CN1449798A - Compound belladonna bismuth-magnesium tablet and preparation process thereof - Google Patents
Compound belladonna bismuth-magnesium tablet and preparation process thereof Download PDFInfo
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- CN1449798A CN1449798A CN 03116871 CN03116871A CN1449798A CN 1449798 A CN1449798 A CN 1449798A CN 03116871 CN03116871 CN 03116871 CN 03116871 A CN03116871 A CN 03116871A CN 1449798 A CN1449798 A CN 1449798A
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- pericarpium citri
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Abstract
The present invention discloses a compound belladonna bismuth-magnesium tablet and its preparation method. It is made from Chinese medicinal materials of rhubarb, tangerine peel, licorice, saussurea root and acorus root and magnesium trisilicate, bismuth subnitrate and sodium hydrogen carbonate are used as main raw material, and adding starch slurry and microcrystal cellulose, etc. as auxiliary material through a certain preparation process. Said invention compound has the functions of clearing heat away and removing toxic material, promoting circulation of qi, stopping pain, fortifying the spleen, dispersing food, etc. and can be used for curing gastroduodenal ulcer and chronic gastritis, etc.
Description
Technical field
What the present invention relates to is medicine in the field of medicaments, especially relates to a kind of sick Complex Belladonna bismuth magnesium sheet such as gastric and duodenal ulcers, chronic gastritis and preparation method thereof for the treatment of.
Background technology
Complex Belladonna bismuth magnesium sheet is a kind of sick medicine such as gastric and duodenal ulcers, chronic gastritis for the treatment of, because the process characteristic of this medicine is with the production technology difference of general Chinese patent medicine tablet, the composition that traditional handicraft is extracted is few, and the diameter of fine powder is excessive, active ingredient is difficult for being absorbed, and therapeutic effect is relatively poor.
Summary of the invention
The object of the present invention is to provide a kind of Complex Belladonna bismuth magnesium sheet that composition diameters many, fine powder are little, active ingredient easily is absorbed, therapeutic effect is good for the treatment of diseases such as gastric and duodenal ulcers, chronic gastritis, extracting and preparation method thereof.
The objective of the invention is such realization: the present invention is made up of following raw material by weight:
Pericarpium Citri Reticulatae 50-90g Radix Aucklandiae 19.5-29.5g
Radix Glycyrrhizae 50-90g Rhizoma Acori Graminei 4-8g
Radix Et Rhizoma Rhei 4-8g magnesium trisilicate 30-70g
Bismuth subnitrate 19.5-29.5g sodium bicarbonate 30-70g
Semen daturae fluid extract 1-3 milliliter
Its best proportioning is:
Pericarpium Citri Reticulatae 70g Radix Aucklandiae 24g
Radix Glycyrrhizae 70g Rhizoma Acori Graminei 6g
Radix Et Rhizoma Rhei 6g magnesium trisilicate 48g
Bismuth subnitrate 24g sodium bicarbonate 48g
2 milliliters of Semen daturae fluid extracts
Its preparation method is:
First kind of preparation method:
(1), Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei are cleaned respectively, remove impurity, be up to the standards;
(2), Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei pulverize separately that will be after the assay was approved become fine powder, obtains Pericarpium Citri Reticulatae fine powder, Radix Aucklandiae fine powder, Radix Glycyrrhizae fine powder, Rhizoma Acori Graminei fine powder, Radix Et Rhizoma Rhei fine powder;
(3), magnesium trisilicate, bismuth subnitrate, sodium bicarbonate pulverize separately are become fine powder, obtain magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder;
(4), with above-mentioned seven kinds of fine powder mix homogeneously, add Semen daturae fluid extract again, stir, add starch slurry then, stir, make soft material, granulate drying;
(5), again add the adjuvant mix homogeneously, tabletting gets product after the packing.
