substance and method of its production - Google Patents
Copper catalysed reaction substance and method of its production Download PDFInfo
- Publication number
- CS244802B2 CS244802B2 CS807189A CS718980A CS244802B2 CS 244802 B2 CS244802 B2 CS 244802B2 CS 807189 A CS807189 A CS 807189A CS 718980 A CS718980 A CS 718980A CS 244802 B2 CS244802 B2 CS 244802B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- copper
- silicon
- reaction mass
- mixture
- less
- Prior art date
Links
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims abstract description 47
- 239000010949 copper Substances 0.000 title claims abstract description 43
- 229910052802 copper Inorganic materials 0.000 title claims abstract description 41
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- 238000000034 method Methods 0.000 title claims description 9
- 238000006555 catalytic reaction Methods 0.000 title claims 2
- 239000000126 substance Substances 0.000 title description 2
- 238000006243 chemical reaction Methods 0.000 claims abstract description 35
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 30
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 27
- 239000010703 silicon Substances 0.000 claims abstract description 27
- 239000002245 particle Substances 0.000 claims abstract description 19
- 229910000676 Si alloy Inorganic materials 0.000 claims abstract description 10
- WCCJDBZJUYKDBF-UHFFFAOYSA-N copper silicon Chemical compound [Si].[Cu] WCCJDBZJUYKDBF-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims abstract description 8
- 230000003197 catalytic effect Effects 0.000 claims abstract description 3
- 239000003054 catalyst Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 4
- 229910045601 alloy Inorganic materials 0.000 claims description 3
- 239000000956 alloy Substances 0.000 claims description 3
- -1 methanol chlorosilanes Chemical class 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 6
- 229910052725 zinc Inorganic materials 0.000 claims 4
- 239000011701 zinc Substances 0.000 claims 4
- BERDEBHAJNAUOM-UHFFFAOYSA-N copper(I) oxide Inorganic materials [Cu]O[Cu] BERDEBHAJNAUOM-UHFFFAOYSA-N 0.000 claims 3
- KRFJLUBVMFXRPN-UHFFFAOYSA-N cuprous oxide Chemical compound [O-2].[Cu+].[Cu+] KRFJLUBVMFXRPN-UHFFFAOYSA-N 0.000 claims 2
- 229940112669 cuprous oxide Drugs 0.000 claims 2
- 239000011541 reaction mixture Substances 0.000 claims 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 229910052787 antimony Inorganic materials 0.000 claims 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims 1
- 229910052785 arsenic Inorganic materials 0.000 claims 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 229910052797 bismuth Inorganic materials 0.000 claims 1
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims 1
- 239000004568 cement Substances 0.000 claims 1
- 239000000460 chlorine Substances 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 229940108928 copper Drugs 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000012535 impurity Substances 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000003595 mist Substances 0.000 claims 1
- 239000002105 nanoparticle Substances 0.000 claims 1
- 239000007921 spray Substances 0.000 claims 1
- YGZSVWMBUCGDCV-UHFFFAOYSA-N chloro(methyl)silane Chemical compound C[SiH2]Cl YGZSVWMBUCGDCV-UHFFFAOYSA-N 0.000 abstract description 8
