CN1751721A - Traditional Chinese medicine soft capsule for ventilating regulating lung, and its prepn. method - Google Patents
Traditional Chinese medicine soft capsule for ventilating regulating lung, and its prepn. method Download PDFInfo
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- CN1751721A CN1751721A CN 200510006974 CN200510006974A CN1751721A CN 1751721 A CN1751721 A CN 1751721A CN 200510006974 CN200510006974 CN 200510006974 CN 200510006974 A CN200510006974 A CN 200510006974A CN 1751721 A CN1751721 A CN 1751721A
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Abstract
A Chinese medicine in the form of soft capsule for ventilating and regulating lung is composed of the core prepared from 11 Chinese-medicinal materials including perilla leaf, peucedanum root, liquorice root, tangerine peel, etc, deluent, suspending aid, and antioxidizing agent, and the shell prepared from gelatin, glycerin, water and antiseptic agent. Its preparing process is also disclosed.
Description
Technical field
What the present invention relates to is a kind of Chinese patent medicine and preparation method thereof, referring in particular to a kind of is the Chinese medicinal soft capsule and preparation method thereof of a kind of Tongxuanlifei of raw material with Chinese herbal medicine Folium Perillae, Radix Peucedani, Radix Platycodonis, Semen Armeniacae Amarum, Herba Ephedrae, Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, Rhizoma Pinelliae (processed), Poria, Fructus Aurantii (parched), Radix Scutellariae, and its medicine is called the Tongxuanlifei soft capsule.
Background technology
This prescription is by Folium Perillae, Radix Peucedani, and Radix Platycodonis, Semen Armeniacae Amarum, Herba Ephedrae, Radix Glycyrrhizae, Pericarpium Citri Reticulatae, Rhizoma Pinelliae (processed), Poria, Fructus Aurantii (parched), Radix Scutellariae ten Chinese medicine are simply formed, and former dosage form tongxuan lifei pills comes from " the 588th page of Chinese pharmacopoeia nineteen ninety-five version; The 210th page of " new drug kind " version in 1992.The Tongxuanlifei oral liquid is used to eliminate cold cough, fever with chills, and the nasal obstruction watery nasal discharge, it is lossless to have a headache, symptoms such as limb aching pain; The tool cold expelling that induces sweat, the effect of lung qi dispersing antitussive; Have antibiotic, antiviral, analgesic, analgesia, antiinflammatory is alleviated lung and bronchospasm, antitussive is eliminated the phlegm and antiasthmatic effect.
Summary of the invention
The object of the present invention is to provide a kind of is the Chinese medicinal soft capsule of a kind of Tongxuanlifei of raw material for 96 parts with 144 parts of Chinese herbal medicine Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae.
It is the preparation method of Chinese medicinal soft capsule of a kind of Tongxuanlifei of Chinese medicine of raw material with Chinese herbal medicine Folium Perillae, Radix Peucedani, Radix Platycodonis, Semen Armeniacae Amarum, Herba Ephedrae, Radix Glycyrrhizae, Pericarpium Citri Reticulatae, Rhizoma Pinelliae (processed), Poria, Fructus Aurantii (parched), Radix Scutellariae that another object of the present invention provides a kind of.
The present invention is implemented by following scheme.
The Chinese medicinal soft capsule of a kind of Chinese medicine Tongxuanlifei of the present invention, comprise capsule liquid, softgel shell, capsule liquid by effective medicinal component (by weight) get 144 parts of Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae more than 96 parts ten simply, Folium Perillae extracts volatile oil, and the aqueous solution after distillation device is in addition collected; Medicinal residues and other ten flavors water concentration shorten the clear paste that relative density is 1.29-1.31 (80 ℃ of heat is surveyed) into, make granule, made principal agent fine powder effective dose and adjuvant formed after spray added Folium Perillae volatile oil, adjuvant comprises diluent, suspending agent, antioxidant, softgel shell is by 10 parts in gelatin, glycerol 3.0-3.3 part, 9.0 parts in water and antiseptic are formed, and effectively the effective dose of medicinal component is that every ball soft capsule contains extract dry extract 60-360mg.
