CN206887267U - A kind of device of the controllable culture complex monocrystal of diffusion rate - Google Patents
A kind of device of the controllable culture complex monocrystal of diffusion rate Download PDFInfo
- Publication number
- CN206887267U CN206887267U CN201720347754.3U CN201720347754U CN206887267U CN 206887267 U CN206887267 U CN 206887267U CN 201720347754 U CN201720347754 U CN 201720347754U CN 206887267 U CN206887267 U CN 206887267U
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- CN
- China
- Prior art keywords
- external container
- container
- rotating shaft
- inner chamber
- diffusion rate
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Abstract
The utility model discloses a kind of device of the controllable culture complex monocrystal of diffusion rate of technical field of single crystal growth,Including external container,The bottom even of the external container is provided with support,Seal closure is provided with the top of the external container,The inner chamber of the external container is provided with internal container,The inner chamber of the internal container is horizontally arranged with holding tray,The outer wall of the holding tray is evenly arranged with standing groove,The inner chamber left and right sidewall of the external container is mounted on radiator valve,The bottom of the internal container is provided with connecting plate,The bottom of the connecting plate is provided with rotating shaft,The bottom of external container is run through in the bottom of the rotating shaft,The bottom of the rotating shaft is provided with handle,The outer wall of the rotating shaft is socketed with bearing,Overcome influence of the external environment to crystal growth,Contribute to the growth of the monocrystalline of perfect structure,Brought convenience to mono-crystalline structures parsing,Save substantial amounts of manpower,Material resources and financial resources.
Description
Technical field
It the utility model is related to technical field of single crystal growth, the controllable culture complex monocrystal of specially a kind of diffusion rate
Device.
Background technology
Design and synthesis have expected structure and the functional complexes monocrystalline of performance, are always one of Coordinative Chemistry research
Focus, has numerous scientific research institutions carrying out related research work both at home and abroad at present, and the production speed and quality of monocrystalline are main
The speed that nucleus is formed and grown is relied on, if nucleation rate is more than growth rate, substantial amounts of crystallite will be formed, and hold
Easily there is crystal reunion, on the contrary, too fast growth rate can cause crystal defect occur, to avoid both problems, usually need
Constantly to test, because when beginning one's study a noval chemical compound, we often do not know the crystallization rule of this noval chemical compound
Rule, generally it is not easy to predict and avoids crystallite or the generation of agglomeration traits, synthetic compound monocrystalline there are many methods, such as evaporates
Crystallisation and lowering temperature crystallization, traditional evaporative crystallization method are two kinds of volumes to target compound different solubility of selection, and
And two kinds of solvents have certain intersolubility, the compound to be crystallized is dissolved in the big solvent of solubility and is placed on small
In container, it is then placed within bulk container, fills the less solvent of solubility in bulk container, the steam meeting of the solvent in bulk container
It is diffused into small container, so as to reduce the solubility of compound, forces it constantly to crystallize, but traditional complex monocrystal steams
Its diffusion rate is difficult to control during hair crystallization, and because the influence of external environment easily causes the growth of complex monocrystal, mirror
In mentioned above the problem of, the utility model designs a kind of device of the controllable culture complex monocrystal of diffusion rate, to solve
The problem of mentioned above.
Utility model content
The purpose of this utility model is the device for providing a kind of controllable culture complex monocrystal of diffusion rate, to solve
Its diffusion rate is difficult to control during the traditional complex monocrystal evaporative crystallization proposed in above-mentioned background technology, and due to the external world
The problem of influence of environment easily causes the growth of complex monocrystal.
