CN104351225B - A kind of Fructus Lycopersici esculenti antibacterial - Google Patents
A kind of Fructus Lycopersici esculenti antibacterial Download PDFInfo
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- CN104351225B CN104351225B CN201410630339.XA CN201410630339A CN104351225B CN 104351225 B CN104351225 B CN 104351225B CN 201410630339 A CN201410630339 A CN 201410630339A CN 104351225 B CN104351225 B CN 104351225B
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- tomato
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- zhongshengmycin
- garlicin
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 28
- VMFXMTJCTSYHCF-HHQUSWFZSA-N [(2r,3r,4s,5r)-5-(hexylamino)-4-hydroxy-2-(hydroxymethyl)-6-[(7-hydroxy-4-oxo-1,3a,5,6,7,7a-hexahydroimidazo[4,5-c]pyridin-2-yl)amino]oxan-3-yl] carbamate Chemical group CCCCCCN[C@@H]1[C@H](O)[C@@H](OC(N)=O)[C@@H](CO)OC1\N=C\1NC(C(=O)NCC2O)C2N/1 VMFXMTJCTSYHCF-HHQUSWFZSA-N 0.000 claims abstract description 35
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 32
- 235000007688 Lycopersicon esculentum Nutrition 0.000 claims abstract description 32
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims abstract description 28
- 230000001580 bacterial effect Effects 0.000 claims abstract description 16
- 239000004615 ingredient Substances 0.000 claims abstract description 15
- 229920001353 Dextrin Polymers 0.000 claims abstract description 14
- 239000004375 Dextrin Substances 0.000 claims abstract description 14
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 14
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims abstract description 14
- 235000019425 dextrin Nutrition 0.000 claims abstract description 14
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 14
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 14
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 14
- 229920002545 silicone oil Polymers 0.000 claims abstract description 14
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 6
- 241000227653 Lycopersicon Species 0.000 claims abstract 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 239000002994 raw material Substances 0.000 claims description 8
- 238000005507 spraying Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 30
- 230000002265 prevention Effects 0.000 abstract description 23
- 239000000839 emulsion Substances 0.000 abstract description 13
- 230000002045 lasting effect Effects 0.000 abstract description 2
- 240000003768 Solanum lycopersicum Species 0.000 description 24
- 239000003814 drug Substances 0.000 description 19
- 239000007921 spray Substances 0.000 description 18
- 239000000575 pesticide Substances 0.000 description 16
- 238000002360 preparation method Methods 0.000 description 9
- 239000000203 mixture Substances 0.000 description 7
- 239000004530 micro-emulsion Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 240000002234 Allium sativum Species 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- 239000003899 bactericide agent Substances 0.000 description 3
- 235000004611 garlic Nutrition 0.000 description 3
- 238000001228 spectrum Methods 0.000 description 3
- 241000234282 Allium Species 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- 208000035143 Bacterial infection Diseases 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 241000233866 Fungi Species 0.000 description 2
- 208000031888 Mycoses Diseases 0.000 description 2
- 244000052616 bacterial pathogen Species 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- JDLKFOPOAOFWQN-VIFPVBQESA-N Allicin Natural products C=CCS[S@](=O)CC=C JDLKFOPOAOFWQN-VIFPVBQESA-N 0.000 description 1
- 241000234280 Liliaceae Species 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- JDLKFOPOAOFWQN-UHFFFAOYSA-N allicin Chemical compound C=CCSS(=O)CC=C JDLKFOPOAOFWQN-UHFFFAOYSA-N 0.000 description 1
- 235000010081 allicin Nutrition 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 208000022362 bacterial infectious disease Diseases 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- OPQARKPSCNTWTJ-UHFFFAOYSA-L copper(ii) acetate Chemical compound [Cu+2].CC([O-])=O.CC([O-])=O OPQARKPSCNTWTJ-UHFFFAOYSA-L 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000035772 mutation Effects 0.000 description 1
- 150000002898 organic sulfur compounds Chemical class 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000004763 spore germination Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000004563 wettable powder Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of Fructus Lycopersici esculenti antibacterial, described Fructus Lycopersici esculenti antibacterial is aqueous emulsion, and effective ingredient is Zhongshengmycin and garlicin, and auxiliary agent is white dextrin, Polyethylene Glycol, silicone oil, styrene polyoxyethylene ether ammonium sulfate salt, ethanol.Tomato bacterial angular leaf spot and graw mold of tomato are had extraordinary prevention effect by the present invention, the present invention utilizes Zhongshengmycin and garlicin that tomato bacterial angular leaf spot and graw mold of tomato have the effect of preventing and treating and potentiation simultaneously, effectively enhance the prevention to tomato bacterial angular leaf spot and graw mold of tomato and the effect for the treatment of, instant effect, lasting period is long, on non-Target crops without impact.