Described diluent is one or more in the vegetable oil, and suspending agent is oily wax mixture, Cera Flava, and antioxidant is dibenzylatiooluene, and antiseptic is benzyl p-hydroxybenzoate class, propylene glycol.
This prescription each component weight proportion also can for:
Group component (gram/grain)
Principal agent fine powder 0.06-0.36
Gelatin 0.04-0.25
Glycerol 0.012-0.0825
Cera Flava 0.02-0.0412
Pigment 0.00002-0.00004
Antioxidant 0.0005-0.001
Antiseptic 0.00003-0.00007
The preparation method of the Chinese medicinal soft capsule of Chinese medicine Tongxuanlifei of the present invention, it mainly comprises following process steps:
(1) get 144 parts of Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae more than 96 parts ten simply, Folium Perillae extracts volatile oil, and the aqueous solution after distillation device is in addition collected;
(2) medicinal residues and other ten flavors water extraction secondary, each two hours, complete also extracting solution, filter, filtrate was left standstill 6-8 hour, and the aqueous solution after getting supernatant and distilling merges, and it is the clear paste of 1.29-1.31 (80 ℃ of heat are surveyed) that reconcentration becomes relative density, make granule, the crushed face fine powder was stand-by after spray added Folium Perillae volatile oil;
(3) gelatin, the dissolving of water heating in water bath add glycerol, antiseptic, stir, and are incubated set aside for use after the vacuumize degassing;
(4) suspending agent is added in the vegetable oil, take by weighing extract principal agent fine powder and mix with the vegetable oil that adds suspending agent, add antioxidant behind the mixing again, stir, room temperature leaves standstill;
(5) medicinal liquid for preparing moves into rolling capsule machine or drips in the system machine, makes soft capsule.
Water bath heating temperature in step (2) can be 85 ℃-95 ℃, and the best is 90 ℃.
Holding temperature in step (2) can be 60 ℃-80 ℃, and the best is 70 ℃.
The Chinese medicinal soft capsule convenient drug administration of Chinese medicine Tongxuanlifei of the present invention, rapid-action, the bioavailability height, the suspension of suspending agent Cera Flava, good stability, side effect are little.Its preparation method technology is simple, is easy to control, constant product quality, no hazard residue.
The specific embodiment
The present invention is further illustrated below in conjunction with embodiment, and following each embodiment only is used to illustrate the present invention, but to not restriction of the present invention.
Embodiment one
Get 144 parts of Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae more than 96 parts ten simply, Folium Perillae extracts volatile oil, and the aqueous solution after distillation device is in addition collected; Medicinal residues and other ten flavors water extraction secondary, each two hours, complete also extracting solution, filter, filtrate was left standstill 6-8 hour, and the aqueous solution after getting supernatant and distilling merges, and it is the clear paste of 1.29-1.31 (80 ℃ of heat are surveyed) that reconcentration becomes relative density, make granule, be ground into fine powder after spray adds Folium Perillae volatile oil.Take by weighing aforesaid principal agent fine powder 600g, PEG4003000g, propylene glycol 1000g, gelatin 2000g, glycerol 800g, pigment 0.3g, dibenzylatiooluene 60g, p-Hydroxybenzoate 0.5g, Cera Flava 200g.Gelatin, water are heated to 90 ℃ of water-bath dissolvings, add glycerol, p-Hydroxybenzoate and pigment, stir, 70 ℃ of insulation set aside for use after the vacuumize degassing; The suspending agent Cera Flava is added in PEG400, the mixed with propylene glycol liquid, with principal agent fine powder 600g and the PEG400, the mixed with propylene glycol that add suspending agent, add dibenzylatiooluene behind the mixing again, stir, room temperature leaves standstill; At last medicinal liquid is moved in the rolling capsule machine, make 10000 soft capsules.
