CN1228339C - 选择性合成三亚乙基二胺的方法 - Google Patents

选择性合成三亚乙基二胺的方法 Download PDF

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Publication number
CN1228339C
CN1228339C CNB028135210A CN02813521A CN1228339C CN 1228339 C CN1228339 C CN 1228339C CN B028135210 A CNB028135210 A CN B028135210A CN 02813521 A CN02813521 A CN 02813521A CN 1228339 C CN1228339 C CN 1228339C
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CN
China
Prior art keywords
zeolite
catalyst
teda
carried out
piperazine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CNB028135210A
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English (en)
Chinese (zh)
Other versions
CN1524083A (zh
Inventor
M·弗劳恩克朗
B·施泰因
O·朗
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CN1524083A publication Critical patent/CN1524083A/zh
Application granted granted Critical
Publication of CN1228339C publication Critical patent/CN1228339C/zh
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
    • C07D487/08—Bridged systems
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Catalysts (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
CNB028135210A 2001-07-05 2002-07-04 选择性合成三亚乙基二胺的方法 Expired - Lifetime CN1228339C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10132499.5 2001-07-05
DE10132499A DE10132499A1 (de) 2001-07-05 2001-07-05 Verfahren zur selektiven Synthese von Triethylendiamin

Publications (2)

Publication Number Publication Date
CN1524083A CN1524083A (zh) 2004-08-25
CN1228339C true CN1228339C (zh) 2005-11-23

Family

ID=7690641

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB028135210A Expired - Lifetime CN1228339C (zh) 2001-07-05 2002-07-04 选择性合成三亚乙基二胺的方法

Country Status (9)

Country Link
US (1) US6958397B2 (enExample)
EP (1) EP1406904B1 (enExample)
JP (1) JP5073914B2 (enExample)
KR (1) KR20040023639A (enExample)
CN (1) CN1228339C (enExample)
AT (1) ATE341551T1 (enExample)
DE (2) DE10132499A1 (enExample)
ES (1) ES2272786T3 (enExample)
WO (1) WO2003004499A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10326137A1 (de) 2003-06-06 2004-12-23 Basf Ag Verfahren zur Erhöhung der Schneidhärte eines Formkörpers enthaltend ein kristallines Alumosilikat und Verwendung dieser Formkörper mit erhöhter Schneidhärte in chemischen Syntheseverfahren, insbesondere in einem Verfahren zur Herstellung von Triethylendiamin (TEDA) durch Umsetzung von Ethylendiamin (EDA) und/oder Piperazin (PIP)
DE10356184A1 (de) 2003-12-02 2005-07-07 Basf Ag Zeolithisches Material vom Pentasil-Strukturtyp, seine Herstellung und seine Verwendung
DE102004013588A1 (de) * 2004-03-19 2005-10-06 Basf Ag Verfahren zur Herstellung von Triethylendiamin aus Monoethanolamin
DE102004024274A1 (de) * 2004-05-15 2005-12-01 Basf Ag Verfahren zur Herstellung einer Lösung von reinem Triethylendiamin (TEDA)
DE102004029544A1 (de) * 2004-06-18 2006-01-05 Basf Ag Formkörper enthaltend ein mikroporöses Material und mindestens ein siliciumhaltiges Bindemittel, Verfahren zu seiner Herstellung und seine Verwendung als Katalysator, insbesondere in einem Verfahren zur Herstellung von Triethylendiamin (TEDA)
WO2009030649A2 (de) * 2007-09-03 2009-03-12 Basf Se Verfahren zur herstellung von teda-derivaten
DE102009027791B4 (de) 2009-07-17 2013-02-21 Basf Se Zusammensetzung enthaltend Triethylendiamin, Monethylenglykol und Borhydrid
US8440586B2 (en) * 2010-02-26 2013-05-14 Corning Incorporated Low pressure drop extruded catalyst filter
CN108906116B (zh) * 2018-07-18 2021-01-29 西安近代化学研究所 一种用于合成2-甲基三乙烯二胺的催化剂和制备方法及应用
CN115920589B (zh) * 2022-12-21 2023-08-11 可迪尔空气技术（北京）有限公司 一种低浓度污水池废气的处理方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5337876B2 (enExample) * 1973-07-19 1978-10-12
EP0158319A3 (en) * 1984-04-10 1988-05-25 Union Carbide Corporation Synthesis of 1-azabicyclo(2.2.2) octanes or 1,4-diazabicyclo(2-2.2)octanes
US4804758A (en) * 1986-10-08 1989-02-14 Basf Aktiengesellschaft Preparation of 1,4-diazabicyclo[2.2.2]octanes
DE3735214A1 (de) * 1987-10-17 1989-04-27 Huels Chemische Werke Ag Verfahren zur herstellung von 1,4-diazabicyclo(2.2.2)-octan aus piperazin
US5731449A (en) * 1996-09-23 1998-03-24 Air Products And Chemicals, Inc. Triethylendiamine synthesis with base-treated zeolites as catalysts
US5741906A (en) * 1996-11-15 1998-04-21 Air Products And Chemicals, Inc. Production of triethylenediamine using surface acidity deactivated zeolite catalysts
US6084096A (en) * 1998-04-09 2000-07-04 Air Products And Chemicals, Inc. Triethylenediamine and piperazine synthesis using zeolite catalysts modified with a silicon-containing compound

Also Published As

Publication number Publication date
ATE341551T1 (de) 2006-10-15
US20040236106A1 (en) 2004-11-25
US6958397B2 (en) 2005-10-25
DE50208348D1 (de) 2006-11-16
EP1406904A1 (de) 2004-04-14
CN1524083A (zh) 2004-08-25
KR20040023639A (ko) 2004-03-18
DE10132499A1 (de) 2003-01-23
EP1406904B1 (de) 2006-10-04
WO2003004499A1 (de) 2003-01-16
JP2005500324A (ja) 2005-01-06
JP5073914B2 (ja) 2012-11-14
ES2272786T3 (es) 2007-05-01

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Granted publication date: 20051123