CN1806660A - Method for preparing natural bamboo charcoal vinegar feed addictive - Google Patents
Method for preparing natural bamboo charcoal vinegar feed addictive Download PDFInfo
- Publication number
- CN1806660A CN1806660A CNA2006100495743A CN200610049574A CN1806660A CN 1806660 A CN1806660 A CN 1806660A CN A2006100495743 A CNA2006100495743 A CN A2006100495743A CN 200610049574 A CN200610049574 A CN 200610049574A CN 1806660 A CN1806660 A CN 1806660A
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- CN
- China
- Prior art keywords
- bamboo
- bamboo charcoal
- char
- natural
- pyrolkigneous liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011425 bamboo Substances 0.000 title claims abstract description 76
- 235000017166 Bambusa arundinacea Nutrition 0.000 title claims abstract description 74
- 235000017491 Bambusa tulda Nutrition 0.000 title claims abstract description 74
- 241001330002 Bambuseae Species 0.000 title claims abstract description 74
- 235000015334 Phyllostachys viridis Nutrition 0.000 title claims abstract description 74
- 239000003610 charcoal Substances 0.000 title claims abstract description 37
- 235000021419 vinegar Nutrition 0.000 title claims abstract description 15
- 239000000052 vinegar Substances 0.000 title claims abstract description 15
- 238000000034 method Methods 0.000 title claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 26
- 239000000843 powder Substances 0.000 claims abstract description 19
- 238000002360 preparation method Methods 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 5
- 239000000047 product Substances 0.000 claims description 8
- 239000011276 wood tar Substances 0.000 claims description 7
- 239000000126 substance Substances 0.000 claims description 6
- 238000009833 condensation Methods 0.000 claims description 4
- 230000005494 condensation Effects 0.000 claims description 4
- 239000012265 solid product Substances 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 2
- 241001465754 Metazoa Species 0.000 abstract description 8
- 244000144977 poultry Species 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000003242 anti bacterial agent Substances 0.000 abstract description 3
- 229940088710 antibiotic agent Drugs 0.000 abstract description 3
- 230000036039 immunity Effects 0.000 abstract description 3
- 235000016709 nutrition Nutrition 0.000 abstract description 2
- 230000035764 nutrition Effects 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 238000001035 drying Methods 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 231100000331 toxic Toxicity 0.000 abstract 1
- 230000002588 toxic effect Effects 0.000 abstract 1
- 241000287828 Gallus gallus Species 0.000 description 10
- 235000013330 chicken meat Nutrition 0.000 description 10
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 6
- 235000013601 eggs Nutrition 0.000 description 5
- 239000000654 additive Substances 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- 239000003674 animal food additive Substances 0.000 description 4
- 239000003814 drug Substances 0.000 description 4
- 230000007613 environmental effect Effects 0.000 description 4
- 235000019750 Crude protein Nutrition 0.000 description 3
- 239000004098 Tetracycline Substances 0.000 description 3
- 230000003115 biocidal effect Effects 0.000 description 3
- PLHJDBGFXBMTGZ-WEVVVXLNSA-N furazolidone Chemical compound O1C([N+](=O)[O-])=CC=C1\C=N\N1C(=O)OCC1 PLHJDBGFXBMTGZ-WEVVVXLNSA-N 0.000 description 3
- 229960001625 furazolidone Drugs 0.000 description 3
- 244000144972 livestock Species 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 235000013372 meat Nutrition 0.000 description 3
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 3
- 229910052753 mercury Inorganic materials 0.000 description 3
- 229940041669 mercury Drugs 0.000 description 3
- 235000013594 poultry meat Nutrition 0.000 description 3
- 230000002265 prevention Effects 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 229960002180 tetracycline Drugs 0.000 description 3
- 229930101283 tetracycline Natural products 0.000 description 3
- 235000019364 tetracycline Nutrition 0.000 description 3
- 150000003522 tetracyclines Chemical class 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 235000012000 cholesterol Nutrition 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 235000013336 milk Nutrition 0.000 description 2
- 239000008267 milk Substances 0.000 description 2
- 210000004080 milk Anatomy 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000011669 selenium Substances 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- 208000031295 Animal disease Diseases 0.000 description 1
- 239000002028 Biomass Substances 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 241000282887 Suidae Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000010171 animal model Methods 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 244000144987 brood Species 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 230000035568 catharsis Effects 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 244000038559 crop plants Species 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003640 drug residue Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 230000002496 gastric effect Effects 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000007726 management method Methods 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000011269 tar Substances 0.000 description 1
- JBQYATWDVHIOAR-UHFFFAOYSA-N tellanylidenegermanium Chemical compound [Te]=[Ge] JBQYATWDVHIOAR-UHFFFAOYSA-N 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
Landscapes
- Fodder In General (AREA)
Abstract
The invention provides a method of making natural charcoal vinegar poultry and animal strains feed stuff addition agent. Char bamboo timber at high temperature to get solid production-bamboo char; cool the production gas to get liquid bamboo pyroligneous; process bamboo char into bamboo char powder, dry said bamboo char into bamboo char powder in no-drying or natural condition with the pH8-10; Carry out refinishing treat to bamboo pyroligneous to remove harmful substance-bamboo gum, then the pH will be 2.6-3.2; extract bamboo pyroligneous and bamboo char in the quality of (2-5):100, use bamboo char powder to absorb, stir homogeneously, wrap it up into bags , and get the faintly alkaline production with pH7.0-7.2. The invention could replace antibiotics addition agent effectively; preparation and refinishing technique is simple; no toxic and side effect, provide all-round nutrition to poultry and animal strains, enhance immunity, support that poultry and animal strains and their productions are pure-natural, organic, nuisance free; the texture is soft, and the egg is elastic especially; reduce the smell in and out the animal house by half and improve the environment.