Second kind of preparation method:
(1), Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei are cleaned respectively, remove impurity, be up to the standards;
(2), Radix Glycyrrhizae, Radix Et Rhizoma Rhei, magnesium trisilicate, bismuth subnitrate, sodium bicarbonate pulverize separately are become fine powder, obtain Radix Glycyrrhizae fine powder, Radix Et Rhizoma Rhei fine powder, magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder;
(3), three kinds of medical materials of Pericarpium Citri Reticulatae, the Radix Aucklandiae, Rhizoma Acori Graminei are mixed, and be ground into coarse powder, from coarse powder, extract volatile oil more according to a conventional method, and ground-slag is broken into fine powder, obtain Pericarpium Citri Reticulatae, the Radix Aucklandiae, Rhizoma Acori Graminei fine powder;
(4), volatile oil is become the volatile oil alcoholic solution with dissolve with ethanol;
(5), with Radix Glycyrrhizae fine powder, Radix Et Rhizoma Rhei fine powder, magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder and Pericarpium Citri Reticulatae, the Radix Aucklandiae, Rhizoma Acori Graminei fine powder mix homogeneously, add starch slurry again and stir, granulate drying;
(6), then add volatile oil alcoholic solution and adjuvant mix homogeneously, tabletting gets product after the packing.
The third preparation method:
(1), with Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei, clean respectively, remove impurity, be up to the standards;
(2), the Radix Glycyrrhizae that is up to the standards added water run through, section decocts with water, collecting decoction was placed liquid and was made precipitation, got supernatant concentration to the thick paste shape, obtained the Radix Glycyrrhizae thick paste;
(3), the Pericarpium Citri Reticulatae with being up to the standards, the Radix Aucklandiae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei, pulverize separately becomes fine powder, obtains Pericarpium Citri Reticulatae fine powder, Radix Aucklandiae fine powder, Rhizoma Acori Graminei fine powder, Radix Et Rhizoma Rhei fine powder;
(4), magnesium trisilicate, bismuth subnitrate, sodium bicarbonate pulverize separately are become fine powder, obtain magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder;
(5), with Pericarpium Citri Reticulatae fine powder, Radix Aucklandiae fine powder, Rhizoma Acori Graminei fine powder, Radix Et Rhizoma Rhei fine powder, magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder mix homogeneously, add Semen daturae fluid extract, Radix Glycyrrhizae thick paste again, mix homogeneously;
(6), again add starch slurry, stir, make soft material, granulate, drying adds adjuvant then, mix homogeneously, and tabletting gets product after the packing.
Adjuvant in these three kinds of preparation methoies is microcrystalline Cellulose, starch, micropowder silica gel, magnesium stearate.
Coarse powder is a 5-20 purpose coarse powder, and the best is 10 purpose coarse powder.
Fine powder is 60-160 purpose fine powder or 200-3000 purpose superfine powder.
The present invention is to be primary raw material with Radix Et Rhizoma Rhei, Pericarpium Citri Reticulatae, Radix Glycyrrhizae, the Radix Aucklandiae, Rhizoma Acori Graminei, magnesium trisilicate, bismuth subnitrate, sodium bicarbonate, be aided with adjuvants such as starch slurry, microcrystalline Cellulose, starch, micropowder silica gel, magnesium stearate again, form by certain prepared.Magnesium trisilicate plays neutralization or cushioning effect to the already present gastric acid of gastric; but the secretion of gastric acid there is not direct influence; and have hypocatharsis and protect the gastric mucosa effect; bismuth subnitrate has the convergence of protection gastric mucosa; anti-diarrhea effect; sodium bicarbonate can neutralize rapidly or cushion gastric acid; Semen daturae fluid extract can be alleviated cramps of gastrointestinal tract and suppress the gastrointestinal tract glandular secretion; Radix Et Rhizoma Rhei purges heat unobstructed in the Chinese medicine; removing pathogenic heat from blood and toxic substance from the body; the Pericarpium Citri Reticulatae regulating qi-flowing for strengthening spleen; but Radix Aucklandiae promoting the circulation of QI to relieve pain; strengthening the spleen to promote digestion; Rhizoma Acori Graminei can whet the appetite in removing dampness; and Radix Glycyrrhizae energy invigorating the spleen and replenishing QI; heat clearing away is separated; relieving spasm to stop pain; therefore Complex Belladonna bismuth magnesium sheet of the present invention can be treated gastric and duodenal ulcers; diseases such as chronic gastritis; the present invention has compared with prior art: production technology more becomes to improving rationally; can keep the active substance in the medical material more; quality standard and product stability improve greatly; the effect duration of medicine reached more than 3 years, and it is many to have a composition of extraction; the diameter of fine powder is little; active ingredient easily is absorbed; the advantage that therapeutic effect is good.
The specific embodiment
Below in conjunction with embodiment the present invention is described in further detail, but should understands the non-scope that only limits to these embodiment of scope of the present invention.
