CN105994332A - Composition for controlling potato beetles and preparation method of composition - Google Patents
Composition for controlling potato beetles and preparation method of composition Download PDFInfo
- Publication number
- CN105994332A CN105994332A CN201610443571.1A CN201610443571A CN105994332A CN 105994332 A CN105994332 A CN 105994332A CN 201610443571 A CN201610443571 A CN 201610443571A CN 105994332 A CN105994332 A CN 105994332A
- Authority
- CN
- China
- Prior art keywords
- parts
- copper sulfate
- tricresyl phosphate
- ethoxysulfuron
- ailanthinone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/36—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< directly attached to at least one heterocyclic ring; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/14—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
- A01N59/20—Copper
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a composition for controlling potato beetles and a preparation method of the composition. The composition is prepared from, by weight, 15-25 parts of ethoxysulfuron, 10-20 parts of ailanthone, 120-140 parts of ethyl alcohol, 440-480 parts of water and 7-9 parts of synergist tricresyl phosphate and copper sulfate, wherein the weight ratio of tricresyl phosphate to copper sulfate is (6-8):1. The composition can control the potato beetles and can be developed into a pesticide controlling the potato beetles, the controlling effect is related to the weight ratio of the synergist tricresyl phosphate to copper sulfate, and when the weight ratio of tricresyl phosphate to copper sulfate is (6-8):1, the controlling effect is the best.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating colorado potato bug and preparation method thereof.
Background technology
Ethoxysulfuron is a kind of highy potent herbicide preventing and kill off direct sowing of rice field weed, and its mechanism of action is to be inhaled by weeds root and stem and leaf
It is transmitted to after receipts in plant, stops Amino acid synthesis, and suppress rapidly the growth of weeds stem and leaf and root to extend, finally result in
Weeds are the most withered.It is mainly used in preventing and kill off annual broadleaf weed, such as Herba monochoriae vaginalis, Herba Ludwigiae Prostratae, mexicana, Herba Cyperi Difformis, pool
Rush down, Sagittaria trifolia L. Var. Angusti-folia(Sieb.) Kitag.(Sagittaria sagittifolia L.) etc..There is the features such as dispenser phase width, easy to use and safety be good.
Have not yet to see ethoxysulfuron and work in coordination with the report preventing and treating colorado potato bug with ailanthinone.
Summary of the invention
It is an object of the invention to provide the compositions of a kind of preventing and treating colorado potato bug containing ethoxysulfuron and ailanthinone and at pesticide
In application.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating colorado potato bug, including the raw material of following weight portion: ethoxysulfuron, 15～25 parts；Ailanthinone,
10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Totally 7～9 parts of synergist tricresyl phosphate and copper sulfate, phosphorus
The weight ratio of acid front three phenolic ester and copper sulfate is 6～8:1.
Further, the compositions of described preventing and treating colorado potato bug includes the raw material of following weight portion: ethoxysulfuron, 20 parts；
Ailanthinone, 15 parts；Ethanol, 130 parts；Water, 460 parts；Totally 8 parts of synergist tricresyl phosphate and copper sulfate, tricresyl phosphate
The weight ratio of cresol ester and copper sulfate is 7:1.
Further, the compositions of described preventing and treating colorado potato bug includes the raw material of following weight portion: ethoxysulfuron, 15 parts；
Ailanthinone, 10 parts；Ethanol, 120 parts；Water, 440 parts；Totally 7 parts of synergist tricresyl phosphate and copper sulfate, tricresyl phosphate
The weight ratio of cresol ester and copper sulfate is 6:1.
Further, the compositions of described preventing and treating colorado potato bug includes the raw material of following weight portion: ethoxysulfuron, 25 parts；
Ailanthinone, 20 parts；Ethanol, 140 parts；Water, 480 parts；Totally 9 parts of synergist tricresyl phosphate and copper sulfate, tricresyl phosphate
The weight ratio of cresol ester and copper sulfate is 8:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, by ethoxysulfuron, ailanthinone and synergist tricresyl phosphate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat colorado potato bug, can develop into the pesticide of preventing and treating colorado potato bug.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit scope with this.To the greatest extent
The present invention is explained in detail by pipe with reference to preferred embodiment, it will be understood by those within the art that, can be to the present invention
Technical scheme modify or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating colorado potato bug
Parts by weight of raw materials compares:
Ethoxysulfuron, 20 parts；Ailanthinone, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist tricresyl phosphate and
Totally 8 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 7:1.
Preparation method:
Step S1, by ethoxysulfuron, ailanthinone and synergist tricresyl phosphate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating colorado potato bug
Parts by weight of raw materials compares:
Ethoxysulfuron, 15 parts；Ailanthinone, 10 parts；Ethanol, 120 parts；Water, 440 parts；Synergist tricresyl phosphate and
Totally 7 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 6:1.
Preparation method:
Step S1, by ethoxysulfuron, ailanthinone and synergist tricresyl phosphate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating colorado potato bug
Parts by weight of raw materials compares:
Ethoxysulfuron, 25 parts；Ailanthinone, 20 parts；Ethanol, 140 parts；Water, 480 parts；Synergist tricresyl phosphate and
Totally 9 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 8:1.
Preparation method:
Step S1, by ethoxysulfuron, ailanthinone and synergist tricresyl phosphate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating colorado potato bug
Parts by weight of raw materials compares:
Ethoxysulfuron, 20 parts；Ailanthinone, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist tricresyl phosphate and
Totally 8 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 6:1.
Preparation method:
Step S1, by ethoxysulfuron, ailanthinone and synergist tricresyl phosphate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating colorado potato bug
Parts by weight of raw materials compares:
Ethoxysulfuron, 20 parts；Ailanthinone, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist tricresyl phosphate and
Totally 8 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 8:1.