Description
Technical field
The present invention relates to a kind of preparation method of natural plant feed additives, relate in particular to a kind of preparation method of natural bamboo charcoal vinegar feed addictive.
Background technology
Feed addictive is of a great variety in the market, does not see open report at present about charcoal vinegar feed addictive.Existing feed addictive mainly is medicated premixs such as antibiotics and chemical synthesis, also useful plant feed additives.The shortcoming of antibiotic and chemical synthetic drug class additive is to use side effect very big for a long time, can cause that pathogenic microorganism develops immunity to drugs on the one hand, reduces the prevention effect of Animal diseases; Can in meat, egg, milk and environment, produce medicament residue on the other hand.Feed addictive is wanted compliance with environmental protection requirements, raising and the measure of maintenance Strategy on Sustainable Development along with people's environmental consciousness, the environmental protection of feed addictive will be that inevitably particularly the synthetic bigger feed addictive of some side effects that waits of antibiotic and chemical industry is progressively superseded, be green feed additive, again surrounding environment played catharsis.So developing a kind of diseases prevention, environmental protection, Eco-power feed addictive is the developing direction of 21 century.
Summary of the invention
In order to make full use of biomass resource, the object of the present invention is to provide a kind of preparation method of natural bamboo charcoal vinegar feed addictive, with powdered carbon and the formulated additive for farm animal feed of vinegar liquid.
The technical solution adopted for the present invention to solve the technical problems is that the step of this method is as follows:
1) with bamboo timber 600 ℃～1000 ℃ following charings, obtain solid product bamboo charcoal; The condensation of gas that produces obtains liquid bamboo pyrolkigneous liquid;
2) the bamboo charcoal is processed into the bamboo charcoal powder of 60～100 order particle diameters, dry bamboo charcoal powder under the moist or natural conditions or in the dry kiln, the pH8 of bamboo charcoal powder～10;
3) the bamboo pyrolkigneous liquid carries out refinement treatment, removes bamboo wood tar harmful substance, bamboo pyrolkigneous liquid pH2.6～3.2;
4) in bamboo pyrolkigneous liquid and bamboo charcoal quality (2～5): 100 ratios extract the bamboo pyrolkigneous liquid, absorb with the bamboo charcoal powder, make to stir, and are packaged into bag, promptly resultant weakly alkaline product with pH7.0～7.2.
Bamboo vinegar liquid makes bamboo wood tar component content＜1% through refinement treatment.
Adopt following analysis determining method: 1, the assay method of VBN, mercury, tetracycline, furazolidone in the chicken: (1) atomic absorption instrument method; (2) high performance liquid chromatography.2, crude protein, cholesterol adopt the OPA development process in the egg.3, in the chicken in VBN, mercury, tetracycline, furazolidone and the egg crude protein, cholesterol and amino acid content measure according to standard GB/T5009.44-2003, GB/T5009.17-2003, NY5039-2001, GB/T5009.116-2003, GB/T5009.9-2003, GB/T5009.122003.
The beneficial effect that the present invention has is:
(1) it contains abundant potassium (k), calcium (Ca), magnesium (Mg) and chromium (Cr), zinc (Zn), selenium (Se) or the like multiple livestock and poultry healthy trace elements with household; (2) it is the high-quality animal and fowl feed addictive of natural plant, it also is respond well functional food, can reduce and substitute part epidemic prevention, medicine (particularly antibiotic) class additive, compare with the antibiotics additive to have and have no side effect, drug residue free, be of value to animal and human's class health;
(3), strengthen immunity, the pure natural of guarantee livestock and poultry and products thereof, organic, nuisanceless for livestock and poultry provide full nutrition;
(4) make the meat softness, egg has more elasticity;
(5) can prevent gastrointestinal damage, flu and leucoderma diarrhoea;
(6) has the bacteria-eliminating efficacy of coliform;
(7) can reduce the inside and outside smell of half animal house, improve environment;
(8) the preparation production technology is fairly simple.
