CN1742583A - 一种复合纳米抗菌材料及其制备方法 - Google Patents
一种复合纳米抗菌材料及其制备方法 Download PDFInfo
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- CN1742583A CN1742583A CN 200510094497 CN200510094497A CN1742583A CN 1742583 A CN1742583 A CN 1742583A CN 200510094497 CN200510094497 CN 200510094497 CN 200510094497 A CN200510094497 A CN 200510094497A CN 1742583 A CN1742583 A CN 1742583A
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- 239000000463 material Substances 0.000 title claims abstract description 117
- 239000002131 composite material Substances 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 230000003115 biocidal effect Effects 0.000 title claims description 115
- 239000003242 anti bacterial agent Substances 0.000 title claims description 106
- 229940088710 antibiotic agent Drugs 0.000 title claims description 106
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 67
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 29
- 239000002086 nanomaterial Substances 0.000 claims abstract description 5
- 239000010949 copper Substances 0.000 claims description 41
- 229910052802 copper Inorganic materials 0.000 claims description 41
- 239000000047 product Substances 0.000 claims description 38
- 238000003756 stirring Methods 0.000 claims description 28
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 21
- 239000011268 mixed slurry Substances 0.000 claims description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 14
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 14
- 239000012065 filter cake Substances 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 11
- 239000002270 dispersing agent Substances 0.000 claims description 9
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 7
- XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical class [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 7
- 229910001961 silver nitrate Inorganic materials 0.000 claims description 7
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical class [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 7
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 7
- ONDPHDOFVYQSGI-UHFFFAOYSA-N zinc nitrate Chemical class [Zn+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ONDPHDOFVYQSGI-UHFFFAOYSA-N 0.000 claims description 7
- ZXAUZSQITFJWPS-UHFFFAOYSA-J zirconium(4+);disulfate Chemical compound [Zr+4].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O ZXAUZSQITFJWPS-UHFFFAOYSA-J 0.000 claims description 7
- LEHFSLREWWMLPU-UHFFFAOYSA-B zirconium(4+);tetraphosphate Chemical compound [Zr+4].[Zr+4].[Zr+4].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LEHFSLREWWMLPU-UHFFFAOYSA-B 0.000 claims description 5
- 239000002002 slurry Substances 0.000 claims description 4
- 229910052588 hydroxylapatite Inorganic materials 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 claims description 2
- 229910000166 zirconium phosphate Inorganic materials 0.000 claims description 2
- 230000000845 anti-microbial effect Effects 0.000 abstract 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 abstract 2
- NEIHULKJZQTQKJ-UHFFFAOYSA-N [Cu].[Ag] Chemical compound [Cu].[Ag] NEIHULKJZQTQKJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000008187 granular material Substances 0.000 abstract 1
- 239000011787 zinc oxide Substances 0.000 abstract 1
- 201000010099 disease Diseases 0.000 description 17
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 17
- 239000003814 drug Substances 0.000 description 14
- 239000000243 solution Substances 0.000 description 14
- 239000002245 particle Substances 0.000 description 5
- 238000002347 injection Methods 0.000 description 4