Description
Technical field
The present invention relates to a kind of Fructus Lycopersici esculenti antibacterial, be specifically related to a kind of aqueous emulsion for preventing and treating tomato bacterial angular leaf spot and graw mold of tomato, its effective ingredient is Zhongshengmycin and garlicin, belongs to technical field of pesticide.
Background technology
Zhongshengmycin belongs to N-glucosides class, is the agricultural bactericidal antibiotic of a kind of wide spectrum, by suppressing the synthesis of bacterium protein and making filamentous fungi mycelia deformity, thus suppressing spore germination and killing spore and cause that pathogenic bacteria is dead.Can resisting gram-positive, negative bacteria, mycobacteria, yeast and filamentous fungi.Producing strains of Zhongshengmycin and preparation method thereof is provided by patent ZL200310103250.X, this disclosure of the invention Strepiomyces lavendulae Hainan mutation CGMCCNo.1026, and after being fermented, obtain Zhongshengmycin by CGMCCNo.1026, provide the method being prepared Zhongshengmycin by this strain simultaneously.Patent ZL200310103513.7 wettable powder composition then providing Zhongshengmycin and preparation method thereof.Patent ZL200510044505.9 provides a kind of agricultural bactericidal composition for plant disease, and said composition is formed by Zhongshengmycin and copper acetate are composite.Zhongshengmycin is a class new antibiotic, and various bacterial disease and fungal disease to crops all have good effect.But on the whole, the complex preparation kind of current Zhongshengmycin is less, it is badly in need of developing its compound product, expands its fungicidal spectrum.
Garlicin (Allicin) is a kind of organosulfur compound extracted from the bulb (Bulbus Allii head) of Liliaceae allium Bulbus Allii (AlliumSativum), exists in Bulbus Allii Cepae and other alliums.Formal name used at school GIUCOSinoate.Pale yellow oily liquid body.Boiling point 80-85 DEG C (0.2kPa), relative density 1.112(20/4 DEG C), index of refraction 1.561.It is dissolved in ethanol, chloroform or ether.Dissolubility 2.5% (quality) (10 DEG C) in water, its pH value of water solution is 6.5, has grease precipitate to be formed during standing.Can dissolve each other with ethanol, ether and benzene.Thermokalite is unstable, acid is stable.By in the bulb being present in liliaceous plant Bulbus Allii, the garlic aminoacid existed converting generation under big allinase effect.Exist in the bulb of Herba Alii fistulosi.Having strong big garlic odour, taste is peppery.
In agricultural production practice, bacterial diseases of plants and fungal disease usually mix generation.Chemical prevention is the important channel alleviating disease loss, boosting agricultural yield.Some bactericidal agent for preventing and treating spectrum is narrower, and peasant must use together in various sterilization agent.But, for a long time, applied chemistry antibacterial in large quantities, it can be developed immunity to drugs so that preventive effect declines rapidly by pathogenic bacteria, it has to strengthens consumption.The abuse of chemical bactericide result in serious environmental pollution and food-safety problem.The exploitation of novel biological bactericide is the important method cracking above-mentioned dilemma.
Summary of the invention
For the problems referred to above, the invention provides a kind of Fructus Lycopersici esculenti antibacterial, be specifically related to a kind of aqueous emulsion for preventing and treating tomato bacterial angular leaf spot and graw mold of tomato, its effective ingredient is Zhongshengmycin and garlicin, instant effect of the present invention, holding effect are long, to non-Target crops safety.
Technical scheme is as follows:
A kind of Fructus Lycopersici esculenti antibacterial, described Fructus Lycopersici esculenti antibacterial is aqueous emulsion, and effective ingredient is Zhongshengmycin and garlicin, and auxiliary agent is white dextrin, Polyethylene Glycol, silicone oil, styrene polyoxyethylene ether ammonium sulfate salt, ethanol.
Further, in antibacterial of the present invention, each raw material components is by mass percentage:
Zhongshengmycin 0.1%-1%, garlicin 0.1%-1%, white dextrin 0.01%-0.1%, Polyethylene Glycol 1%-10%, silicone oil 0.1%-0.4%, styrene polyoxyethylene ether ammonium sulfate salt 5%-10%, ethanol 3%-8%, deionized water supply 100%.