Embodiment 2
Get 144 parts of Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae more than 96 parts ten simply, Folium Perillae extracts volatile oil, and the aqueous solution after distillation device is in addition collected; Medicinal residues and other ten flavors water extraction secondary, each two hours, complete also extracting solution, filter, filtrate was left standstill 6-8 hour, and the aqueous solution after getting supernatant and distilling merges, and it is the clear paste of 1.29-1.31 (80 ℃ of heat are surveyed) that reconcentration becomes relative density, make granule, be ground into fine powder after spray adds Folium Perillae volatile oil.Take by weighing aforesaid principal agent fine powder 900g, Oleum Arachidis hypogaeae semen 3500g, propylene glycol 500g, gelatin 1500g, glycerol 500g, pigment 0.3g, hydroxypropyl cellulose 60g, benzyl p-hydroxybenzoate 0.5g, Cera Flava 200g.Gelatin, water are heated to 85 ℃ of water-bath dissolvings, add glycerol, benzyl p-hydroxybenzoate, stir, 60 ℃ of insulation set aside for use after the vacuumize degassing; The suspending agent Cera Flava is added in Oleum Arachidis hypogaeae semen, the mixed with propylene glycol liquid, with principal agent fine powder 900g and the Oleum Arachidis hypogaeae semen, the mixed with propylene glycol that add suspending agent, add hydroxypropyl cellulose and pigment behind the mixing again, stir, room temperature leaves standstill; At last medicinal liquid is moved into and drip in system machine or the rolling capsule machine, make 10000 soft capsules.
Embodiment 3
Get 144 parts of Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae more than 96 parts ten simply, Folium Perillae extracts volatile oil, and the aqueous solution after distillation device is in addition collected; Medicinal residues and other ten flavors water extraction secondary, each two hours, complete also extracting solution, filter, filtrate was left standstill 6-8 hour, and the aqueous solution after getting supernatant and distilling merges, and it is the clear paste of 1.29-1.31 (80 ℃ of heat are surveyed) that reconcentration becomes relative density, make granule, be ground into fine powder after spray adds Folium Perillae volatile oil.Take by weighing aforesaid principal agent fine powder 600g, Oleum Glycines 1000g, gelatin 500g, glycerol 150g, pigment 0.4g, ethyl hydroxypropyl cellulose 50g, benzyl p-hydroxybenzoate 0.5g, Cera Flava 200g.Gelatin, water are heated to 85 ℃ of water-bath dissolvings, add glycerol, benzyl p-hydroxybenzoate, stir, 60 ℃ of insulation set aside for use after the vacuumize degassing; The suspending agent Cera Flava is added in Oleum Arachidis hypogaeae semen, the mixed with propylene glycol liquid, with principal agent fine powder 900g and the Oleum Arachidis hypogaeae semen, the mixed with propylene glycol that add suspending agent, add hydroxypropyl cellulose and pigment behind the mixing again, stir, room temperature leaves standstill; At last medicinal liquid is moved into and drip in system machine or the rolling capsule machine, make soft capsule.
Embodiment 4
Get 144 parts of Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae more than 96 parts ten simply, Folium Perillae extracts volatile oil, and the aqueous solution after distillation device is in addition collected; Medicinal residues and other ten flavors water extraction secondary, each two hours, complete also extracting solution, filter, filtrate was left standstill 6-8 hour, and the aqueous solution after getting supernatant and distilling merges, and it is the clear paste of 1.29-1.31 (80 ℃ of heat are surveyed) that reconcentration becomes relative density, make granule, be ground into fine powder after spray adds Folium Perillae volatile oil.Take by weighing aforesaid principal agent fine powder 3600g, PEG400 3600g, gelatin 2500g, glycerol 825g, pigment 0.4g, hydroxypropyl cellulose 10g, p-Hydroxybenzoate 0.7g, Cera Flava 400g.Gelatin, water are heated to 95 ℃ of water-bath dissolvings, add glycerol, p-Hydroxybenzoate, stir, 80 ℃ of insulation set aside for use after the vacuumize degassing; The suspending agent Cera Flava is added among the PEG400, principal agent fine powder 3600g is mixed with the PEG400 that adds suspending agent, add hydroxypropyl cellulose and pigment behind the mixing again, stir, room temperature leaves standstill; At last medicinal liquid is moved in the rolling capsule machine, make soft capsule.