The present invention is used for cowboying, and the butterfat of milk cow increases, more delicious taste; Be used to raise pigs, can significantly reduce the smell of pig, improve feed efficiency, improve meat, strong viscera function.
The specific embodiment
Embodiment 1:
1) charing under 600 ℃ of high temperature of charing outlet temperature with bamboo wood or timber obtains solid product bamboo charcoal; The further condensation of gas that produces obtains liquid bamboo vinegar liquid.
2) the bamboo charcoal is processed into 80 purpose bamboo charcoal powders, dry under field conditions (factors) bamboo charcoal powder, the pH8.5 of bamboo charcoal powder.
3) raw liquid of bamboo vinegar is carried out the way of distillation, remove harmful substances such as bamboo tar, control bamboo wood tar content is 0.8%.Bamboo pyrolkigneous liquid pH2.8.
4) extract the bamboo pyrolkigneous liquid in 2: 100 ratios of quality, absorb with the bamboo charcoal powder, make to stir, be packaged into bag, the promptly resultant weakly alkaline product mix that has about pH7.0 is added in 1.5% ratio with this product and feeds chicken in the feed.
Embodiment 2:
1) charing under 1000 ℃ of high temperature of charing outlet temperature with bamboo wood or timber obtains solid product bamboo charcoal; The further condensation of gas that produces obtains liquid bamboo pyrolkigneous liquid.
2) the bamboo charcoal is processed into 60 purpose bamboo charcoal powders, dry under field conditions (factors) bamboo charcoal powder, the pH9.0 of bamboo charcoal powder.
3) bamboo pyrolkigneous liquid stoste is carried out the way of distillation, remove harmful substances such as bamboo wood tar, control bamboo wood tar content is 0.5%.Bamboo pyrolkigneous liquid pH3.0.
4) extract the bamboo pyrolkigneous liquid in 5: 100 ratios of quality, absorb with the bamboo charcoal powder, make to stir, be packaged into bag, the promptly resultant weakly alkaline product mix that has about pH7.2 is added in 1.5% ratio with this product and feeds chicken in the feed.
For showing effect of the present invention, provide following test data:
1, experimental animal and branch group selection 1 age in days are divided into 3 groups at random from 315 of fryer, and 104 every group, that is: 1. A group-charcoal vinegar compound prescription (); 2. B group-charcoal vinegar compound prescription (two); 3. the prescription (contrast) of C group-certain company.
2, the feeding and management method test is carried out in the herding chicken farm.From on April 16th, 2004---on August 16th, 2004, from brood time.Normal humidity of Artificial Control hen house and temperature.Test chicken group free choice feeding and drinking-water.Regularly prevent epidemic by normal procedure.
3, through the feeding experiment in 4 months skies, situations such as the weightening finish of each group, death see Table 1.
Table 1 April 16 in 2004---on August 16th, 2004 each group situations such as weightening finish, death
| Original/plumage | Death toll/plumage | Existing/plumage | Gross weight/Kg | Total feed/g | |
| The A group | 104 | 55 | 49 | 55.25 | 172.45 |
| The B group | 104 | 54 | 50 | 57.5 | 179.4 |
| The C group | 104 | 61 | 43 | 49.0 | 164.45 |
As shown in Table 1: (1) A organizes the death rate 52.88%, B group 51.9%, C group 58.65%;
(2) counterpoise: A organizes 1.13Kg, and B organizes 1.15Kg, and C organizes 1.14Kg;
The result shows: used the interior smell (stink) of the field stop of raising chickens of charcoal vinegar composite feed additive not have special rank smell, smell relaxes, and control group is special smelly; The sick rate of chicken obviously descends, and the chicken group self is grown fine; The content 7.92mg/100g of VBN, mercury 8.65*10 in the chicken
-4Mg/kg, tetracycline and furazolidone are for detecting, and explanation is the environment-friendly and green product; Crude protein content in the egg improves 8.0%, and cholesterol level descends 5.0%.
Claims (2)
1, a kind of preparation method of natural bamboo charcoal vinegar feed addictive is characterized in that the step of this method is as follows:
1) with bamboo timber 600 ℃～1000 ℃ following charings, obtain solid product bamboo charcoal; The condensation of gas that produces obtains liquid bamboo pyrolkigneous liquid;
2) the bamboo charcoal is processed into the bamboo charcoal powder of 60～100 order particle diameters, dry bamboo charcoal powder under the moist or natural conditions or in the dry kiln, the pH8 of bamboo charcoal powder～10;
3) the bamboo pyrolkigneous liquid carries out refinement treatment, removes bamboo wood tar harmful substance, bamboo pyrolkigneous liquid pH2.6～3.2;
4) in bamboo pyrolkigneous liquid and bamboo charcoal quality (2～5): 100 ratios extract the bamboo pyrolkigneous liquid, absorb with the bamboo charcoal powder, make to stir, and are packaged into bag, promptly resultant weakly alkaline product with pH7.0～7.2.
