CN1640488A - Method for preparing supermicro powder preparation of cordyceps sinensis mycelium - Google Patents
Method for preparing supermicro powder preparation of cordyceps sinensis mycelium Download PDFInfo
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Abstract
The present invention relates to a preparation method of caterpillar fungus mycelium ultramicropowder preparation. Said preparation method includes the following steps: making the separated caterpillar fungus strain undergo the processes of slant cultivation, shake cultivation, fermentor cultivation, filtration, drying, ultralow temperature vacuum drying and ultramicro wall-breaking pulverization to obtain caterpillar fungus ultramicropowder, then adding two or three or four kinds of 0.5-4 % of yeast ertract, 1-20% of medical dextrin, 0.5-3% of panaquilon, 10-20% of American ginseng micropowder, 15-30% of ganoderma micropowder and other components in 70-98.5% of caterpillar fungus ultramicropowder, mixing them, drying so as to obtain its powder or tablet or capsule preparation.
Description
Affiliated technical field: the invention belongs to the preparation field of functional health-care food, specifically is a kind of preparation method of Cordyceps mycelium micropowders preparation.
Background technology: along with the raising day by day of people's living standard, the continuous quickening of social activity frequency, successful personage of various circles of society and vast young and middle-aged worker load and further strengthen, middle-aged and elderly people and part children are badly in need of improving and health invigorating, and develop senior natural nutrition health food becomes a urgency key areas leaved for development for this reason.
Cordyceps is the strengthening by means of tonics rare Chinese medicine that there is long medicinal history in China; modern age, the pharmacology medicineization studies show that it contained 18 necessary seed amino acids of adenosine, mannitol and human body and is rich in multiple beneficial in healthy trace element, have blood fat reducing, prevent and treat arteriosclerosis, blood vessel dilating, protection heart and brain tissues, tranquillizing and allaying excitement, enhancing macrophage, improve immunologic function, suppress the mice ehrlich carcinoma, the good action of antiinflammatory, antibiotic, anoxia enduring.
Radix Panacis Quinquefolii, put down in writing at China's pharmacy in modern age works " Bencao Congxin ": " going out Atlantic Ocean Fo Nanxi, the rough Radix Ginseng in the likeness in form east area of the Liao River, coextensive with eastern and southern Liaoning Province ", so the Western Radix Ginseng of name.Wherein, " producing the star-spangled banner U.S. " person has another name called Radix Panacis Quinquefolii." the medicine output is distinguished " record: Radix Panacis Quinquefolii nature and flavor: bitter, little sweet, cold, GUIXIN, lung, kidney channel, are relieved inflammation or internal heat and are promoted the production of body fluid at boosting qi and nourishing yin.Cure mainly YIN-deficiency of the lung and kidney, deficiency of both QI and YIN, body fluid and lose empty all diseases.Modern study proves: Radix Panacis Quinquefolii contains multiple ginsenoside, ginseng polysaccharide and various trace elements.Main component has analgesia, calmness, analgesic, spasmolysis.Significant resisting fatigue, diuresis, anti-anoxia ability are arranged, can also blood sugar lowering and anti-heart rhythm disorders effect.
Pollen, Shennong's Herbal claim to obey for a long time pollen can " keep fit, QI invigorating prolong life ".Adopt the pollen (processed by breaking wall) of micronizing processing, can improve its bioavailability to greatest extent.
Chinese patent 96113170.5,99114824.X, 03103962.6 have all proposed the compound scheme of utilizing about the Cordyceps superfine powder, and still, Chinese patent 96113170.5 does not provide concrete technological parameter and compositely proportional; Chinese patent 99114824.X is when the Cordyceps micronizing, and temperature is too high, and the consumption of Cordyceps superfine powder is lower, and compound raw material type is less; The consumption of the Cordyceps superfine powder of Chinese patent 03103962.6 is lower.