Embodiment 5
Get 144 parts of Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae more than 96 parts ten simply, Folium Perillae extracts volatile oil, and the aqueous solution after distillation device is in addition collected; Medicinal residues and other ten flavors water extraction secondary, each two hours, complete also extracting solution, filter, filtrate was left standstill 6-8 hour, and the aqueous solution after getting supernatant and distilling merges, and it is the clear paste of 1.29-1.31 (80 ℃ of heat are surveyed) that reconcentration becomes relative density, make granule, be ground into fine powder after spray adds Folium Perillae volatile oil.Take by weighing aforesaid principal agent fine powder 1000g, Oleum Arachidis hypogaeae semen 3000g, propylene glycol 500g, gelatin 1500g, glycerol 525g, pigment 0.3g, hydroxypropyl cellulose 60g, benzyl p-hydroxybenzoate 0.5g, oily wax mixture 200g.Gelatin: glycerol: water is in 1: 0.33: 0.90 putting of the ratio glue bucket, and 90 ℃ of heating in water bath dissolvings add benzyl p-hydroxybenzoate and pigment, stirs 65 ℃ of insulation set aside for use after the vacuumize degassing; Suspending agent oil wax mixture is added in Oleum Arachidis hypogaeae semen, the mixed with propylene glycol liquid, with principal agent fine powder 1000g and the Oleum Arachidis hypogaeae semen, the mixed with propylene glycol that add suspending agent, add hydroxypropyl cellulose behind the mixing more again, stir, standing over night makes its dissolving, and is standby behind the ultrasonic degas.The temperature of regulating SCM-100 type encapsulating machine glue box at last is 50 ℃, and the temperature of sprinkler body is 41 ℃-43 ℃, and the thickness of rubber is at 0.7-0.8mm.Medicinal liquid is poured in the medicinal liquid bucket, be pressed into soft capsule with mould.
The soft gelatin capsule of compacting cleans with ultrasound wave soft capsule cleaning machine, the full-automatic dry machine drying of crawler type, and the qualified back packing of quality testing, labeling, packing promptly get Tongxuanlifei soft capsule finished product, automatically cover blister package machine packing.
Claims (6)
1. the Chinese medicinal soft capsule of a Tongxuanlifei, comprise capsule liquid, softgel shell, capsule liquid by effective medicinal component (by weight) get 144 parts of Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae more than 96 parts ten simply, Folium Perillae extracts volatile oil, and the aqueous solution after distillation device is in addition collected; Medicinal residues and other ten flavors water concentration shorten the clear paste that relative density is 1.29-1.31 (80 ℃ of heat is surveyed) into, make granule, made principal agent fine powder effective dose and adjuvant formed after spray added Folium Perillae volatile oil, it is characterized in that: adjuvant comprises diluent, antioxidant, suspending agent, softgel shell is by 10 parts in gelatin, glycerol 3.0-3.3 part, 9.0 parts in water and antiseptic are formed, and effectively the effective dose of medicinal component is that every ball soft capsule contains extract dry extract 60-360mg.
2. the Chinese medicinal soft capsule of a kind of Tongxuanlifei as claimed in claim 1, it is characterized in that: described diluent is one or more in the vegetable oil, suspending agent is oily wax mixture, Cera Flava, and antioxidant is dibenzylatiooluene, and antiseptic is benzyl p-hydroxybenzoate class, propylene glycol.
3. the Chinese medicinal soft capsule of a kind of Tongxuanlifei as claimed in claim 2 is characterized in that the weight proportion of each component is:
Group component (gram/grain)
Principal agent fine powder 0.06-0.36
Gelatin 0.04-0.25
Glycerol 0.012-0.0825
Cera Flava 0.02-0.04
Pigment 0.00002-0.00004
Antioxidant 0.0005-0.001
Antiseptic 0.00003-0.00007.