To achieve the above object, the utility model provides following technical scheme：A kind of controllable culture of diffusion rate coordinates
The device of thing monocrystalline, including external container, the bottom even of the external container are provided with support, the top of the external container
Seal closure is provided with, the inner chamber of the external container is provided with internal container, and the inner chamber of the internal container, which is horizontally arranged with, puts
Disk is put, the outer wall of the holding tray is evenly arranged with standing groove, and the inner chamber left and right sidewall of the external container is mounted on constant temperature
Controller, the bottom of the internal container are provided with connecting plate, and the bottom of the connecting plate is provided with rotating shaft, the bottom of the rotating shaft
The bottom of external container is run through in portion, and the bottom of the rotating shaft is provided with handle, and the outer wall of the rotating shaft is socketed with bearing, the axle
Hold the bottom for being arranged on external container.
Preferably, the inwall of the standing groove is provided with rubber wear-resisting pad.
Preferably, it is provided with sealing gasket between the external container and rotating shaft.
Preferably, the bottom of the external container offers bearing groove, and the bearing is arranged on the inner chamber of bearing groove.
Preferably, neck is offered at the top of the external container, the bottom of the seal closure is connected to the inner chamber of neck.
Compared with prior art, the beneficial effects of the utility model are：The controllable culture complex list of this kind of diffusion rate
Brilliant device, so as to drive the rotating speed of internal container, increases the complex in internal container by the way that manually handle is adjusted
The evaporation rate of monocrystalline, and control requirement of experiment to enter the setting of trip temperature, the temperature of radiator valve by radiator valve
It is adjustable to control the evaporation rate of culture monocrystalline, overcomes influence of the external environment to crystal growth, contribute to structure complete
The growth of beautiful monocrystalline, brought convenience to mono-crystalline structures parsing, help to make laughs and carry out investigative test, save substantial amounts of people
Power, material resources and financial resources.
Brief description of the drawings
Fig. 1 is the utility model structure diagram.
In figure：1 external container, 2 supports, 3 seal closures, 4 internal containers, 5 holding trays, 6 standing grooves, 7 radiator valves, 8
Connecting plate, 9 rotating shafts, 10 handles, 11 bearings.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made
The every other embodiment obtained, belong to the scope of the utility model protection.
Referring to Fig. 1, the utility model provides a kind of technical scheme：A kind of controllable culture complex monocrystal of diffusion rate
Device, including external container 1, the bottom even of the external container 1 be provided with support 2, and the top of the external container 1 is set
Seal closure 3 is equipped with, the inner chamber of the external container 1 is provided with internal container 4, and the inner chamber of the internal container 4 is horizontally arranged with
Holding tray 5, the outer wall of the holding tray 5 are evenly arranged with standing groove 6, and the inner chamber left and right sidewall of the external container 1 is respectively mounted
There is radiator valve 7, the bottom of the internal container 4 is provided with connecting plate 8, and the bottom of the connecting plate 8 is provided with rotating shaft 9,
The bottom of external container 1 is run through in the bottom of the rotating shaft 9, and the bottom of the rotating shaft 9 is provided with handle 10, the rotating shaft 9 it is outer
Wall is socketed with bearing 11, and the bearing 11 is arranged on the bottom of external container 1.
Wherein, the inwall of the standing groove 6 is provided with rubber wear-resisting pad, is easy to place the container for holding culture monocrystalline,
Anti- sliding stop, sealing gasket is provided between the external container 1 and rotating shaft 9, prevents the solvent in external container 1 from seepage occurs,
The bottom of the external container 1 offers bearing groove, and the bearing 11 is arranged on the inner chamber of bearing groove, the external container 1
Top offers neck, and the bottom of the seal closure 3 is connected to the inner chamber of neck, is easy to the installation and removal to seal closure 3.
Operation principle：Manually rotating shaft 9 is driven to be rotated by handle 10, rotating shaft 9 is arranged on outer wall by bearing 11 and held
The bottom inner chamber of device 1, it is easy to the rotation of rotating shaft 9, rotating shaft 9 is connected by connecting plate 8 with internal container 4, therefore by adjusting hand
Handle 10 adjusts the rotation of internal container 4, so that the culture monocrystalline evaporation rate in internal container 4 is accelerated, Ke Yigeng
Fast crystallize, and when being crystallized, external container 1 is sealed by seal closure 3, prevents external environment from influenceing culture
The evaporation of monocrystalline, requirement of experiment can control to enter the setting of trip temperature by radiator valve 7, also can be by radiator valve 7
Temperature adjustment control the evaporation rate of culture monocrystalline.