Summary of the invention: the preparation method that the object of the present invention is to provide a kind of Cordyceps mycelium micropowders preparation, adopt reasonably prescription and technology, to improve the bioavailability and the medicinal health effect of product, improve the dissolution rate of effective ingredient, improve the mouthfeel of product, be beneficial to the health-care effect of enhancing human body.
The objective of the invention is by adopting following technical scheme to realize:
The preparation method of Cordyceps mycelium micropowders preparation of the present invention, be with isolating Cordyceps Paecilomyces hepiali Chinese caterpillar fungus strain under 24～25 ℃, slant culture 5～6 days; Again with the shaking table training method under 24～25 ℃, carry out first order seed and cultivated 5～6 days, secondary seed was cultivated 5～6 days, 24～26 ℃ of following amplification culture 3 days; Cultivated 5～6 days in 24～26 ℃ of bottom fermentation jars then; Centrifugal filtration, filter cake is after below 75 ℃ dry 4～6 hours, be crushed to 60～80 orders, in 55 ℃ of following cold drying 5～6 hours, under-104 ℃, 0.6Mpa, carry out the ultra low temperature vacuum drying again, carry out the ultra micro wall breaking pulverization with the supersonic gas of the 1.92M/min fluidizing fluid-bed jet mill in bottom of flowing through again, make 325～560 orders ,≤the Cordyceps superfine powder of 38um; In 70～98.5% Cordyceps superfine powder, add two or three in the following batching or four kind in proportion: 0.5～4% yeastex, 1～20% medical dextrin, 0.5～3% Radix Panacis Quinquefolii saponin, 10～20% Radix Panacis Quinquefolii micropowder, the ultra micro pollen (processed by breaking wall) of 15～30% Ganoderma micropowder 1～20%, 0.5～3% protein sugar, 1～2% Oleum menthae, 3～5%CMC-Na (sodium carboxymethyl cellulose), 0.5～2% magnesium stearate; Obtain powder or tablet or capsular Cordyceps mycelium micropowders preparation through mixing, drying, component, packing, sterilization.
The present invention carries out purification, rejuvenation, fermentation culture, refinement drying to gather Qinghai-Tibet natural cs through repeated screening, isolating peacilomyce hepiahi Chinese caterpillar fungus strain, and carry out ultra micro respectively with Radix Panacis Quinquefolii or pollen and process, fill a prescription, add auxiliary agents such as flavoring agent, filler, antiseize paste, freshener and be prepared into powder, oral buccal tablet, to obtain good mouthfeel and the health-care effect of Geng Jia.Product is light brown powder shape, sundown special-shaped tablets, has kidney invigorating and YANG supporting, lung benefiting cough-relieving, is applicable to that impotence and seminal emission, spontaneous perspiration frequent micturition, Mental fatigue power lack, and strengthen the resisting fatigue and the resistance against diseases of human body human body.
The preparation method of Cordyceps mycelium micropowders preparation of the present invention, utilization international advanced low-temperature vacuum drying dehydration technique and supersonic airstream crushing technology, Cordyceps mycelium and corresponding prescription major ingredient are carried out wall breaking pulverization, raw material granularity is reached below the 40um, minority reaches below the 10nm, has largest specific surface area and porosity, has improved the bioavailability and the medicinal health effect of product to greatest extent, can strengthen body immunity, improve the human body anti-fatigue effect.
The present invention adopts rational prescription and technology, has improved the bioavailability and the medicinal health effect of product, has improved the dissolution rate of effective ingredient, has improved the mouthfeel of product, is beneficial to the health-care effect of enhancing to human body.
By the powder of the present invention's preparation, meet country about food hygienic standard through component, packing, sterilization, check, it is Powdered that finished product is sundown, inlet exquisiteness, little hardship, raw meat perfume (or spice), delicious.The powder product of this prepared is through checking: total nitrogen is higher than a bit 05 percentage points of like product standard, and total amino acid content exceeds seven percentage points than standard, and the standard fineness is 200 orders, and product fineness reaches more than 320 orders.
