CN1830915A - Biological organic fertilizer contg. pyroligneous liquor and its prepn. method - Google Patents

Biological organic fertilizer contg. pyroligneous liquor and its prepn. method Download PDF

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Publication number
CN1830915A
CN1830915A CNA2006100458000A CN200610045800A CN1830915A CN 1830915 A CN1830915 A CN 1830915A CN A2006100458000 A CNA2006100458000 A CN A2006100458000A CN 200610045800 A CN200610045800 A CN 200610045800A CN 1830915 A CN1830915 A CN 1830915A
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China
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pyroligneous liquor
organic fertilizer
bio
chamajasmin
ailanthone
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CNA2006100458000A
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Chinese (zh)
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冯善有
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Individual
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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Abstract

An organic fertilizer with durable fertility, and high effect to prevent and eliminate diseases and pests, benefit the reproduction of useful bacteria, and decomposed the harmful chemical residue and residual plant and animal is proportionally prepared from wooden vinegar, chitosan, ailanthinone and extract of fischer euphorbia root.

Description

A kind of pyroligneous liquor bio-organic fertilizer and preparation method thereof
Technical field the present invention relates to a kind of ecological organic fertilizer, especially a kind of pyroligneous liquor bio-organic fertilizer that utilizes pyroligneous liquor for carrier.The invention still further relates to the making method of this organic fertilizer.
Background technology is present, hazard residue material at food agricultural produce is too high, soil with organic matter content continues to reduce, the problem that the disease and pest resistance strengthens, ecotope is seriously damaged, the domestic and international ecological organic fertilizer of all developing green non-pollution at active development.The organic fertilizer ubiquity that existing development is used to pest repelling effects such as insect, scale insects a little less than, include total nutrient and be not enough to satisfy crop demand, release structures defectiveness, that fertilizer efficiency is difficult for is lasting, material choice does not pass a test, quality be cannot say for sure shortcomings such as card.
Summary of the invention the purpose of this invention is to provide a kind of lasting pyroligneous liquor bio-organic fertilizer that adapts to practical situation behind China's soil long-term application chemical fertilizer simultaneously again of stronger disease and insect resistance, fertilizer efficiency that has.
Another object of the present invention provides the making method of this pyroligneous liquor bio-organic fertilizer.
For achieving the above object, the present invention adopts following technical scheme: it is mixed and made into by weight ratio by following raw material, pyroligneous liquor 52-80%, chitosan 12-40%, ailanthone 1-3%, chamajasmin 3-5%.
Pyroligneous liquor in this pyroligneous liquor bio-organic fertilizer extracts from the herbal drug Herba Oxalidis Corniculatae, contain the required trace element of abundant plant, has extremely strong seepage force and sticking power, utilize these characteristics of pyroligneous liquor, generate compound prescription such as the chitosan composition that has additional nutrients by adding fermented-source of fish marine organisms; Strengthen slow release effect by the gel-like substance in the fermented-marine organisms glycan.Strengthen pest-resistant, the bactericidal properties of fertilizer by potent traditional Chinese medicine ingredients such as the ailanthone that adds flavonoid, the chamajasmin compound of terpene; Can be at the characteristics of denitrification flora weak tendency in the chemical fertilizer of China's soil deposition, the soil, the present invention adds the nutritive substance of the useful active flora breeding of multiple suitable soil, promote the breeding of soil beneficial organism population, and then change soil physico-chemical property, decompose the harmful chemical residual of soil, increase is strengthened organic matter accumulation to the capacity of decomposition of plant and animal residues.
As the further improvement of technical solution of the present invention, be mixed and made into pyroligneous liquor 52-80%, chitosan 1240%, matrine 1-4%, ailanthone 1-3%, chamajasmin 3-5% by weight ratio by following raw material.Wherein matrine has desinsection, anti-microbial effect.
As the further improvement of technical solution of the present invention, be mixed and made into pyroligneous liquor 50-80%, chitosan 12-40%, matrine 1-4%, ailanthone 1-3%, chamajasmin 3-5%, vulgarin 3-10% by weight ratio by following raw material.Wherein vulgarin has expelling parasite, strengthens the crop blade face to the nutrient absorbing effect.