- 239000007924 injection Substances 0.000 description 4
- 229940079593 drug Drugs 0.000 description 3
- 230000002147 killing effect Effects 0.000 description 3
- 208000030507 AIDS Diseases 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000002114 nanocomposite Substances 0.000 description 2
- 210000001640 nerve ending Anatomy 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 238000001050 pharmacotherapy Methods 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- 208000004926 Bacterial Vaginosis Diseases 0.000 description 1
- 241000222122 Candida albicans Species 0.000 description 1
- 206010007134 Candida infections Diseases 0.000 description 1
- 241000606161 Chlamydia Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 1
- 206010018612 Gonorrhoea Diseases 0.000 description 1
- 206010018693 Granuloma inguinale Diseases 0.000 description 1
- 208000001688 Herpes Genitalis Diseases 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 241000204031 Mycoplasma Species 0.000 description 1
- 241000588653 Neisseria Species 0.000 description 1
- 208000019802 Sexually transmitted disease Diseases 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 241000589884 Treponema pallidum Species 0.000 description 1
- 208000005448 Trichomonas Infections Diseases 0.000 description 1
- 206010044620 Trichomoniasis Diseases 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 201000003984 candidiasis Diseases 0.000 description 1
- 229960004755 ceftriaxone Drugs 0.000 description 1
- VAAUVRVFOQPIGI-SPQHTLEESA-N ceftriaxone Chemical compound S([C@@H]1[C@@H](C(N1C=1C(O)=O)=O)NC(=O)\C(=N/OC)C=2N=C(N)SC=2)CC=1CSC1=NC(=O)C(=O)NN1C VAAUVRVFOQPIGI-SPQHTLEESA-N 0.000 description 1
- 201000004308 chancroid Diseases 0.000 description 1
- 229910001431 copper ion Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001827 electrotherapy Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 201000004946 genital herpes Diseases 0.000 description 1
- 210000004392 genitalia Anatomy 0.000 description 1
- 208000020426 gonococcal urethritis Diseases 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 208000001581 lymphogranuloma venereum Diseases 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 231100000017 mucous membrane irritation Toxicity 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 210000002445 nipple Anatomy 0.000 description 1
- 231100001083 no cytotoxicity Toxicity 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- OAEYYFGETMINBA-UHFFFAOYSA-N phosphoric acid;propanoic acid;propan-2-ol Chemical compound CC(C)O.CCC(O)=O.OP(O)(O)=O OAEYYFGETMINBA-UHFFFAOYSA-N 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 229960000268 spectinomycin Drugs 0.000 description 1
- UNFWWIHTNXNPBV-WXKVUWSESA-N spectinomycin Chemical compound O([C@@H]1[C@@H](NC)[C@@H](O)[C@H]([C@@H]([C@H]1O1)O)NC)[C@]2(O)[C@H]1O[C@H](C)CC2=O UNFWWIHTNXNPBV-WXKVUWSESA-N 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000007920 subcutaneous administration Methods 0.000 description 1
- 230000000153 supplemental effect Effects 0.000 description 1
- 208000011580 syndromic disease Diseases 0.000 description 1
- 208000006379 syphilis Diseases 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 210000003905 vulva Anatomy 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
Claims (8)
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CNB2005100944979A CN100361583C (zh) | 2005-09-23 | 2005-09-23 | 一种复合纳米抗菌材料及其制备方法 |
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CNB2005100944979A CN100361583C (zh) | 2005-09-23 | 2005-09-23 | 一种复合纳米抗菌材料及其制备方法 |
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CN1742583A true CN1742583A (zh) | 2006-03-08 |