By the tablet of the present invention's preparation, add auxiliary agent mixing granulation, drying, tabletting, packing, sterilization, check through raw material micropowder prescription, meet country about edible function Sexual health promotion sanitary standard, finished product is the sundown special-shaped tablets, containing in mouthful, little acid of distinguishing the flavor of has the natural fragrance of Cordyceps.The tablet product of this prepared all meets national standard through checking every sanitary index, and the main component check: adenosine, mannitol, content of ginsenoside all are significantly higher than state specified standards.
The specific embodiment: be described in further detail the present invention below in conjunction with embodiment.
Embodiment one
Will be isolating Cordyceps Paecilomyces hepiali Chinese caterpillar fungus strain under 24～25 ℃, slant culture 5～6 days; Again with the shaking table training method under 24～25 ℃, carry out first order seed and cultivated 5～6 days, secondary seed was cultivated 5～6 days, 24～26 ℃ of following amplification culture 3 days; Cultivated 5～6 days in 24～26 ℃ of bottom fermentation jars then; Centrifugal filtration, filter cake is after below 75 ℃ dry 4～6 hours, be crushed to 60～80 orders, in 55 ℃ of following cold drying 5～6 hours, under-104 ℃, 0.6Mpa, carry out the ultra low temperature vacuum drying again, carry out the ultra micro wall breaking pulverization with the supersonic gas of the 1.92M/min fluidizing fluid-bed jet mill in CBF-250 type bottom of flowing through again, make 325～560 orders ,≤the Cordyceps superfine powder of 38um; The yeastex that adds 0.5 kilogram in 98.5 kilograms of Cordyceps superfine powder, 1 kilogram medical dextrin is made the Cordyceps mycelium micropowders powder through mixing, drying, component, packing, sterilization.Product specification is: 2g, 3g, 6g, 8g, 12g dress, content's index: adenosine 〉=0.15%, mannitol 〉=5%.
Embodiment two
The preparation of Cordyceps superfine powder is with embodiment one; The yeastex that adds 4 kilograms in 76 kilograms of Cordyceps superfine powder, 20 kilograms medical dextrin is made the Cordyceps mycelium micropowders powder through mixing, drying, component, packing, sterilization.Product specification is: 2g, 3g, 6g, 8g, 12g dress, content's index: adenosine 〉=0.15%, mannitol 〉=5%.
Embodiment three
The preparation of Cordyceps superfine powder is with embodiment one; The yeastex that adds 1 kilogram in 89 kilograms of Cordyceps superfine powder, 10 kilograms medical dextrin is made the Cordyceps mycelium micropowders powder through mixing, drying, component, packing, sterilization.Product specification is: 2g, 3g, 6g, 8g, 12g dress, content's index: adenosine 〉=0.15%, mannitol 〉=5%.
Embodiment four
The preparation of Cordyceps superfine powder is with embodiment one; The yeastex that in 92.5 kilograms of Cordyceps superfine powder, adds 2 kilograms, 5 kilograms medical dextrin, 0.5 kilogram protein sugar is made the Cordyceps mycelium micropowders powder through mixing, drying, component, packing, sterilization.Product specification is: 2g, 3g, 6g, 8g, 12g dress, content's index: adenosine 〉=0.15%, mannitol 〉=5%.
Embodiment five
The preparation of Cordyceps superfine powder is with embodiment one; The yeastex that in 97 kilograms of Cordyceps superfine powder, adds 1 kilogram, 1 kilogram medical dextrin, 1 kilogram ultra micro pollen (processed by breaking wall) is made the Cordyceps mycelium micropowders powder through mixing, drying, component, packing, sterilization.Product specification is: 2g, 3g, 6g, 8g, 12g dress, content's index: adenosine 〉=0.15%, mannitol 〉=5%.
Embodiment six
The preparation of Cordyceps superfine powder is with embodiment one; The yeastex that adds 1 kilogram in 98 kilograms of Cordyceps superfine powder, 1 kilogram ultra micro pollen (processed by breaking wall) is made the Cordyceps mycelium micropowders powder through mixing, drying, component, packing, sterilization.Product specification is: 2g, 3g, 6g, 8g, 12g dress, content's index: adenosine 〉=0.15%, mannitol 〉=5%.