Optimal way of the present invention is to be mixed and made into pyroligneous liquor 50%, chitosan 39%, matrine 2%, ailanthone 3%, chamajasmin 3%, vulgarin 3% by the optimum weight proportioning by following raw material.
Described ailanthone can be any flavonoid antimicrobial compoundss such as Stellera chamaejasme L. glucoside, rotenoid.
Described chamajasmin can have material antibiotic, insecticidal action for any terpenes such as sesquiterpene lactones class, triterpenes sulfation triterpenoid saponins.
Described matrine can have desinsection, anti-microbial effect alkaloids for coniine, napelline, wilforine, Stemoninine, Jervine, false Jervine, rubine Jervine, germerine, veratroylzygadenine etc. are any.
Because the present invention has selected potent pest-resistant herbal medicine for use, insect resistance capacity reaches more than 80%, and the fertilizer efficiency sustainability reached 70-100 days from 50-70 days.Use the nutrient situation of pyroligneous liquor of the present invention to be significantly improved, detect, use the pyroligneous liquor nutrient changing value of the present invention front and back to see the following form through Chinese materia medica Molecular Biology Lab of Dalian Medical Univ:
Before using product of the present invention After using product of the present invention
PH 3.91 PH 3.24
Potassium 0.13mmol/l Potassium 9.67mmol/l
Phosphorus 0.31mmol/l Phosphorus 11.14mmol/l
Total protein 11.7g/l Total protein 62.3g/l
Blood urea nitrogen 1.7mg/dl Blood urea nitrogen 34.4mg/dl
Creatinine 699.7umol/l Creatinine 1863.8umol/l
Effectively viable bacteria falls 0 The effective viable bacteria 57CFU/ml that falls
In addition by adding the nutritive substance of the useful active flora breeding of multiple suitable soil, promote the breeding of soil beneficial organism population, and then change soil physico-chemical property, decompose the harmful chemical residual of soil, increase capacity of decomposition, discharge that a part has been hydrolyzed or oxidation fixed nitrogen, phosphoric plant and animal residues, strengthen the accumulation of organic matter decomposition and humic acids, the little ecology of rehabilitating soil progressively, the balance soil nutrient status strengthens farm crop self resistance.Simultaneously effectively having utilized crop straw, is to return crop stocks to the field to improve another effective means of added value.
Description of drawings Fig. 1 is the process flow sheet of pyroligneous liquor bio-organic fertilizer of the present invention and preparation method thereof.
Embodiment as shown in Figure 1, pyroligneous liquor bio-organic fertilizer of the present invention and preparation method thereof is for to be made by following raw material and operation.Concrete operations are as follows: at first, trees branch, gramineous crop straw, fruit tree tree-pruning branch etc. are pulverized the partial heat energy that mixes through the steam boiler generation, carry out 100 ℃ of-450 ℃ of destructive distillation processing and make pyroligneous liquor solution.Again Chinese medicine materials such as kuh-seng, tree-of-heaven skin, the root of langdu, radix aconiti agrestis, hemlock, trypterygine, black false hellebore, argy wormwood, trifoliate jewelvine are mixed, different properties according to above-mentioned each Chinese medicine material composition, adopt methods such as hydrolysis lixiviate, supercritical extraction, hydro-thermal lixiviate, alcohol extracting, oil immersion body to extract, carry out separation and purification again and become drug crystallization or mixture suspension liquid, emulsion etc.Simultaneously edible mushrooms piece such as edible Xianggu-mushroom being adopted mixing such as substratum behind the mushroom etc., fishery products tankage such as fish, shrimp, shell mixes with the pyroligneous liquor solution that has prepared, simple substance crystallization or mixture suspension liquid, emulsion proportioning through solid fermentation, through centrifugal separation process after gas-chromatography, liquid chromatography, mass spectroscopy after the assay was approved, are carried out the canned and solids package of liquid.Can make following three kinds of products:
Embodiment one:
Contain pyroligneous liquor 50%, chitosan 39%, matrine 2%, ailanthone 3%, chamajasmin 3%, vulgarin 3%.
Embodiment two:
Contain pyroligneous liquor 80%, chitosan 10%, matrine 2%, ailanthone 1.5%, chamajasmin 3.5%, vulgarin 3%.
Embodiment three:
Contain pyroligneous liquor 65%, chitosan 25%, matrine 2.5%, ailanthone 2%, chamajasmin 2.5%, vulgarin 3%.
The present invention is by adding the nutritive substance of the useful active flora breeding of multiple suitable soil, promote the breeding of soil beneficial organism population, and then change soil physico-chemical property, decompose the harmful chemical residual of soil, increase is strengthened the soil with organic matter accumulation to the capacity of decomposition of plant and animal residues.