While there has been shown and described that embodiment of the present utility model, for the ordinary skill in the art,
It is appreciated that these embodiments can be carried out with a variety of changes in the case where not departing from principle of the present utility model and spirit, repaiied
Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.
Claims (5)
1. a kind of device of the controllable culture complex monocrystal of diffusion rate, including external container (1), it is characterised in that：It is described
The bottom even of external container (1) is provided with support (2), and seal closure (3) is provided with the top of the external container (1), described
The inner chamber of external container (1) is provided with internal container (4), and the inner chamber of the internal container (4) is horizontally arranged with holding tray (5),
The outer wall of the holding tray (5) is evenly arranged with standing groove (6), and the inner chamber left and right sidewall of the external container (1) is mounted on
Radiator valve (7), the bottom of the internal container (4) are provided with connecting plate (8), and the bottom of the connecting plate (8) is provided with
The bottom of external container (1) is run through in rotating shaft (9), the bottom of the rotating shaft (9), and the bottom of the rotating shaft (9) is provided with handle
(10), the outer wall of the rotating shaft (9) is socketed with bearing (11), and the bearing (11) is arranged on the bottom of external container (1).
A kind of 2. device of the controllable culture complex monocrystal of diffusion rate according to claim 1, it is characterised in that：Institute
The inwall for stating standing groove (6) is provided with rubber wear-resisting pad.
A kind of 3. device of the controllable culture complex monocrystal of diffusion rate according to claim 1, it is characterised in that：Institute
State and be provided with sealing gasket between external container (1) and rotating shaft (9).
A kind of 4. device of the controllable culture complex monocrystal of diffusion rate according to claim 1, it is characterised in that：Institute
The bottom for stating external container (1) offers bearing groove, and the bearing (11) is arranged on the inner chamber of bearing groove.
A kind of 5. device of the controllable culture complex monocrystal of diffusion rate according to claim 1, it is characterised in that：Institute
State and neck is offered at the top of external container (1), the bottom of the seal closure (3) is connected to the inner chamber of neck.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720347754.3U CN206887267U (en) | 2017-04-05 | 2017-04-05 | A kind of device of the controllable culture complex monocrystal of diffusion rate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720347754.3U CN206887267U (en) | 2017-04-05 | 2017-04-05 | A kind of device of the controllable culture complex monocrystal of diffusion rate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206887267U true CN206887267U (en) | 2018-01-16 |
Family
ID=61323484
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720347754.3U Expired - Fee Related CN206887267U (en) | 2017-04-05 | 2017-04-05 | A kind of device of the controllable culture complex monocrystal of diffusion rate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206887267U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109652854A (en) * | 2018-12-29 | 2019-04-19 | 宁波卢米蓝新材料有限公司 | A kind of single crystal cultivation device and monocrystal cultivation method |
| CN113718341A (en) * | 2021-09-02 | 2021-11-30 | 郑州大学 | Visual single crystal culture apparatus |
-
2017
- 2017-04-05 CN CN201720347754.3U patent/CN206887267U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109652854A (en) * | 2018-12-29 | 2019-04-19 | 宁波卢米蓝新材料有限公司 | A kind of single crystal cultivation device and monocrystal cultivation method |
| CN113718341A (en) * | 2021-09-02 | 2021-11-30 | 郑州大学 | Visual single crystal culture apparatus |
| CN113718341B (en) * | 2021-09-02 | 2022-04-22 | 郑州大学 | Visual single crystal culture apparatus |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180116 Termination date: 20180405 |