Embodiment 1:
(1), Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei are cleaned respectively, remove impurity, be up to the standards;
(2), 50 gram Pericarpium Citri Reticulataes, the 19.5 gram Radix Aucklandiae, 50 gram Radix Glycyrrhizaes, the 4 gram Rhizoma Acori Graminei, 4 that take by weighing respectively after the assay was approved restrain Radix Et Rhizoma Rhei, Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei pulverize separately are become 60 order fine powders, obtain Pericarpium Citri Reticulatae fine powder, Radix Aucklandiae fine powder, Radix Glycyrrhizae fine powder, Rhizoma Acori Graminei fine powder, Radix Et Rhizoma Rhei fine powder;
Take by weighing 30 gram magnesium trisilicate, 19.5 gram bismuth subnitrates, 30 gram sodium bicarbonate, magnesium trisilicate, bismuth subnitrate, sodium bicarbonate pulverize separately are become 60 order fine powders, obtain magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder (3), respectively;
(4), with Pericarpium Citri Reticulatae fine powder, Radix Aucklandiae fine powder, Radix Glycyrrhizae fine powder, Rhizoma Acori Graminei fine powder, gram Radix Et Rhizoma Rhei fine powder, magnesium silicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder mix homogeneously, add 1 milliliter of Semen daturae fluid extract again, stir, add starch slurry then, stir, make soft material, granulate drying;
(5), again add the adjuvant mix homogeneously, tabletting gets product after the packing.
Embodiment 2:
(1), Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei are cleaned respectively, remove impurity, be up to the standards;
(2), take by weighing 90 gram Radix Glycyrrhizaes, 8 gram Radix Et Rhizoma Rhei, magnesium trisilicate 70 grams, 29.5 gram bismuth subnitrates, 70 gram sodium bicarbonate respectively, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, magnesium trisilicate, bismuth subnitrate, sodium bicarbonate pulverize separately are become 160 order fine powders, obtain Radix Glycyrrhizae fine powder, Radix Et Rhizoma Rhei fine powder, magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder;
Take by weighing 90 gram Pericarpium Citri Reticulataes, the 29.5 gram Radix Aucklandiae, 8 gram Rhizoma Acori Graminei, three kinds of medical materials are mixed, and be ground into 10 order coarse powder, from coarse powder, extract volatile oil more according to a conventional method, and ground-slag is broken into 160 order fine powders, obtain Pericarpium Citri Reticulatae, the Radix Aucklandiae, Rhizoma Acori Graminei fine powder (3), respectively;
(4), volatile oil is become the volatile oil alcoholic solution with dissolve with ethanol;
(5), with Radix Glycyrrhizae fine powder, Radix Et Rhizoma Rhei fine powder, magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder and Pericarpium Citri Reticulatae, the Radix Aucklandiae, Rhizoma Acori Graminei fine powder mix homogeneously, add starch slurry again and stir, granulate drying;
(6), then add volatile oil alcoholic solution and adjuvant mix homogeneously, tabletting gets product after the packing.
Embodiment 3:
(1), with Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei, clean respectively, remove impurity, be up to the standards;
(2), take by weighing 70 the gram Radix Glycyrrhizaes, Radix Glycyrrhizae is added water runs through, the section, decoct with water, collecting decoction was placed liquid and was made precipitation, got supernatant concentration to the thick paste shape, obtained the Radix Glycyrrhizae thick paste;
(3), respectively take by weighing 70 gram Pericarpium Citri Reticulataes, the 24 gram Radix Aucklandiae, 6 gram Rhizoma Acori Graminei, 6 gram Radix Et Rhizoma Rhei, with Pericarpium Citri Reticulatae, the Radix Aucklandiae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei, pulverize separately becomes 3000 order superfine powder, obtains Pericarpium Citri Reticulatae superfine powder, Radix Aucklandiae superfine powder, Rhizoma Acori Graminei superfine powder, Radix Et Rhizoma Rhei superfine powder;
Take by weighing 48 gram magnesium trisilicate, 24 gram bismuth subnitrates, 48 gram sodium bicarbonate, magnesium trisilicate, bismuth subnitrate, sodium bicarbonate pulverize separately are become 1000 order superfine powder, obtain magnesium trisilicate superfine powder, bismuth subnitrate superfine powder, sodium bicarbonate superfine powder (4), respectively;
(5), with Pericarpium Citri Reticulatae superfine powder, Radix Aucklandiae superfine powder, Rhizoma Acori Graminei superfine powder, Radix Et Rhizoma Rhei superfine powder, magnesium trisilicate superfine powder, bismuth subnitrate superfine powder, sodium bicarbonate superfine powder mix homogeneously, add Radix Glycyrrhizae thick paste and 2 milliliters of Semen daturae fluid extracts again, mix homogeneously;
(6), again add starch slurry, stir, make soft material, granulate, drying adds adjuvant then, mix homogeneously, and tabletting gets product after the packing.
