CN1317242C - Organic liquid fertilizer and its preparation method - Google Patents
Organic liquid fertilizer and its preparation method Download PDFInfo
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- CN1317242C CN1317242C CNB2005100486858A CN200510048685A CN1317242C CN 1317242 C CN1317242 C CN 1317242C CN B2005100486858 A CNB2005100486858 A CN B2005100486858A CN 200510048685 A CN200510048685 A CN 200510048685A CN 1317242 C CN1317242 C CN 1317242C
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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Abstract
The present invention discloses an organic liquid fertilizer and a preparation method thereof. Waste molasses generated in the process of the production of white sugar is used as a main raw material for production; the waste molasses is treated through a series of steps, such as dilution, filtration, pH value adjustment, fermentation, etc., and finally, the waste molasses is treated through pasteurization to obtain the final product. The organic liquid fertilizer rich in elements, such as nitrogen, phosphorus, potassium, etc., can promote the propagation of beneficial microbes in soil, enhance the water preserving capability, the fertilizer preserving capability and the metabolism capability of the soil and effectively solve soil organic matter losses caused by a 'depredatory' planting mode. The present invention has the advantages of simple and convenient process, low cost, and safe and reliable product. The present invention has outstanding economic benefit, ecological benefit and social benefit.
Description
Technical field
The invention belongs to the chemical fertilizers production technical field, be specifically related to a kind of organic liquid fertilizer and preparation method thereof.
Background technology
China is large agricultural country, and since ancient times, fertilizer is fertile as the basis of agricultural and forestry production always.But along with the fast development of plant husbandry, use chemical fertilizer easy quick-acting, can increase production the common recognition that becomes a lot of people gradually fast.But the life-time service of chemical fertilizer can cause consuming excessively with soil fertility of a large amount of Nonrenewable energy resources to be failed.In order to deal with this situation, people have to strengthen fertilizer amount gradually, and form vicious cycle, thereby cause serious day by day ecotope negative effect, and it is bad that the physico-chemical property of soil becomes.Present stage, soil acidification, harden, farm crop chemical fertilizer residual quantity problem such as exceed standard is seen in report often, and these problems become the bottleneck of the restriction national economic development gradually.And existing solid organic fertilizer not only total nutrient content is lower, fertilizer efficiency can not show a candle to inorganic fertilizer.Simultaneously,, contain a large amount of pathogenic micro-organisms,, very likely cause secondary pollution if sterilization is not thorough because its raw material sources are mainly feces of livestock and poultry and stalk.
It should be noted that in the sugar industry production process to produce the surprising waste of quantity, as waste molasses.These wastes can cause severe contamination to water source and surrounding environment if not adding just to handle directly discharges.Though and also be no lack of the method for processing in the prior art, exist all that energy consumption is big, working cost is high, administer and thoroughly, easily do not cause secondary pollution problems.But then, contain a large amount of available resources in these wastes again.With the waste molasses is example, wherein just contains abundant organism, protein and nitrogen sulphur compounds.These resources then will produce far-reaching influence in economic and social aspect if can be converted into the raw material of organic fertilizer production.Therefore, how to improve the fertilizer efficiency utilization ratio of organic fertilizer, realize the comprehensive utilization of waste molasses, just become the technical problem that needs to be resolved hurrily in the prior art.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, with waste molasses as main production raw material, provide a kind of fertilizer efficiency remarkable, safe in utilization, and can improve Soil structure organic liquid fertilizer.
Another object of the present invention provides the preparation method of described organic liquid fertilizer.
Purpose of the present invention is achieved by the following technical programs.
Organic liquid fertilizer of the present invention is made up of the raw material of following weight parts: 10～30 parts of waste molasses, 0.3～1 part in ammonium sulfate, 4～4.5 parts in urea, 3～8 parts of monoammonium phosphates, 4～8 parts of vitriolate of tartar, 50～70 parts in water, 0.1～0.2 part in sulfuric acid.
Become the method for organic liquid fertilizer to form by following steps successively the feedstock production of above-mentioned weight part:
(1) waste molasses is placed in the fermentor tank with the clear water dilution, filter, add sulfuric acid, regulate pH value to 4.5～5.0;
(2) sealed fermenting jar is heated while stirring to 20 ℃～30 ℃;
(3) stir after 2～3 days, treat that pot liquid begins to stop heating when spontaneous fermentation heats up, when temperature in the jar reaches 35 ℃～40 ℃, open and jar add an ammonium sulfate, and then airtight stirring 2～3 days;
(4) open jar, add urea, monoammonium phosphate and vitriolate of tartar successively, airtight stirring 1～2 day is after the sterilization of crust formula promptly obtains organic liquid fertilizer.