Embodiment seven
The preparation of Cordyceps superfine powder is with embodiment one; The medical dextrin that in 97 kilograms of Cordyceps superfine powder, adds 2 kilograms, 0.5 kilogram Radix Panacis Quinquefolii saponin, 0.5 kilogram protein sugar is made the Cordyceps mycelium micropowders powder through mixing, drying, component, packing, sterilization.Product specification is: 2g, 3g, 6g, 8g, 12g dress, content's index: adenosine 〉=0.15%, mannitol 〉=5%.
It is Powdered that embodiment one to embodiment seven prepared Cordyceps mycelium micropowders powder is sundown, inlet exquisiteness, little hardship, raw meat perfume (or spice), delicious, total nitrogen is higher than a bit 05 percentage points of like product standard, total amino acid content exceeds seven percentage points than standard, the standard fineness is 200 orders, and product fineness reaches more than 320 orders.Be called Cordyceps pot, be used to stew chicken, duck, fish, meat, Steamed chicken egg, taste are very bright fragrant, are applicable to that especially sexual impotence, seminal emission, lumbago due to renal deficiency, weak weak person eat.Collection health care, nutrition, color are one, are a kind of rare nourishing, strong medicated diet good merchantable brand.
Embodiment eight
The preparation of Cordyceps superfine powder is with embodiment one; The Radix Panacis Quinquefolii saponin that in 93.5 kilograms of Cordyceps superfine powder, adds 3 kilograms, 3 kilograms CMC-Na, 0.5 kilogram magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g, 0.5g/ sheet, content's index: adenosine 〉=0.45mg/g, mannitol 〉=3%, Radix Panacis Quinquefolii saponin 〉=0.25%.
Embodiment nine
The preparation of Cordyceps superfine powder is with embodiment one; The Radix Panacis Quinquefolii saponin that in 92.5 kilograms of Cordyceps superfine powder, adds 0.5 kilogram, 5 kilograms CMC-Na, 2 kilograms magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g, 0.5g/ sheet, content's index: adenosine 〉=0.45mg/g, mannitol 〉=3%, Radix Panacis Quinquefolii saponin 〉=0.25%.
Embodiment ten
The preparation of Cordyceps superfine powder is with embodiment one; The Radix Panacis Quinquefolii micropowder that in 85 kilograms of Cordyceps superfine powder, adds 10 kilograms, 4 kilograms CMC-Na, 1 kilogram magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g, 0.5g/ sheet, content's index: adenosine 〉=0.45mg/g, mannitol 〉=3%, Radix Panacis Quinquefolii saponin 〉=0.25%.
Embodiment 11
The preparation of Cordyceps superfine powder is with embodiment one; The Radix Panacis Quinquefolii micropowder that in 73 kilograms of Cordyceps superfine powder, adds 20 kilograms, 5 kilograms CMC-Na, 2 kilograms magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g, 0.5g/ sheet, content's index: adenosine 〉=0.45mg/g, mannitol 〉=3%, Radix Panacis Quinquefolii saponin 〉=0.25%.
Embodiment 12
The preparation of Cordyceps superfine powder is with embodiment one; The yeastex that in 80 kilograms of Cordyceps superfine powder, adds 0.5 kilogram, 16 kilograms Radix Panacis Quinquefolii micropowder, 3 kilograms CMC-Na, 0.5 kilogram magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g, 0.5g/ sheet, content's index: adenosine 〉=0.45mg/g, mannitol 〉=3%, Radix Panacis Quinquefolii saponin 〉=0.25%.
Embodiment 13
The preparation of Cordyceps superfine powder is with embodiment one; The Radix Panacis Quinquefolii micropowder that in 70 kilograms of Cordyceps superfine powder, adds 20 kilograms, 3 kilograms ultra micro pollen (processed by breaking wall), 5 kilograms CMC-Na, 2 kilograms magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g, 0.5g/ sheet, content's index: adenosine 〉=0.45mg/g, mannitol 〉=3%, Radix Panacis Quinquefolii saponin 〉=0.25%.