- 239000011856 silicon-based particle Substances 0.000 abstract description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical compound ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 239000011863 silicon-based powder Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 229940050176 methyl chloride Drugs 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- SBEQWOXEGHQIMW-UHFFFAOYSA-N silicon Chemical compound [Si].[Si] SBEQWOXEGHQIMW-UHFFFAOYSA-N 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/12—Organo silicon halides
- C07F7/16—Preparation thereof from silicon and halogenated hydrocarbons direct synthesis
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/087,798 US4314908A (en) | 1979-10-24 | 1979-10-24 | Preparation of reaction mass for the production of methylchlorosilane |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS244802B2 true CS244802B2 (en) | 1986-08-14 |
Family
ID=22207326
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS807189A CS244802B2 (en) | 1979-10-24 | 1980-10-23 | Copper catalysed reaction substance and method of its production |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4314908A (fr) |
| EP (1) | EP0028009B1 (fr) |
| JP (1) | JPS5948139B2 (fr) |
| AT (1) | ATE13537T1 (fr) |
| CA (1) | CA1158629A (fr) |
| CS (1) | CS244802B2 (fr) |
| DE (1) | DE3070708D1 (fr) |
| SU (1) | SU1526580A3 (fr) |
Families Citing this family (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4487950A (en) * | 1982-04-16 | 1984-12-11 | General Electric Company | Method for making methylchlorosilanes |
| GB2127032A (en) * | 1982-09-17 | 1984-04-04 | Gen Electric | A catalyst for a process for producing silicones |
| JPS5955891A (ja) * | 1982-09-27 | 1984-03-31 | ゼネラル・エレクトリツク・カンパニイ | 改良触媒によるオルガノハロシランの製法 |
| US4500724A (en) * | 1983-07-28 | 1985-02-19 | General Electric Company | Method for making alkylhalosilanes |
| USRE33452E (en) * | 1983-07-28 | 1990-11-20 | General Electric Company | Method for making alkylhalosilanes |
| US4504597A (en) * | 1983-11-04 | 1985-03-12 | Scm Corporation | Cupreous catalyst and process making same |
| GB2153697B (en) * | 1984-02-13 | 1988-04-27 | Gen Electric | Catalysts for the production of organohalosilanes |
| US4520130A (en) * | 1984-05-08 | 1985-05-28 | Scm Corporation | Halosilane catalyst and process for making same |
| US4593114A (en) * | 1984-09-13 | 1986-06-03 | Union Carbide Corporation | Direct process for preparing dimethylsiloxanes |
| US4864044A (en) * | 1985-02-15 | 1989-09-05 | Union Carbide Corporation | Tin containing activated silicon for the direct reaction |
| US4602101A (en) * | 1985-11-12 | 1986-07-22 | Dow Corning Corporation | Method of manufacturing alkylhalosilanes |
| US4762940A (en) * | 1987-12-11 | 1988-08-09 | Dow Corning Corporation | Method for preparation of alkylhalosilanes |
| US4973725A (en) * | 1988-06-28 | 1990-11-27 | Union Carbide Chemicals And Plastics Company Inc. | Direct synthesis process for organohalohydrosilanes |
| GB8910967D0 (en) * | 1989-05-12 | 1989-06-28 | Univ Leicester | Abstracting electronegative elements from heteromolecules |
| US5061672A (en) * | 1990-01-30 | 1991-10-29 | Elkem Metals Company | Active mass for making organohalosilanes |
| US5250716A (en) * | 1992-05-28 | 1993-10-05 | Mui Jeffrey Y P | Method for making a silicon/copper contact mass suitable for direct reaction |
| US5243061A (en) * | 1992-12-09 | 1993-09-07 | General Electric Company | Method for making organohalosilanes |
| US5281739A (en) * | 1992-12-23 | 1994-01-25 | Dow Corning Corporation | Process for manufacture of alkylhalosilanes |
| US5783720A (en) | 1996-10-10 | 1998-07-21 | Osi Specialties, Inc. | Surface-active additives in the direct synthesis of trialkoxysilanes |