CN100361583C CN100361583C (zh) | 2008-01-16 |
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CNB2005100944979A Expired - Fee Related CN100361583C (zh) | 2005-09-23 | 2005-09-23 | 一种复合纳米抗菌材料及其制备方法 |
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Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101402844B (zh) * | 2008-03-14 | 2013-04-03 | 东莞拓扑实业有限公司 | 防紫外、抗菌纳米功能粉体及其制备方法 |
CN103044611A (zh) * | 2012-12-17 | 2013-04-17 | 上海师范大学 | 含有卤胺官能团的聚合物抗菌纳米粒子和磁性抗菌纳米粒子的制备 |
CN103668978A (zh) * | 2013-11-27 | 2014-03-26 | 江苏中新资源集团有限公司 | 一种织物抗菌整理剂及其制备方法 |
CN104170820A (zh) * | 2013-05-22 | 2014-12-03 | 上海奇维纺织科技有限公司 | 一种含纳米锌保护银离子无机抗菌粉体及制备方法 |
TWI511919B (zh) * | 2013-05-08 | 2015-12-11 | ||
CN105780473A (zh) * | 2014-12-22 | 2016-07-20 | 常熟市虹桥印染有限公司 | 织物抗菌整理剂 |
CN106106522A (zh) * | 2016-06-23 | 2016-11-16 | 中国人民解放军军事医学科学院卫生学环境医学研究所 | 一种纳米氧化锌‑载银壳聚糖复合抗菌剂及其制备方法 |
CN107529715A (zh) * | 2015-04-17 | 2018-01-02 | 住友化学株式会社 | 包衣水稻种子及其制备方法 |
CN108271808A (zh) * | 2018-02-01 | 2018-07-13 | 叶剑 | 一种抗菌纳米材料的制备方法 |
CN108867049A (zh) * | 2018-06-27 | 2018-11-23 | 苏州市贝克生物科技有限公司 | 壳聚糖抗菌材料及其制备方法 |
CN110306345A (zh) * | 2019-05-29 | 2019-10-08 | 安徽元和工贸有限责任公司 | 一种医用抗菌棉纱布的制备方法 |
CN111466408A (zh) * | 2020-04-14 | 2020-07-31 | 安徽万兴实业有限公司 | 抗菌材料的制备方法、抗菌纳米纤维布制造方法及应用 |
CN111838183A (zh) * | 2020-08-12 | 2020-10-30 | 高时(厦门)石业有限公司 | 复合金属胶体无机抗菌剂及其制备方法、及其无机人造石 |
CN111996083A (zh) * | 2020-08-10 | 2020-11-27 | 上海大学 | 一种用于织物抗菌抗病毒的洗涤剂及其制备方法 |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6835381B2 (ja) * | 2018-05-25 | 2021-02-24 | Dr.C医薬株式会社 | 害虫発生抑制方法 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0687714A (ja) * | 1992-09-09 | 1994-03-29 | Sangi Co Ltd | 抗菌性セラミックス |
CN1383723A (zh) * | 2002-04-29 | 2002-12-11 | 兴国纳米科技实业有限公司 | 纳米抗菌粉体及其制备工艺 |
CN100525629C (zh) * | 2002-06-12 | 2009-08-12 | 骆天荣 | 纳米无机抗菌剂及其制备方法 |
CN1253086C (zh) * | 2004-02-27 | 2006-04-26 | 中国皮革和制鞋工业研究院 | 一种用于抗菌除臭防霉的活性炭制剂的制备方法 |
-
2005
- 2005-09-23 CN CNB2005100944979A patent/CN100361583C/zh not_active Expired - Fee Related
Cited By (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101402844B (zh) * | 2008-03-14 | 2013-04-03 | 东莞拓扑实业有限公司 | 防紫外、抗菌纳米功能粉体及其制备方法 |
CN103044611A (zh) * | 2012-12-17 | 2013-04-17 | 上海师范大学 | 含有卤胺官能团的聚合物抗菌纳米粒子和磁性抗菌纳米粒子的制备 |
CN103044611B (zh) * | 2012-12-17 | 2015-06-10 | 上海师范大学 | 含有卤胺官能团的聚合物抗菌纳米粒子和磁性抗菌纳米粒子的制备 |
TWI511919B (zh) * | 2013-05-08 | 2015-12-11 | ||
CN104170820A (zh) * | 2013-05-22 | 2014-12-03 | 上海奇维纺织科技有限公司 | 一种含纳米锌保护银离子无机抗菌粉体及制备方法 |
CN103668978A (zh) * | 2013-11-27 | 2014-03-26 | 江苏中新资源集团有限公司 | 一种织物抗菌整理剂及其制备方法 |
CN103668978B (zh) * | 2013-11-27 | 2015-12-30 | 江苏中新资源集团有限公司 | 一种织物抗菌整理剂及其制备方法 |
CN105780473A (zh) * | 2014-12-22 | 2016-07-20 | 常熟市虹桥印染有限公司 | 织物抗菌整理剂 |
CN107529715A (zh) * | 2015-04-17 | 2018-01-02 | 住友化学株式会社 | 包衣水稻种子及其制备方法 |
CN106106522A (zh) * | 2016-06-23 | 2016-11-16 | 中国人民解放军军事医学科学院卫生学环境医学研究所 | 一种纳米氧化锌‑载银壳聚糖复合抗菌剂及其制备方法 |
CN106106522B (zh) * | 2016-06-23 | 2019-05-14 | 中国人民解放军军事医学科学院卫生学环境医学研究所 | 一种纳米氧化锌-载银壳聚糖复合抗菌剂及其制备方法 |
CN108271808A (zh) * | 2018-02-01 | 2018-07-13 | 叶剑 | 一种抗菌纳米材料的制备方法 |
CN108867049A (zh) * | 2018-06-27 | 2018-11-23 | 苏州市贝克生物科技有限公司 | 壳聚糖抗菌材料及其制备方法 |
CN110306345A (zh) * | 2019-05-29 | 2019-10-08 | 安徽元和工贸有限责任公司 | 一种医用抗菌棉纱布的制备方法 |
CN110306345B (zh) * | 2019-05-29 | 2022-07-08 | 青岛中腾生物技术有限公司 | 一种医用抗菌棉纱布的制备方法 |
CN111466408A (zh) * | 2020-04-14 | 2020-07-31 | 安徽万兴实业有限公司 | 抗菌材料的制备方法、抗菌纳米纤维布制造方法及应用 |
CN111996083A (zh) * | 2020-08-10 | 2020-11-27 | 上海大学 | 一种用于织物抗菌抗病毒的洗涤剂及其制备方法 |
CN111838183A (zh) * | 2020-08-12 | 2020-10-30 | 高时(厦门)石业有限公司 | 复合金属胶体无机抗菌剂及其制备方法、及其无机人造石 |
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