Claims (8)

1, a kind of pyroligneous liquor bio-organic fertilizer, it is characterized in that: it is mixed and made into by weight ratio by following raw material, pyroligneous liquor 52-80%, chitosan 12-40%, ailanthone 1-3%, chamajasmin 3-5%.
2, a kind of pyroligneous liquor bio-organic fertilizer, it is characterized in that: it is mixed and made into by weight ratio by following raw material, pyroligneous liquor 52-80%, chitosan 12-40%, ailanthone 1-3%, chamajasmin 3-5%, matrine 1-4%.
3, a kind of pyroligneous liquor bio-organic fertilizer, it is characterized in that: it is mixed and made into by weight ratio by following raw material, pyroligneous liquor 50-80%, chitosan 12-40%, ailanthone 1-3%, chamajasmin 3-5%, matrine 1-4%, vulgarin 3-10%.
4, according to any described pyroligneous liquor bio-organic fertilizer of claim 1 to 3, it is characterized in that: it is mixed and made into by the optimum weight proportioning by following raw material, pyroligneous liquor 50%, chitosan 39%, matrine 2%, ailanthone 3%, chamajasmin 3%, vulgarin 3%.
5, according to any described pyroligneous liquor bio-organic fertilizer of claim 1 to 4, it is characterized in that: described ailanthone can be any flavonoid antimicrobial compoundss such as Stellera chamaejasme L. glucoside, rotenoid.
6, according to any described pyroligneous liquor bio-organic fertilizer of claim 1 to 4, it is characterized in that: described chamajasmin can be any terpene substances such as sesquiterpene lactones class, triterpenes sulfation triterpenoid saponin.
7, according to any described pyroligneous liquor bio-organic fertilizer of claim 2 to 4, it is characterized in that: described matrine can be any alkaloidss such as coniine, napelline, wilforine, Stemoninine, Jervine, false Jervine, rubine Jervine, germerine, veratroylzygadenine.
8, a kind of making method of pyroligneous liquor bio-organic fertilizer, it is characterized in that: at first, trees branch, gramineous crop straw, fruit tree tree-pruning branch etc. are pulverized the partial heat energy that mixes through the steam boiler generation, carry out 100 ℃ of-450 ℃ of destructive distillation processing and make pyroligneous liquor solution.Again Chinese medicine materials such as kuh-seng, tree-of-heaven skin, the root of langdu, radix aconiti agrestis, hemlock, trypterygine, black false hellebore, argy wormwood, trifoliate jewelvine are mixed, different properties according to above-mentioned each Chinese medicine material composition, method is extracted to adopt that hydrolysis lixiviate, supercritical extraction, hydro-thermal lixiviate, alcohol extracting, oil immersion are carried etc., becomes herbal liquid medicine carrying out separation and purification.Simultaneously edible mushrooms piece such as edible Xianggu-mushroom being adopted mixing such as substratum behind the mushroom etc., fishery products tankage such as fish, shrimp, shell mixes with the pyroligneous liquor solution that has prepared, herbal liquid medicine proportioning through fermentation, through centrifugal separation process after gas-chromatography, liquid chromatography, mass spectrum inspection qualified after, make and contain 50% pyroligneous liquor, 39% chitosan, 2% matrine, 3% ailanthone, 3% chamajasmin, 3% vulgarin, carry out the canned and solids package of liquid.
CNA2006100458000A 2006-01-28 2006-01-28 Biological organic fertilizer contg. pyroligneous liquor and its prepn. method Pending CN1830915A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102349551A (en) * 2011-07-21 2012-02-15 北京林业大学 Plant culturing medium regulator and preparation method thereof
CN105348016A (en) * 2015-12-10 2016-02-24 北京林业大学 Compound fertilizer containing wood vinegar and Chinese herbal medicine for promoting garlic growth
CN105994332A (en) * 2016-06-19 2016-10-12 殷佩琼 Composition for controlling potato beetles and preparation method of composition
CN106490035A (en) * 2016-10-31 2017-03-15 郑州思辩科技有限公司 One grows tobacco special Anti-bacterium agricultural chemicals and preparation method thereof
CN108323382A (en) * 2018-01-29 2018-07-27 广西宜州天源绿佳农业科技有限公司 A kind of implantation methods of pawpaw
CN111620888A (en) * 2018-02-13 2020-09-04 陕西含光生物科技有限公司 Method for preparing ailanthinone by utilizing biological fermentation technology

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102349551A (en) * 2011-07-21 2012-02-15 北京林业大学 Plant culturing medium regulator and preparation method thereof
CN102349551B (en) * 2011-07-21 2014-04-02 北京林业大学 Plant culturing medium regulator and preparation method thereof
CN105348016A (en) * 2015-12-10 2016-02-24 北京林业大学 Compound fertilizer containing wood vinegar and Chinese herbal medicine for promoting garlic growth
CN105994332A (en) * 2016-06-19 2016-10-12 殷佩琼 Composition for controlling potato beetles and preparation method of composition
CN106490035A (en) * 2016-10-31 2017-03-15 郑州思辩科技有限公司 One grows tobacco special Anti-bacterium agricultural chemicals and preparation method thereof
CN108323382A (en) * 2018-01-29 2018-07-27 广西宜州天源绿佳农业科技有限公司 A kind of implantation methods of pawpaw
CN111620888A (en) * 2018-02-13 2020-09-04 陕西含光生物科技有限公司 Method for preparing ailanthinone by utilizing biological fermentation technology

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