In the process of the described heating while stirring of step 2, use air compressor machine to carry out not intermittent aeration processing, the air of feeding is handled through activated carbon canister and is filtered.
In the described airtight once more whipping process of step 3, use air compressor machine to carry out not intermittent aeration processing, the air of feeding is handled through activated carbon canister and is filtered.
The present invention has following advantage with respect to prior art: 1, for farm crop provide full nutrition, promote plant growth.Elements such as the nitrogen that it was rich in, phosphorus, potassium can promote beneficial microorganism breeding in the soil, strengthen soil water-reataining fertilizer-keeping ability and metabolic ability, improve the soil organism that causes because of " predation formula " planting patterns effectively and run off.2, utilize the waste molasses that produces in the white sugar production process as main raw material, both reduced the exhaust emission in the Closed Circulation in Sugar Production, increased the added value that sugar-refining industry is produced simultaneously, product safety is reliable.3, use with respect to solid fertilizer convenient, be used with chemical fertilizer can emergency help mutually, complementary short long.4, technology is easy, with low cost, has remarkable economical, ecology and social benefit.
The present invention detects through Yunnan Academy of Agricultural Sciences, and detected result sees Table 1.
Table 1
| Project | Index | |
| Total nutrient (N+P 2O 5+K 2O) massfraction/% | ≥ | 8.0 |
| Organic massfraction/% | ≥ | 7.5 |
| Humic acids 1% | ≥ | 15 |
| Water-insoluble % | ≤ | 5.0 |
| PH value | 3.5-6.0 | |
| Induced worm egg death rate % | ≥ | 95 |
| Colititre | ≥ | 10 -1 |
| Massfraction/the % of arsenic and compound thereof (in As) | ≤ | 0.0050 |
| Massfraction/the % of cadmium and compound thereof (in Cd) | ≤ | 0.0010 |
| Massfraction/the % of lead and compound thereof (in Pb) | ≤ | 0.0150 |
| Massfraction/the % of chromium and compound thereof (in Cr) | ≤ | 0.0500 |
| Massfraction/the % of mercury and compound thereof (in Hg) | ≤ | 0.0005 |
Embodiment
Below in conjunction with embodiment and Application Example the present invention is described in further detail, but they are not limitation of the invention.
Embodiment 1
10 portions of waste molasses are placed in the fermentor tank with 50 parts of clear water dilutions, filter, adds 0.1 part of sulfuric acid, adjusting pH value to 4.5～5.0; The sealed fermenting jar is heated 20 ℃ while stirring, uses air compressor machine to carry out not intermittent aeration processing therebetween, and the air of feeding is handled through activated carbon canister and filtered; Stir after 2 days, treat that pot liquid begins to stop heating when spontaneous fermentation heats up, when temperature in the jar reaches 35 ℃, open and jar add 0.3 part of ammonium sulfate, and then airtight stirring 2 days, intermittent aeration is not handled therebetween; Open jar, add 4 parts of 4 parts in urea, 3 parts of monoammonium phosphates and vitriolate of tartar successively, airtight stirring 1 day is after the sterilization of crust formula promptly gets organic liquid fertilizer.
Embodiment 2
Repeat embodiment 1, following difference is arranged: the raw material of interpolation is respectively 20 parts of waste molasses, 0.5 part in ammonium sulfate, 4.3 parts in urea, 6 parts of monoammonium phosphates, 6 parts of vitriolate of tartar, 63 parts in water, 0.15 part in sulfuric acid.
Embodiment 3
Repeat embodiment 1, following difference is arranged: 30 parts in molasses, 0.8 part in ammonium sulfate, 4.5 parts in urea, 8 parts of monoammonium phosphates, 8 parts of vitriolate of tartar, 70 parts in water, 0.2 part in sulfuric acid.
Embodiment 4～6
Repeat embodiment 1, following difference is arranged: the waste molasses of interpolation is respectively 15 parts, 18 parts, 25 parts.
Embodiment 7
Repeat embodiment 1, following difference is arranged: the raw material of interpolation is respectively 18 parts of waste molasses, 1 part in ammonium sulfate, 4.5 parts in urea, 6 parts of monoammonium phosphates, 8 parts of vitriolate of tartar.