4. the preparation method of the Chinese medicinal soft capsule of a kind of Tongxuanlifei as claimed in claim 1 is characterized in that it comprises following process steps:
(1) get 144 parts of Folium Perillaes, 96 parts of Radix Peucedanis, 96 parts of Radix Platycodoniss, 72 parts of Semen Armeniacae Amarums, 96 parts in Herba Ephedrae, 72 parts in Radix Glycyrrhizae, 96 parts of Pericarpium Citri Reticulataes, 72 parts of Rhizoma Pinelliae (processed), 96 parts in Poria, 96 parts of Fructus Aurantii (parched), Radix Scutellariae more than 96 parts ten simply, Folium Perillae extracts volatile oil, and the aqueous solution after distillation device is in addition collected;
(2) medicinal residues and other ten flavors water extraction secondary, each two hours, complete also extracting solution, filter, filtrate was left standstill 6-8 hour, and the aqueous solution after getting supernatant and distilling merges, and it is the clear paste of 1.29-1.31 (80 ℃ of heat are surveyed) that reconcentration becomes relative density, make granule, spray adds that to be ground into fine powder behind the Folium Perillae volatile oil stand-by;
(3) gelatin, the dissolving of water heating in water bath add glycerol, antiseptic, stir, and are incubated set aside for use after the vacuumize degassing;
(4) suspending agent is added in the vegetable oil, take by weighing extract principal agent fine powder and mix with the vegetable oil that adds suspending agent, add antioxidant behind the mixing again, stir, room temperature leaves standstill;
(5) medicinal liquid for preparing moves into rolling capsule machine or drips in the system machine, makes soft capsule.
5. the preparation method of the Chinese medicinal soft capsule of a kind of Tongxuanlifei as claimed in claim 4, it is characterized in that: the water bath heating temperature in the step (2) is 85 ℃-95 ℃; Holding temperature is 60 ℃-80 ℃.
6. the preparation method of the Chinese medicinal soft capsule of a kind of Tongxuanlifei as claimed in claim 5, it is characterized in that: the water bath heating temperature in the step (2) is 90 ℃; Holding temperature is 70 ℃.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200510006974 CN1751721A (en) | 2005-01-14 | 2005-01-14 | Traditional Chinese medicine soft capsule for ventilating regulating lung, and its prepn. method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200510006974 CN1751721A (en) | 2005-01-14 | 2005-01-14 | Traditional Chinese medicine soft capsule for ventilating regulating lung, and its prepn. method |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104013755A (en) * | 2014-05-28 | 2014-09-03 | 王庚禹 | Extract product for preparation of lung ventilating and regulating preparation |
| CN106266851A (en) * | 2015-06-02 | 2017-01-04 | 北京海吉星医疗科技有限公司 | A kind of chewable tablet of Chinese medicine composition |
| CN106310059A (en) * | 2015-06-30 | 2017-01-11 | 北京海吉星医疗科技有限公司 | Effervescent tablet of traditional Chinese medicine composition |
| CN114224960A (en) * | 2021-12-31 | 2022-03-25 | 哈尔滨瀚钧现代制药有限公司 | Lung-ventilating and regulating granule and preparation process thereof |
| CN116570668A (en) * | 2023-06-27 | 2023-08-11 | 重庆希尔安药业有限公司 | Lung-ventilating and regulating granule and preparation method thereof |
-
2005
- 2005-01-14 CN CN 200510006974 patent/CN1751721A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104013755A (en) * | 2014-05-28 | 2014-09-03 | 王庚禹 | Extract product for preparation of lung ventilating and regulating preparation |
| CN106266851A (en) * | 2015-06-02 | 2017-01-04 | 北京海吉星医疗科技有限公司 | A kind of chewable tablet of Chinese medicine composition |
| CN106310059A (en) * | 2015-06-30 | 2017-01-11 | 北京海吉星医疗科技有限公司 | Effervescent tablet of traditional Chinese medicine composition |
| CN114224960A (en) * | 2021-12-31 | 2022-03-25 | 哈尔滨瀚钧现代制药有限公司 | Lung-ventilating and regulating granule and preparation process thereof |
| CN116570668A (en) * | 2023-06-27 | 2023-08-11 | 重庆希尔安药业有限公司 | Lung-ventilating and regulating granule and preparation method thereof |
| CN116570668B (en) * | 2023-06-27 | 2023-11-24 | 重庆希尔安药业有限公司 | Lung-ventilating and regulating granule and preparation method thereof |
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