Claims (8)
1, a kind of Complex Belladonna bismuth magnesium sheet is characterized in that: be made up of following raw material by weight:
Pericarpium Citri Reticulatae 50-90g Radix Aucklandiae 19.5-29.5g
Radix Glycyrrhizae 50-90g Rhizoma Acori Graminei 4-8g
Radix Et Rhizoma Rhei 4-8g magnesium trisilicate 30-70g
Bismuth subnitrate 19.5-29.5g sodium bicarbonate 30-70g
Semen daturae fluid extract 1-3 milliliter.
2, Complex Belladonna bismuth magnesium sheet as claimed in claim 1, it is characterized in that: its best proportioning is:
Pericarpium Citri Reticulatae 70g Radix Aucklandiae 24g
Radix Glycyrrhizae 70g Rhizoma Acori Graminei 6g
Radix Et Rhizoma Rhei 6g magnesium trisilicate 48g
Bismuth subnitrate 24g sodium bicarbonate 48g
2 milliliters of Semen daturae fluid extracts.
3, the method for preparation Complex Belladonna bismuth magnesium sheet as claimed in claim 1 or 2 is characterized in that:
(1), Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei are cleaned respectively, remove impurity, be up to the standards;
(2), Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei pulverize separately that will be after the assay was approved become fine powder, obtains Pericarpium Citri Reticulatae fine powder, Radix Aucklandiae fine powder, Radix Glycyrrhizae fine powder, Rhizoma Acori Graminei fine powder, Radix Et Rhizoma Rhei fine powder;
(3), magnesium trisilicate, bismuth subnitrate, sodium bicarbonate pulverize separately are become fine powder, obtain magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder;
(4), with above-mentioned seven kinds of fine powder mix homogeneously, add Semen daturae fluid extract again, stir, add starch slurry then, stir, make soft material, granulate drying;
(5), again add the adjuvant mix homogeneously, tabletting gets product after the packing.
4, the method for preparation Complex Belladonna bismuth magnesium sheet as claimed in claim 1 or 2 is characterized in that:
(1), Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei are cleaned respectively, remove impurity, be up to the standards;
(2), Radix Glycyrrhizae, Radix Et Rhizoma Rhei, magnesium trisilicate, bismuth subnitrate, sodium bicarbonate pulverize separately are become fine powder, obtain Radix Glycyrrhizae fine powder, Radix Et Rhizoma Rhei fine powder, magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder;
(3), three kinds of medical materials of Pericarpium Citri Reticulatae, the Radix Aucklandiae, Rhizoma Acori Graminei are mixed, and be ground into coarse powder, from coarse powder, extract volatile oil more according to a conventional method, and ground-slag is broken into fine powder, obtain Pericarpium Citri Reticulatae, the Radix Aucklandiae, Rhizoma Acori Graminei fine powder;
(4), volatile oil is become the volatile oil alcoholic solution with dissolve with ethanol;
(5), with Radix Glycyrrhizae fine powder, Radix Et Rhizoma Rhei fine powder, magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder and Pericarpium Citri Reticulatae, the Radix Aucklandiae, Rhizoma Acori Graminei fine powder mix homogeneously, add starch slurry again and stir, granulate drying;
(6), then add volatile oil alcoholic solution and adjuvant mix homogeneously, tabletting gets product after the packing.
5, the method for preparation Complex Belladonna bismuth magnesium sheet as claimed in claim 4, it is characterized in that: coarse powder is a 5-20 purpose coarse powder, the best is 10 purpose coarse powder.