Further, in antibacterial of the present invention, each raw material components is by mass percentage:
Zhongshengmycin 0.1%-0.6%, garlicin 0.1%-0.6%, white dextrin 0.02%-0.09%, Polyethylene Glycol 2%-8%, silicone oil 0.15%-0.35%, styrene polyoxyethylene ether ammonium sulfate salt 5.5%-8%, ethanol 4%-7%, deionized water supply 100%.
Further, in antibacterial of the present invention, each raw material components is by mass percentage:
Zhongshengmycin 0.15%-0.5%, garlicin 0.2%-0.6%, white dextrin 0.03%-0.08%, Polyethylene Glycol 3%-5%, silicone oil 0.2%-0.35%, styrene polyoxyethylene ether ammonium sulfate salt 6%-8%, ethanol 4%-6%, deionized water supply 100%.
Further, in antibacterial of the present invention, each raw material components is by mass percentage:
Zhongshengmycin 0.15%, garlicin 0.35%, white dextrin 0.06%, Polyethylene Glycol 5%, silicone oil 0.3%, styrene polyoxyethylene ether ammonium sulfate salt 7%, ethanol 5%, deionized water supply 100%.
Described Fructus Lycopersici esculenti antibacterial is used for preventing and treating tomato bacterial angular leaf spot and graw mold of tomato, early stage dispenser of falling ill；Annual spraying times is 1 or 2 time；Effective ingredient dosage is 3 grams/ha-10 grams/ha, it is preferred that dosage is 4.5 grams/ha.
Tomato bacterial angular leaf spot and graw mold of tomato are had extraordinary prevention effect by the present invention, the present invention utilizes Zhongshengmycin and garlicin that tomato bacterial angular leaf spot and graw mold of tomato have the effect of preventing and treating and potentiation simultaneously, effectively enhance the prevention to tomato bacterial angular leaf spot and graw mold of tomato and the effect for the treatment of, instant effect, lasting period is long, on non-Target crops without impact.
Detailed description of the invention
Below in conjunction with specific embodiment further describe the present invention, advantages of the present invention and feature will be with describe and apparent.But embodiment is only exemplary, the scope of the present invention is not constituted any restriction.It will be understood by those skilled in the art that and the details of technical solution of the present invention and form can be modified or replace lower without departing from the spirit and scope of the present invention, but these amendments and replacement each fall within protection scope of the present invention.
1 one kinds of Fructus Lycopersici esculenti antibacterial of embodiment
Effective ingredient is Zhongshengmycin and garlicin, and auxiliary agent is white dextrin, Polyethylene Glycol, silicone oil, styrene polyoxyethylene ether ammonium sulfate salt, ethanol.
In antibacterial, each raw material components is by mass percentage:
Zhongshengmycin 0.15%, garlicin 0.35%, white dextrin 0.06%, Polyethylene Glycol 5%, silicone oil 0.3%, styrene polyoxyethylene ether ammonium sulfate salt 7%, ethanol 5%, deionized water supply 100%.
By above-mentioned each composition application conventional pesticide process technology, the aqueous emulsion goods being suitable for agriculturally using made.In the present embodiment, the co-toxicity coefficient of Zhongshengmycin and garlicin is 286.24.
It is used for preventing and treating tomato bacterial angular leaf spot by the aqueous emulsion that the embodiment of the present invention 1 obtains, tomato bacterial angular leaf spot their early stage dispenser, effective ingredient dosage is 4.5 grams/ha, sprays 2 times, the prevention effect of 7 days, 14 days respectively 81.2%, 83.3% after secondary medicine.1% Zhongshengmycin microemulsion by 4.17 grams/ha of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 60.3%, 56.4% after secondary medicine.0.3% garlicin water preparation by 2000 times of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 59.6%, 62.3% after secondary medicine.
The aqueous emulsion that the embodiment of the present invention 1 obtains is used for preventing and treating graw mold of tomato, graw mold of tomato their early stage dispenser, and effective ingredient dosage is 4.5 grams/ha, sprays 2 times, the prevention effect of 7 days, 14 days respectively 83.6%, 89.5% after secondary medicine.1% Zhongshengmycin microemulsion by 4.5 grams/ha of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 55.6%, 59.4% after secondary medicine.0.3% garlicin water preparation by 3000 times of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 63.8%, 69.1% after secondary medicine.
2 one kinds of Fructus Lycopersici esculenti antibacterial of embodiment
Effective ingredient is Zhongshengmycin and garlicin, and auxiliary agent is white dextrin, Polyethylene Glycol, silicone oil, styrene polyoxyethylene ether ammonium sulfate salt, ethanol.