| JPH1111926A (ja) * | 1997-06-20 | 1999-01-19 | Mitsui Chem Inc | 銅−珪素合金が珪素粉末表面に高度に分散した珪素粉末及びその製造方法 |
| US6156380A (en) * | 1998-10-05 | 2000-12-05 | Shin-Etsu Chemical Co., Ltd. | Method for preparing contact mass for organohalosilane synthesis |
| US6528674B1 (en) | 2000-04-20 | 2003-03-04 | General Electric Company | Method for preparing a contact mass |
| DE10044796A1 (de) * | 2000-09-11 | 2002-04-04 | Bayer Ag | Verfahren zur Herstellung von Chlorsilanen |
| CN101189245B (zh) * | 2005-03-09 | 2012-06-13 | 瑞科硅公司 | 制备氢氯硅烷的方法 |
| WO2011094140A2 (fr) | 2010-01-26 | 2011-08-04 | Dow Corning Corporation | Procédé de préparation d'un organohalosilane |
| US8722915B2 (en) * | 2010-05-28 | 2014-05-13 | Dow Corning Corporation | Preparation of organohalosilanes |
| US8772525B2 (en) * | 2010-05-28 | 2014-07-08 | Dow Corning Corporation | Method for preparing a diorganodihalosilane |
| KR20130105618A (ko) | 2010-09-08 | 2013-09-25 | 다우 코닝 코포레이션 | 트라이할로실란의 제조 방법 |
| CN103261208A (zh) | 2010-12-17 | 2013-08-21 | 道康宁公司 | 制备二有机二卤代硅烷的方法 |
| WO2012082686A1 (fr) | 2010-12-17 | 2012-06-21 | Dow Corning Corporation | Procédé de fabrication d'un trihalosilane |
| JP2014507416A (ja) * | 2011-01-25 | 2014-03-27 | ダウ コーニング コーポレーション | ジオルガノジハロシランの調製方法 |
| KR101422080B1 (ko) | 2011-09-06 | 2014-07-22 | 인스티튜트 오브 아이온-플라즈마엔드 레이저 테크놀러지스 | 트리알콕시실란의 제조방법 |
| CN104736547A (zh) | 2012-08-13 | 2015-06-24 | 道康宁公司 | 通过使氢、卤硅烷和有机卤化物在铜催化剂上以两步法反应制备有机卤硅烷的方法 |
| EP2909217B1 (fr) | 2012-10-16 | 2016-10-26 | Dow Corning Corporation | Procédé de préparation de silahydrocarbylènes halogénés |
| WO2015073213A1 (fr) | 2013-11-12 | 2015-05-21 | Dow Corning Corporation | Procédé de préparation d'un halogénosilane |
| KR101616043B1 (ko) | 2014-07-22 | 2016-04-27 | 한화케미칼 주식회사 | 삼염화실란의 제조방법 |
| EP3233731B1 (fr) | 2014-12-18 | 2020-08-05 | Dow Silicones Corporation | Procédé de production de silanes à fonction aryle |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2380996A (en) * | 1941-09-26 | 1945-08-07 | Gen Electric | Preparation of organosilicon halides |
| US2449821A (en) * | 1945-12-08 | 1948-09-21 | Gen Electric | Method for preparing organosilicon compounds |
| US2686194A (en) * | 1951-05-31 | 1954-08-10 | Kellogg M W Co | Organosilicon compounds |
| US3069452A (en) * | 1959-01-26 | 1962-12-18 | Goldschmidt Ag Th | Process for the production of a silane mixture |
| FR1545407A (fr) * | 1966-11-28 | 1968-11-08 | Midland Silicones Ltd | Procédé de préparation d'organohalosilanes |
-
1979
- 1979-10-24 US US06/087,798 patent/US4314908A/en not_active Expired - Lifetime
-
1980
- 1980-08-22 CA CA000358871A patent/CA1158629A/fr not_active Expired
- 1980-10-23 EP EP80106464A patent/EP0028009B1/fr not_active Expired
- 1980-10-23 SU SU802998452A patent/SU1526580A3/ru active
- 1980-10-23 CS CS807189A patent/CS244802B2/cs unknown
- 1980-10-23 AT AT80106464T patent/ATE13537T1/de not_active IP Right Cessation
- 1980-10-23 DE DE8080106464T patent/DE3070708D1/de not_active Expired
- 1980-10-23 JP JP55148867A patent/JPS5948139B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CA1158629A (fr) | 1983-12-13 |
| US4314908A (en) | 1982-02-09 |
| JPS5948139B2 (ja) | 1984-11-24 |
| JPS5673544A (en) | 1981-06-18 |
| EP0028009A2 (fr) | 1981-05-06 |
| SU1526580A3 (ru) | 1989-11-30 |
| EP0028009A3 (en) | 1982-05-26 |
| DE3070708D1 (en) | 1985-07-04 |
| EP0028009B1 (fr) | 1985-05-29 |
| ATE13537T1 (de) | 1985-06-15 |
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