Embodiment 8
Repeat embodiment 1, following difference is arranged: heat while stirring to 25 ℃.
Embodiment 9
Repeat embodiment 1, following difference is arranged: heat while stirring to 30 ℃.
Embodiment 10
Repeat embodiment 1, following difference is arranged: when temperature in the jar reaches 40 ℃, open a jar adding ammonium sulfate.
Application Example 1
Test unit: clay fertilizer station, Chenggong County, Kunming, Yunnan Province
Trial crops: romaine lettuce
Test site: vegetables base, dragon city, Chenggong County, Kunming, Yunnan Province, height above sea level 1900m, 14.7 ℃ of average annual temperature, annual precipitation 789mm, soil are the vegetable plot soil that forms after the dry farming of submerging type rice soil.Soil fertility is medium, and the previous crops Caulis et Folium Brassicae capitatae is a plastic film mulching cultivation.
Randomized block design is adopted in test, three test group, and three repetitions, a control group (ck) adopts conventional fertilizer application, 0.02 mu of region area.
Test group 1: water and execute organic fertilizer 10kg/ mu;
Test group 2: spray organic fertilizer 2kg/ mu;
Test group 3: water and execute organic fertilizer 10kg/ mu+spray organic fertilizer 1kg/ mu.
Test in beginning on July 6th, 2005, the romaine lettuce seedling age of transplanting 24 days, seeding row spacing 36.3 * (38+47) cm, 4 duplicate rows in every sub-district, every row 11 strains, every mu 4321 strain is amounted in 88 strains of every sub-district.After ripening on August 19 results are carried out moisture management therebetween in good time and sick Chinese caterpillar fungus is prevented and kill off.
Test-results sees Table 2,3,4.
Table 2: cell production (kg)
| Handle | Cell production | Tt (total) | Xt (on average) | Amount to per mu yield | Than ck ± | |||
| I | II | III | kg | ％ | ||||
| 1 | 32.6 | 31.1 | 33.2 | 96.9 | 32.3 | 2393 | 96 | 4.18 |
| 2 | 31.6 | 31.1 | 32.8 | 95.5 | 31.8 | 2358 | 62 | 2.70 |
| 3 | 33.4 | 32.0 | 32.8 | 98.2 | 32.7 | 2425 | 129 | 5.62 |
| Ck | 30.3 | 31.3 | 31.4 | 93.0 | 31.0 | 2296 | ||
| Tr (total) | 127.9 | 125.5 | 130.2 | 383.6 | ||||
| Xr (on average) | 32.0 | 31.4 | 32.6 |
Table 3: economic benefit relatively
| Handle | Output (kg/ mu) | New units increased in production (kg/ mu) | New output value (unit/mu) | Additional cost (unit/mu) | The newly-increased income (unit/mu) of depositing | Go into operation and compare |
| 1 | 2393 | 96 | 153.60 | 40.00 | 113.60 | 1∶3.84 |
| 2 | 2358 | 62 | 99.20 | 8.00 | 91.20 | 1∶12.40 |
| 3 | 2425 | 129 | 206.40 | 44.00 | 162.40 | 1∶4.69 |
| Ck | 2296 |
Annotate: unit price is by market price 1.60/kg (clean vegetables output)
Table 4: plant biological character
| Handle | Plant height (cm) | Than ck ± (cm) | Degree of development (cm) | Than ck ± (cm) | Individual plant heavy (g) | Than ck ± (g) |
| 1 | 22.7 | 0.4 | 34.6 | 0.7 | 598 | 24 |
| 2 | 22.5 | 0.2 | 34.5 | 0.6 | 589 | 15 |
| 3 | 23.1 | 0.8 | 34.9 | 1.0 | 606 | 32 |
| ck | 22.3 | 33.9 | 574 |
Claims (4)
1, a kind of organic liquid fertilizer, this fertilizer is made up of the raw material of following weight parts: 10～30 parts of waste molasses, 0.3～1 part in ammonium sulfate, 4～4.5 parts in urea, 3～8 parts of monoammonium phosphates, 4～8 parts of vitriolate of tartar, 50～70 parts in water, 0.1～0.2 part in sulfuric acid.