Preparation method:
Step S1, by ethoxysulfuron, ailanthinone and synergist tricresyl phosphate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, tricresyl phosphate and copper sulfate is 5:1
Parts by weight of raw materials compares:
Ethoxysulfuron, 20 parts；Ailanthinone, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist tricresyl phosphate and
Totally 8 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 5:1.
Preparation method:
Step S1, by ethoxysulfuron, ailanthinone and synergist tricresyl phosphate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, tricresyl phosphate and copper sulfate is 9:1
Parts by weight of raw materials compares:
Ethoxysulfuron, 20 parts；Ailanthinone, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist tricresyl phosphate and
Totally 8 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 9:1.
Preparation method:
Step S1, by ethoxysulfuron, ailanthinone and synergist tricresyl phosphate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
The compositions of the testing example 1～7 preparation preventing and treating effective percentage (%) to colorado potato bug respectively.
During use, present composition water carries out 40 times of dilutions, and fountain height is 25 liters/mu.
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 100 |
| Embodiment 4 | 98 |
| Embodiment 5 | 99 |
| Embodiment 6 | 72 |
| Embodiment 7 | 74 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat colorado potato bug, can develop into preventing and treating colorado potato bug
Pesticide, prevention effect is relevant with the weight ratio of synergist tricresyl phosphate and copper sulfate in raw material, tricresyl phosphate
When being 6～8:1 with the weight ratio of copper sulfate, prevention effect is best.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit protection scope of the present invention with this.
It will be understood by those within the art that, technical scheme can be modified or equivalent, and not take off
Essence and protection domain from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating colorado potato bug, it is characterised in that include the raw material of following weight portion: ethoxysulfuron, 15～25
Part；Ailanthinone, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Synergist tricresyl phosphate and copper sulfate
Totally 7～9 parts, the weight ratio of tricresyl phosphate and copper sulfate is 6～8:1.
The compositions of preventing and treating colorado potato bug the most according to claim 1, it is characterised in that include the former of following weight portion
Material: ethoxysulfuron, 20 parts；Ailanthinone, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist tricresyl phosphate and
Totally 8 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 7:1.
The compositions of preventing and treating colorado potato bug the most according to claim 1, it is characterised in that include the former of following weight portion
Material: ethoxysulfuron, 15 parts；Ailanthinone, 10 parts；Ethanol, 120 parts；Water, 440 parts；Synergist tricresyl phosphate and
Totally 7 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 6:1.
The compositions of preventing and treating colorado potato bug the most according to claim 1, it is characterised in that include the former of following weight portion
Material: ethoxysulfuron, 25 parts；Ailanthinone, 20 parts；Ethanol, 140 parts；Water, 480 parts；Synergist tricresyl phosphate and
Totally 9 parts of copper sulfate, the weight ratio of tricresyl phosphate and copper sulfate is 8:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, by ethoxysulfuron, ailanthinone and synergist tricresyl phosphate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610443571.1A CN105994332A (en) | 2016-06-19 | 2016-06-19 | Composition for controlling potato beetles and preparation method of composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610443571.1A CN105994332A (en) | 2016-06-19 | 2016-06-19 | Composition for controlling potato beetles and preparation method of composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105994332A true CN105994332A (en) | 2016-10-12 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610443571.1A Pending CN105994332A (en) | 2016-06-19 | 2016-06-19 | Composition for controlling potato beetles and preparation method of composition |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106857681A (en) * | 2016-12-31 | 2017-06-20 | 新昌县云河虫害防治技术开发有限公司 | Kill insecticide of colorado potato bug and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61200901A (en) * | 1985-03-04 | 1986-09-05 | Sumitomo Chem Co Ltd | Herbicide |
| CN1830915A (en) * | 2006-01-28 | 2006-09-13 | 冯善有 | Biological organic fertilizer contg. pyroligneous liquor and its prepn. method |
| CN102217628A (en) * | 2011-05-06 | 2011-10-19 | 浙江泰达作物科技有限公司 | Ethoxysulfuron, fenoxaprop-ethyl and mefenpyr-diethyl emulsion in water and preparation method of emulsion |
| CN104413032A (en) * | 2013-09-06 | 2015-03-18 | 浙江泰达作物科技有限公司 | Ethoxysulfuron and fenoxaprop-p-ethyl compound emulsion in water and preparation method thereof |
-
2016
- 2016-06-19 CN CN201610443571.1A patent/CN105994332A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61200901A (en) * | 1985-03-04 | 1986-09-05 | Sumitomo Chem Co Ltd | Herbicide |
| CN1830915A (en) * | 2006-01-28 | 2006-09-13 | 冯善有 | Biological organic fertilizer contg. pyroligneous liquor and its prepn. method |
| CN102217628A (en) * | 2011-05-06 | 2011-10-19 | 浙江泰达作物科技有限公司 | Ethoxysulfuron, fenoxaprop-ethyl and mefenpyr-diethyl emulsion in water and preparation method of emulsion |
| CN104413032A (en) * | 2013-09-06 | 2015-03-18 | 浙江泰达作物科技有限公司 | Ethoxysulfuron and fenoxaprop-p-ethyl compound emulsion in water and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 印德麟 主编: "《简明精细化工大辞典》", 30 June 1999, 沈阳：辽宁科学技术出版社 * |
| 曹立耘: "硫酸铜在蔬菜病害防治上的使用", 《农药市场信息》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106857681A (en) * | 2016-12-31 | 2017-06-20 | 新昌县云河虫害防治技术开发有限公司 | Kill insecticide of colorado potato bug and preparation method thereof |
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Application publication date: 20161012 |