6, the method for preparation Complex Belladonna bismuth magnesium sheet as claimed in claim 1 or 2 is characterized in that:
(1), with Pericarpium Citri Reticulatae, the Radix Aucklandiae, Radix Glycyrrhizae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei, clean respectively, remove impurity, be up to the standards;
(2), the Radix Glycyrrhizae that is up to the standards added water run through, section decocts with water, collecting decoction was placed liquid and was made precipitation, got supernatant concentration to the thick paste shape, obtained the Radix Glycyrrhizae thick paste;
(3), the Pericarpium Citri Reticulatae with being up to the standards, the Radix Aucklandiae, Rhizoma Acori Graminei, Radix Et Rhizoma Rhei, pulverize separately becomes fine powder, obtains Pericarpium Citri Reticulatae fine powder, Radix Aucklandiae fine powder, Rhizoma Acori Graminei fine powder, Radix Et Rhizoma Rhei fine powder;
(4), magnesium trisilicate, bismuth subnitrate, sodium bicarbonate pulverize separately are become fine powder, obtain magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder;
(5), with Pericarpium Citri Reticulatae fine powder, Radix Aucklandiae fine powder, Rhizoma Acori Graminei fine powder, Radix Et Rhizoma Rhei fine powder, magnesium trisilicate fine powder, bismuth subnitrate fine powder, sodium bicarbonate fine powder mix homogeneously, add Semen daturae fluid extract, Radix Glycyrrhizae thick paste again, mix homogeneously;
(6), again add starch slurry, stir, make soft material, granulate, drying adds adjuvant then, mix homogeneously, and tabletting gets product after the packing.
7, preparation is as the method for claim 3 or 4 or 6 described Complex Belladonna bismuth magnesium sheets, and it is characterized in that: adjuvant is microcrystalline Cellulose, starch, micropowder silica gel, magnesium stearate.
8, preparation is as the method for claim 3 or 4 or 6 described Complex Belladonna bismuth magnesium sheets, and it is characterized in that: fine powder is 60-160 purpose fine powder or 200-3000 purpose superfine powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03116871 CN1449798A (en) | 2003-05-09 | 2003-05-09 | Compound belladonna bismuth-magnesium tablet and preparation process thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03116871 CN1449798A (en) | 2003-05-09 | 2003-05-09 | Compound belladonna bismuth-magnesium tablet and preparation process thereof |
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| CN1449798A true CN1449798A (en) | 2003-10-22 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1297304C (en) * | 2005-03-24 | 2007-01-31 | 倪友洪 | Aquilarid distillate suspensoid agent and its preparation method |
| CN1314407C (en) * | 2005-02-18 | 2007-05-09 | 广州白云山侨光制药有限公司 | Compound vitamin U atropa belladonna bismuth-aluminium medicine table for treating gastric ulcer |
| CN100425263C (en) * | 2005-06-15 | 2008-10-15 | 肖万郁 | Gastric medicine and its preparation method |
| CN108272931A (en) * | 2018-04-12 | 2018-07-13 | 成都倍特药业有限公司 | A kind of sweet bismuth magnesium compound medicine and preparation method thereof |
| CN109771649A (en) * | 2018-02-26 | 2019-05-21 | 上海金城药业有限公司 | For preventing and treating chronic gastritis and alleviating the new pharmaceutical compositions and preparation method thereof of hyperhydrochloria initiation disease |
-
2003
- 2003-05-09 CN CN 03116871 patent/CN1449798A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1314407C (en) * | 2005-02-18 | 2007-05-09 | 广州白云山侨光制药有限公司 | Compound vitamin U atropa belladonna bismuth-aluminium medicine table for treating gastric ulcer |
| CN1297304C (en) * | 2005-03-24 | 2007-01-31 | 倪友洪 | Aquilarid distillate suspensoid agent and its preparation method |
| CN100425263C (en) * | 2005-06-15 | 2008-10-15 | 肖万郁 | Gastric medicine and its preparation method |
| CN109771649A (en) * | 2018-02-26 | 2019-05-21 | 上海金城药业有限公司 | For preventing and treating chronic gastritis and alleviating the new pharmaceutical compositions and preparation method thereof of hyperhydrochloria initiation disease |
| CN109771649B (en) * | 2018-02-26 | 2021-12-28 | 上海金城素智药业有限公司 | Novel pharmaceutical composition for preventing and treating chronic gastritis and relieving diseases caused by hyperacidity and preparation method thereof |
| CN108272931A (en) * | 2018-04-12 | 2018-07-13 | 成都倍特药业有限公司 | A kind of sweet bismuth magnesium compound medicine and preparation method thereof |
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