Embodiment eight to embodiment 13 prepared Cordyceps mycelium micropowders tablets are the sundown special-shaped tablets, are called Cordyceps Radix Panacis Quinquefolii buccal tablet.
Embodiment 14
The preparation of Cordyceps superfine powder is with embodiment one; The protein sugar that in 97 kilograms of Cordyceps superfine powder, adds 1 kilogram, 1 kilogram Oleum menthae, 1 kilogram magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g/ sheet, 0.5g/ sheet, content's index: adenosine 〉=0.35mg/g, mannitol 〉=2.5%.
Embodiment 15
The preparation of Cordyceps superfine powder is with embodiment one; The protein sugar that in 93 kilograms of Cordyceps superfine powder, adds 3 kilograms, 2 kilograms Oleum menthae, 2 kilograms magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g/ sheet, 0.5g/ sheet, content's index: adenosine 〉=0.35mg/g, mannitol 〉=2.5%.
Embodiment 16
The preparation of Cordyceps superfine powder is with embodiment one; The ultra micro pollen (processed by breaking wall) that in 94 kilograms of Cordyceps superfine powder, adds 3 kilograms, 1 kilogram Oleum menthae, 2 kilograms magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g/ sheet, 0.5g/ sheet, content's index: adenosine 〉=0.35mg/g, mannitol 〉=2.5%.
Embodiment 17
The preparation of Cordyceps superfine powder is with embodiment one; The ultra micro pollen (processed by breaking wall) that in 95 kilograms of Cordyceps superfine powder, adds 1 kilogram, 1 kilogram protein sugar, 1 kilogram Oleum menthae, 2 kilograms magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g/ sheet, 0.5g/ sheet, content's index: adenosine 〉=0.35mg/g, mannitol 〉=2.5%.
Embodiment 18
The preparation of Cordyceps superfine powder is with embodiment one; The ultra micro pollen (processed by breaking wall) that in 93 kilograms of Cordyceps superfine powder, adds 2 kilograms, 2 kilograms protein sugar, 1.5 kilograms Oleum menthae, 1.5 kilograms magnesium stearate through mixing, granulation, drying, tabletting, packing, sterilization, promptly gets the Cordyceps mycelium micropowders buccal tablet.Product specification: 1.0g/ sheet, 0.5g/ sheet, content's index: adenosine 〉=0.35mg/g, mannitol 〉=2.5%.
Embodiment 14 to embodiment 18 prepared Cordyceps mycelium micropowders tablets are the sundown special-shaped tablets, are called the cordyceps-pollen buccal tablet.
Embodiment 19
The preparation of Cordyceps superfine powder is with embodiment one; Add 1 kilogram of yeastex in 98 kilograms of Cordyceps powder, 1 kilogram of medical dextrin promptly gets the Cordyceps mycelium micropowders capsule through mixing, drying, granulation, encapsulated, packing, sterilization, quality inspection.Product specification is 0.25g, 0.30g, 0.50g, content's index: total nitrogen 〉=3.43%, aminoacid 〉=19.00%, adenosine 〉=0.45mg/g.
Embodiment 20
The preparation of Cordyceps superfine powder is with embodiment one; In 97.5 kilograms of Cordyceps superfine powder, add 2 kilograms of medical dextrin, the Radix Panacis Quinquefolii saponin that adds 0.5 kilogram, promptly get Cordyceps mycelium Radix Panacis Quinquefolii saponin capsule through mixing, drying, granulation, encapsulated, packing, sterilization, quality inspection, product specification is 0.25g, 0.30g, 0.50g, content's index: total nitrogen 〉=3.4%, aminoacid 〉=19.5%, Radix Panacis Quinquefolii saponin 〉=0.2%.