2, the method for preparing the described organic liquid fertilizer of claim 1 is characterized in that this method is made up of following steps:
(1) waste molasses is placed in the fermentor tank with the clear water dilution, filter, add sulfuric acid, regulate pH value to 4.5～5.0;
(2) sealed fermenting jar is heated while stirring to 20 ℃～30 ℃;
(3) stir after 2～3 days, treat that pot liquid begins to stop heating when spontaneous fermentation heats up, when temperature in the jar reaches 35 ℃～40 ℃, open and jar add an ammonium sulfate, and then airtight stirring 2～3 days;
(4) open jar, add urea, monoammonium phosphate and vitriolate of tartar successively, airtight stirring 1～2 day is after the sterilization of crust formula promptly obtains organic liquid fertilizer.
3, method according to claim 2 is characterized in that: in the described process of heating while stirring of step 2, use air compressor machine to carry out not intermittent aeration processing, the air of feeding is handled through activated carbon canister and is filtered.
4, method according to claim 2 is characterized in that: in the described airtight once more whipping process of step 3, use air compressor machine to carry out not intermittent aeration processing, the air of feeding is handled through activated carbon canister and is filtered.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100486858A CN1317242C (en) | 2005-12-13 | 2005-12-13 | Organic liquid fertilizer and its preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100486858A CN1317242C (en) | 2005-12-13 | 2005-12-13 | Organic liquid fertilizer and its preparation method |
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| CN1785931A CN1785931A (en) | 2006-06-14 |
| CN1317242C true CN1317242C (en) | 2007-05-23 |
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| CNB2005100486858A Expired - Fee Related CN1317242C (en) | 2005-12-13 | 2005-12-13 | Organic liquid fertilizer and its preparation method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101774834B (en) * | 2009-02-27 | 2011-12-28 | 张志元 | Plant nutritional agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102659465B (en) * | 2012-05-30 | 2014-08-13 | 广西新方向化学工业有限公司 | High-concentration organic and inorganic foliar fertilizer containing major elements and trace elements, and preparation method thereof |
| CN103392546B (en) * | 2013-08-09 | 2016-03-09 | 重庆富博生物技术有限公司 | The cultivating and growing process of a kind of paddy rice |
| CN104557184A (en) * | 2013-10-14 | 2015-04-29 | 北京世纪阿姆斯生物技术股份有限公司 | Molasses fermentation liquor water-soluble fertilizer and preparation method thereof |
| CN104628475A (en) * | 2015-02-03 | 2015-05-20 | 黑龙江八一农垦大学 | Method for preparing organic punching fertilizer from metheglin |
| CN105646085A (en) * | 2016-03-01 | 2016-06-08 | 深圳市芭田生态工程股份有限公司 | Liquid microbial organic fertilizer |
| CN114988937A (en) * | 2019-05-08 | 2022-09-02 | 内蒙古佰惠生新农业科技股份有限公司 | Special liquid fertilizer for beet prepared by using yeast concentrated solution |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1042726C (en) * | 1990-12-30 | 1999-03-31 | 顺德县食品公司均安有机肥料厂 | Method for producing organic composition fertilizer from fermented waste liquid of sugar |
| CN1480430A (en) * | 2002-09-04 | 2004-03-10 | 莫志鸿 | Liquid fertilizer made from waste fluid of molasses and alcohol as well as its preparing method |
-
2005
- 2005-12-13 CN CNB2005100486858A patent/CN1317242C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1042726C (en) * | 1990-12-30 | 1999-03-31 | 顺德县食品公司均安有机肥料厂 | Method for producing organic composition fertilizer from fermented waste liquid of sugar |
| CN1480430A (en) * | 2002-09-04 | 2004-03-10 | 莫志鸿 | Liquid fertilizer made from waste fluid of molasses and alcohol as well as its preparing method |
Non-Patent Citations (1)
| Title |
|---|
| 日本糖蜜酒精废液处理技术 周素华，酿酒科技，第3期 2003 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101774834B (en) * | 2009-02-27 | 2011-12-28 | 张志元 | Plant nutritional agent |
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| CN1785931A (en) | 2006-06-14 |
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Owner name: WEI ZHIGANG; APPLICANT Free format text: FORMER OWNER: WEI ZHIGANG Effective date: 20061103 |
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Effective date of registration: 20061103 Address after: 650225, No. 7, No. 1-203, Jinzhou Bay District, Beijing Road, Kunming, Yunnan Applicant after: Wei Zhigang Co-applicant after: Ma Ruofei Address before: 650225, No. 7, No. 1-203, Jinzhou Bay District, Beijing Road, Kunming, Yunnan Applicant before: Wei Zhigang |
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