CN1565727A - 一种新的负载型纳米金催化剂的制备方法 - Google Patents
一种新的负载型纳米金催化剂的制备方法 Download PDFInfo
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- CN1565727A CN1565727A CN 03138786 CN03138786A CN1565727A CN 1565727 A CN1565727 A CN 1565727A CN 03138786 CN03138786 CN 03138786 CN 03138786 A CN03138786 A CN 03138786A CN 1565727 A CN1565727 A CN 1565727A
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- Prior art keywords
- carrier
- gold
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- ion
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000010931 gold Substances 0.000 title claims abstract description 35
- 229910052737 gold Inorganic materials 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title claims abstract description 25
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 title claims description 24
- 239000003054 catalyst Substances 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000006243 chemical reaction Methods 0.000 claims abstract description 18
- 229920006395 saturated elastomer Polymers 0.000 claims abstract description 8
- 239000003513 alkali Substances 0.000 claims abstract description 4
- 238000002360 preparation method Methods 0.000 claims description 19
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 14
- 239000008367 deionised water Substances 0.000 claims description 11
- 229910021641 deionized water Inorganic materials 0.000 claims description 9
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 7
- 230000000274 adsorptive effect Effects 0.000 claims description 7
- 238000005470 impregnation Methods 0.000 claims description 7
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 6
- 239000002184 metal Substances 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 238000007598 dipping method Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 4
- FDWREHZXQUYJFJ-UHFFFAOYSA-M gold monochloride Chemical compound [Cl-].[Au+] FDWREHZXQUYJFJ-UHFFFAOYSA-M 0.000 claims description 4
- 238000001514 detection method Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 229910003771 Gold(I) chloride Inorganic materials 0.000 claims description 2
- 229910003803 Gold(III) chloride Inorganic materials 0.000 claims description 2
- 238000010521 absorption reaction Methods 0.000 claims description 2
- 230000032683 aging Effects 0.000 claims description 2
- 239000000919 ceramic Substances 0.000 claims description 2
- RJHLTVSLYWWTEF-UHFFFAOYSA-K gold trichloride Chemical compound Cl[Au](Cl)Cl RJHLTVSLYWWTEF-UHFFFAOYSA-K 0.000 claims description 2
- 229940076131 gold trichloride Drugs 0.000 claims description 2
- 238000000465 moulding Methods 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000002243 precursor Substances 0.000 claims description 2
- 230000003197 catalytic effect Effects 0.000 abstract description 8
- 239000006185 dispersion Substances 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 22
- 239000007789 gas Substances 0.000 description 7
- 150000002500 ions Chemical class 0.000 description 6
- 238000001556 precipitation Methods 0.000 description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000001257 hydrogen Substances 0.000 description 5
- 229910052739 hydrogen Inorganic materials 0.000 description 5
- 238000006555 catalytic reaction Methods 0.000 description 4
- 238000000975 co-precipitation Methods 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- 239000006228 supernatant Substances 0.000 description 4
- 230000001603 reducing effect Effects 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- 206010013786 Dry skin Diseases 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 210000000481 breast Anatomy 0.000 description 2
- 238000001802 infusion Methods 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000002803 maceration Methods 0.000 description 1
- 239000003863 metallic catalyst Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000012495 reaction gas Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
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Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 03138786 CN1259131C (zh) | 2003-07-08 | 2003-07-08 | 一种新的负载型纳米金催化剂的制备方法 |
Applications Claiming Priority (1)
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CN 03138786 CN1259131C (zh) | 2003-07-08 | 2003-07-08 | 一种新的负载型纳米金催化剂的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1565727A true CN1565727A (zh) | 2005-01-19 |
CN1259131C CN1259131C (zh) | 2006-06-14 |
Family
ID=34470589
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN 03138786 Expired - Fee Related CN1259131C (zh) | 2003-07-08 | 2003-07-08 | 一种新的负载型纳米金催化剂的制备方法 |
Country Status (1)
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CN (1) | CN1259131C (zh) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100435944C (zh) * | 2007-03-13 | 2008-11-26 | 浙江大学 | 一种负载型纳米金催化剂及制备方法 |
CN101254473B (zh) * | 2008-03-07 | 2010-06-02 | 厦门大学 | 一种带有机微球负载金纳米颗粒的固相催化剂的合成方法 |
CN101139332B (zh) * | 2007-09-27 | 2010-12-15 | 复旦大学 | 用负载型纳米金催化剂催化制备γ-丁内酯的方法 |
CN101157677B (zh) * | 2007-09-27 | 2011-05-04 | 复旦大学 | 一种用负载型纳米金催化剂制备δ-戊内酯的方法 |
CN100998940B (zh) * | 2006-01-10 | 2012-05-30 | 中国人民解放军63971部队 | 一种co催化材料的制备方法 |
CN113634251A (zh) * | 2021-09-08 | 2021-11-12 | 烟台大学 | 镨基载体负载纳米金催化剂,其制备方法及应用 |
CN114345327A (zh) * | 2022-03-01 | 2022-04-15 | 南京艾伊科技有限公司 | 电化学二氧化硫传感器的负载型纳米金催化剂及制备方法 |
-
2003
- 2003-07-08 CN CN 03138786 patent/CN1259131C/zh not_active Expired - Fee Related
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100998940B (zh) * | 2006-01-10 | 2012-05-30 | 中国人民解放军63971部队 | 一种co催化材料的制备方法 |
CN100435944C (zh) * | 2007-03-13 | 2008-11-26 | 浙江大学 | 一种负载型纳米金催化剂及制备方法 |
CN101139332B (zh) * | 2007-09-27 | 2010-12-15 | 复旦大学 | 用负载型纳米金催化剂催化制备γ-丁内酯的方法 |
CN101157677B (zh) * | 2007-09-27 | 2011-05-04 | 复旦大学 | 一种用负载型纳米金催化剂制备δ-戊内酯的方法 |
CN101254473B (zh) * | 2008-03-07 | 2010-06-02 | 厦门大学 | 一种带有机微球负载金纳米颗粒的固相催化剂的合成方法 |
CN113634251A (zh) * | 2021-09-08 | 2021-11-12 | 烟台大学 | 镨基载体负载纳米金催化剂,其制备方法及应用 |
CN113634251B (zh) * | 2021-09-08 | 2023-09-15 | 烟台大学 | 镨基载体负载纳米金催化剂,其制备方法及应用 |
CN114345327A (zh) * | 2022-03-01 | 2022-04-15 | 南京艾伊科技有限公司 | 电化学二氧化硫传感器的负载型纳米金催化剂及制备方法 |
Also Published As
Publication number | Publication date |
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CN1259131C (zh) | 2006-06-14 |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: SHANDONG RUISHI PROTECTION TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: AN LIDUN Effective date: 20090522 |
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C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20090522 Address after: Shanxi Province, Taiyuan City, No. 9 West Palace Xinghualing District building seven storey block B No. C Patentee after: Shanxi Ruishi Protection Technology Co., Ltd. Address before: Institute of applied catalysis, College of chemistry, Laishan District, Yantai, Shandong, China Patentee before: An Lidun |
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C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20060614 Termination date: 20130708 |