2, the preparation method of a kind of natural bamboo charcoal vinegar feed addictive according to claim 1 is characterized in that: the bamboo pyrolkigneous liquid makes bamboo wood tar component content＜1% through refinement treatment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100495743A CN100396191C (en) | 2006-02-23 | 2006-02-23 | Method for preparing natural bamboo charcoal vinegar feed addictive |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100495743A CN100396191C (en) | 2006-02-23 | 2006-02-23 | Method for preparing natural bamboo charcoal vinegar feed addictive |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1806660A true CN1806660A (en) | 2006-07-26 |
| CN100396191C CN100396191C (en) | 2008-06-25 |
Family
ID=36838887
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100495743A Expired - Fee Related CN100396191C (en) | 2006-02-23 | 2006-02-23 | Method for preparing natural bamboo charcoal vinegar feed addictive |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100396191C (en) |
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| CN100592873C (en) * | 2008-04-30 | 2010-03-03 | 浙江林学院 | Production process of multi-effect pesticidal preparations |
| WO2011044905A1 (en) * | 2009-10-12 | 2011-04-21 | Blackcarbon A/S | A method for reducing emission of carbonaceous gasses |
| CN102084937A (en) * | 2010-05-24 | 2011-06-08 | 浙江林学院 | Fodder acidulant and application method thereof |
| CN101428057B (en) * | 2008-12-12 | 2011-09-28 | 广东高山动物药业有限公司 | Antimicrobial powder for reinforcing immune, strengthening the body resistance and removing toxicity for livestock and poultry |
| CN102987107A (en) * | 2012-09-29 | 2013-03-27 | 凤台县瑞普农业发展有限公司 | Chick feed |
| CN103005200A (en) * | 2012-12-17 | 2013-04-03 | 凤台县腾元家禽养殖有限公司 | Duck feed containing bamboo charcoal and production method thereof |
| CN103202402A (en) * | 2013-04-08 | 2013-07-17 | 南京农业大学 | Chicken feed capable of lowering blood fat and promoting production property of broiler chickens as well as feed additive |
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| CN1404974A (en) * | 2001-08-13 | 2003-03-26 | 株洲开发区大智新型建筑材料研究所 | Method for obtaining high-temp. bamboo charcoal and fine bamboo-wax from bamboo material |
| CN1397534A (en) * | 2002-08-17 | 2003-02-19 | 浙江林学院 | Process for purifying raw liquid of bamboo vinegar |
| CN1590528A (en) * | 2003-08-29 | 2005-03-09 | 郭伟光 | Multieffect microbiological active liquid and its production technology |
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| KR20040074667A (en) * | 2004-08-04 | 2004-08-25 | 채민지 | Feed additive containing bamboo vinegar |
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| CN105309782A (en) * | 2015-10-21 | 2016-02-10 | 滁州红琊山养殖有限公司 | Orange-flavor pig feed flavoring agent |
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| CN105309804A (en) * | 2015-10-21 | 2016-02-10 | 滁州红琊山养殖有限公司 | Flavoring agent for improving flavor of pork pig feed |
| CN105309805A (en) * | 2015-10-21 | 2016-02-10 | 滁州红琊山养殖有限公司 | Pig feed flavoring agent increasing feed intake |
| CN105309800A (en) * | 2015-10-21 | 2016-02-10 | 滁州红琊山养殖有限公司 | Flavoring agent for improving favor of stress pig feed |
| CN105309798A (en) * | 2015-10-21 | 2016-02-10 | 滁州红琊山养殖有限公司 | Flavoring agent for frankincense pig feed |
| CN105309797A (en) * | 2015-10-21 | 2016-02-10 | 滁州红琊山养殖有限公司 | Anti-disease pig feed flavoring agent |
| CN105309802A (en) * | 2015-10-21 | 2016-02-10 | 滁州红琊山养殖有限公司 | Pig feed flavoring agent with cereal flavor |
| CN106173255A (en) * | 2016-08-05 | 2016-12-07 | 商丘三利新能源有限公司淮北分公司 | Antibiotic-free feed |
| CN109384526A (en) * | 2017-08-08 | 2019-02-26 | 林振衡 | A kind of farming and animal husbandry is to pollute the environmental protection round-robin method of pollution treatment dye |
| CN107889944A (en) * | 2017-10-31 | 2018-04-10 | 合肥申仁养殖有限公司 | One kind enhancing pork pig is immune to make every effort to promote digestion feed |
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