In antibacterial, each raw material components is by mass percentage:
Zhongshengmycin 0.1%, garlicin 0.9%, white dextrin 0.05%, Polyethylene Glycol 3%, silicone oil 0.1%, styrene polyoxyethylene ether ammonium sulfate salt 6%, ethanol 3%, deionized water supply 100%.
By above-mentioned each composition application conventional pesticide process technology, the aqueous emulsion goods being suitable for agriculturally using made.In the present embodiment, the co-toxicity coefficient of Zhongshengmycin and garlicin is 254.32.
It is used for preventing and treating tomato bacterial angular leaf spot by the aqueous emulsion that the embodiment of the present invention 2 obtains, tomato bacterial angular leaf spot their early stage dispenser, effective ingredient dosage is 4.5 grams/ha, sprays 2 times, the prevention effect of 7 days, 14 days respectively 78.3%, 79.9% after secondary medicine.1% Zhongshengmycin microemulsion by 4.17 grams/ha of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 60.3%, 56.4% after secondary medicine.0.3% garlicin water preparation by 2000 times of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 59.6%, 62.3% after secondary medicine.
The aqueous emulsion that the embodiment of the present invention 2 obtains is used for preventing and treating graw mold of tomato, graw mold of tomato their early stage dispenser, and effective ingredient dosage is 4.5 grams/ha, sprays 2 times, the prevention effect of 7 days, 14 days respectively 81.2%, 83.6% after secondary medicine.1% Zhongshengmycin microemulsion by 4.5 grams/ha of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 55.6%, 59.4% after secondary medicine.0.3% garlicin water preparation by 3000 times of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 63.8%, 69.1% after secondary medicine.
3 one kinds of Fructus Lycopersici esculenti antibacterial of embodiment
Effective ingredient is Zhongshengmycin and garlicin, and auxiliary agent is white dextrin, Polyethylene Glycol, silicone oil, styrene polyoxyethylene ether ammonium sulfate salt, ethanol.
In antibacterial, each raw material components is by mass percentage:
Zhongshengmycin 0.9%, garlicin 0.1%, white dextrin 0.06%, Polyethylene Glycol 7%, silicone oil 0.3%, styrene polyoxyethylene ether ammonium sulfate salt 7%, ethanol 5%, deionized water supply 100%.
By above-mentioned each composition application conventional pesticide process technology, the aqueous emulsion goods being suitable for agriculturally using made.In the present embodiment, the co-toxicity coefficient of Zhongshengmycin and garlicin is 213.4.
It is used for preventing and treating tomato bacterial angular leaf spot by the aqueous emulsion that the embodiment of the present invention 3 obtains, tomato bacterial angular leaf spot their early stage dispenser, effective ingredient dosage is 4.5 grams/ha, sprays 2 times, the prevention effect of 7 days, 14 days respectively 80.2%, 81.4% after secondary medicine.1% Zhongshengmycin microemulsion by 4.17 grams/ha of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 60.3%, 56.4% after secondary medicine.0.3% garlicin water preparation by 2000 times of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 59.6%, 62.3% after secondary medicine.
The aqueous emulsion that the embodiment of the present invention 3 obtains is used for preventing and treating graw mold of tomato, graw mold of tomato their early stage dispenser, and effective ingredient dosage is 4.5 grams/ha, sprays 2 times, the prevention effect of 7 days, 14 days respectively 81.5%, 85.7% after secondary medicine.1% Zhongshengmycin microemulsion by 4.5 grams/ha of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 55.6%, 59.4% after secondary medicine.0.3% garlicin water preparation by 3000 times of spray pesticides 2 times, the prevention effect of 7 days, 14 days respectively 63.8%, 69.1% after secondary medicine.
Claims (1)
1. a Fructus Lycopersici esculenti antibacterial, it is characterised in that in described Fructus Lycopersici esculenti antibacterial, effective ingredient is Zhongshengmycin and garlicin, auxiliary agent is white dextrin, Polyethylene Glycol, silicone oil, styrene polyoxyethylene ether ammonium sulfate salt, ethanol；
In described antibacterial, each raw material components is by mass percentage:
Zhongshengmycin 0.15%, garlicin 0.35%, white dextrin 0.06%, Polyethylene Glycol 5%, silicone oil 0.3%, styrene polyoxyethylene ether ammonium sulfate salt 7%, ethanol 5%, deionized water supply 100%；
Described antibacterial is used for preventing and treating tomato bacterial angular leaf spot and graw mold of tomato；Dispenser period is morbidity early stage；Annual spraying times is 2 times；Dosage is 4.5 grams/ha.
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