Embodiment 21
The preparation of Cordyceps superfine powder is with embodiment one; In 79 kilograms of Cordyceps superfine powder, add 20 kilograms of Radix Panacis Quinquefolii powder superfine powder, 1 kilogram of yeastex, promptly get the Cordyceps mycelium American ginseng capsule through mixing, drying, granulation, encapsulated, packing, sterilization, quality inspection, product specification is 0.25g, 0.30g, 0.50g, content's index: total nitrogen 〉=3.3%, aminoacid 〉=19.0%, Radix Panacis Quinquefolii saponin 〉=0.25%.
Embodiment 22
The preparation of Cordyceps superfine powder is with embodiment one; Add 20 kilograms of ultra micro pollen (processed by breaking wall) in 79 kilograms of Cordyceps superfine powder, 1 kilogram of yeastex promptly gets the Cordyceps mycelium pollen capsule through mixing, drying, granulation, encapsulated, packing, sterilization, quality inspection.Product specification is 0.25g, 0.30g, 0.50g, content's index: total nitrogen 〉=3.4%, aminoacid 〉=19%, adenosine 〉=0.45mg/g.
Embodiment 23
The preparation of Cordyceps superfine powder is with embodiment one; Add 10 kilograms of ultra micro pollen (processed by breaking wall) in 89 kilograms of Cordyceps superfine powder, 1 kilogram of medical dextrin promptly gets the Cordyceps mycelium pollen capsule through mixing, drying, granulation, encapsulated, packing, sterilization, quality inspection.Product specification is 0.25g, 0.30g, 0.50g, content's index: total nitrogen 〉=3.4%, aminoacid 〉=19%, adenosine 〉=0.45mg/g.
Embodiment 24
The preparation of Cordyceps superfine powder is with embodiment one; Add 20 kilograms of Ganoderma superfine powder in 79 kilograms of Cordyceps superfine powder, 1 kilogram of medical dextrin promptly gets the Cordyceps mycelium LINGZHI JIAONANG through mixing, drying, granulation, encapsulated, packing, sterilization, quality inspection.Product specification is 0.25g, 0.30g, 0.50g, content's index: mannitol 〉=3%, aminoacid 〉=19%, adenosine 〉=0.45mg/g.
Claims (1)
1. the preparation method of a Cordyceps mycelium micropowders preparation is characterized in that with isolating Cordyceps Paecilomyces hepiali Chinese caterpillar fungus strain under 24～25 ℃ slant culture 5～6 days; Again with the shaking table training method under 24～25 ℃, carry out first order seed and cultivated 5～6 days, secondary seed was cultivated 5～6 days, 24～26 ℃ of following amplification culture 3 days; Cultivated 5～6 days in 24～26 ℃ of bottom fermentation jars then; Centrifugal filtration, filter cake is after below 75 ℃ dry 4～6 hours, be crushed to 60～80 orders, in 55 ℃ of following cold drying 5～6 hours, under-104 ℃, 0.6Mpa, carry out the ultra low temperature vacuum drying again, carry out the ultra micro wall breaking pulverization with the supersonic gas of the 1.92M/min fluidizing fluid-bed jet mill in bottom of flowing through again, make 325～560 orders ,≤the Cordyceps superfine powder of 38um; In 70～98.5% Cordyceps superfine powder, add two or three in the following batching or four kind in proportion: 0.5～4% yeastex, 1～20% medical dextrin, 0.5～3% Radix Panacis Quinquefolii saponin, 10～20% Radix Panacis Quinquefolii micropowder, 15～30% Ganoderma micropowder, 1～20% ultra micro pollen (processed by breaking wall), 0.5～3% protein sugar, 1～2% Oleum menthae, 3～5%CMC-Na (sodium carboxymethyl cellulose), 0.5～2% magnesium stearate; Obtain powder or tablet or capsular Cordyceps mycelium micropowders preparation through mixing, drying, component, packing, sterilization.
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2004
- 2004-01-09 CN CN 200410021637 patent/CN1640488A/en active Pending
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