ATE341551T1 - Verfahren zur selektiven synthese von triethylendiamin - Google Patents
Verfahren zur selektiven synthese von triethylendiaminInfo
- Publication number
- ATE341551T1 ATE341551T1 AT02782456T AT02782456T ATE341551T1 AT E341551 T1 ATE341551 T1 AT E341551T1 AT 02782456 T AT02782456 T AT 02782456T AT 02782456 T AT02782456 T AT 02782456T AT E341551 T1 ATE341551 T1 AT E341551T1
- Authority
- AT
- Austria
- Prior art keywords
- zeolite
- triethylenediamine
- sub
- selective synthesis
- piperazine
- Prior art date
Links
- IMNIMPAHZVJRPE-UHFFFAOYSA-N triethylenediamine Chemical compound C1CN2CCN1CC2 IMNIMPAHZVJRPE-UHFFFAOYSA-N 0.000 title abstract 4
- 230000015572 biosynthetic process Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 238000003786 synthesis reaction Methods 0.000 title 1
- GLUUGHFHXGJENI-UHFFFAOYSA-N Piperazine Chemical compound C1CNCCN1 GLUUGHFHXGJENI-UHFFFAOYSA-N 0.000 abstract 4
- 239000010457 zeolite Substances 0.000 abstract 4
- 229910021536 Zeolite Inorganic materials 0.000 abstract 3
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 3
- DXOHZOPKNFZZAD-UHFFFAOYSA-N 2-ethylpiperazine Chemical compound CCC1CNCCN1 DXOHZOPKNFZZAD-UHFFFAOYSA-N 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 230000001629 suppression Effects 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
- C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
- C07D487/08—Bridged systems
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/30—After treatment, characterised by the means used
- B01J2229/42—Addition of matrix or binder particles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Catalysts (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10132499A DE10132499A1 (de) | 2001-07-05 | 2001-07-05 | Verfahren zur selektiven Synthese von Triethylendiamin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE341551T1 true ATE341551T1 (de) | 2006-10-15 |
Family
ID=7690641
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT02782456T ATE341551T1 (de) | 2001-07-05 | 2002-07-04 | Verfahren zur selektiven synthese von triethylendiamin |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6958397B2 (enExample) |
| EP (1) | EP1406904B1 (enExample) |
| JP (1) | JP5073914B2 (enExample) |
| KR (1) | KR20040023639A (enExample) |
| CN (1) | CN1228339C (enExample) |
| AT (1) | ATE341551T1 (enExample) |
| DE (2) | DE10132499A1 (enExample) |
| ES (1) | ES2272786T3 (enExample) |
| WO (1) | WO2003004499A1 (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10326137A1 (de) | 2003-06-06 | 2004-12-23 | Basf Ag | Verfahren zur Erhöhung der Schneidhärte eines Formkörpers enthaltend ein kristallines Alumosilikat und Verwendung dieser Formkörper mit erhöhter Schneidhärte in chemischen Syntheseverfahren, insbesondere in einem Verfahren zur Herstellung von Triethylendiamin (TEDA) durch Umsetzung von Ethylendiamin (EDA) und/oder Piperazin (PIP) |
| DE10356184A1 (de) | 2003-12-02 | 2005-07-07 | Basf Ag | Zeolithisches Material vom Pentasil-Strukturtyp, seine Herstellung und seine Verwendung |
| DE102004013588A1 (de) * | 2004-03-19 | 2005-10-06 | Basf Ag | Verfahren zur Herstellung von Triethylendiamin aus Monoethanolamin |
| DE102004024274A1 (de) * | 2004-05-15 | 2005-12-01 | Basf Ag | Verfahren zur Herstellung einer Lösung von reinem Triethylendiamin (TEDA) |
| DE102004029544A1 (de) * | 2004-06-18 | 2006-01-05 | Basf Ag | Formkörper enthaltend ein mikroporöses Material und mindestens ein siliciumhaltiges Bindemittel, Verfahren zu seiner Herstellung und seine Verwendung als Katalysator, insbesondere in einem Verfahren zur Herstellung von Triethylendiamin (TEDA) |
| US20100204438A1 (en) * | 2007-09-03 | 2010-08-12 | Basf Se | Method for producing teda derivatives |
| DE102009027791B4 (de) | 2009-07-17 | 2013-02-21 | Basf Se | Zusammensetzung enthaltend Triethylendiamin, Monethylenglykol und Borhydrid |
| US8440586B2 (en) * | 2010-02-26 | 2013-05-14 | Corning Incorporated | Low pressure drop extruded catalyst filter |
| CN108906116B (zh) * | 2018-07-18 | 2021-01-29 | 西安近代化学研究所 | 一种用于合成2-甲基三乙烯二胺的催化剂和制备方法及应用 |
| CN115920589B (zh) * | 2022-12-21 | 2023-08-11 | 可迪尔空气技术（北京）有限公司 | 一种低浓度污水池废气的处理方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5337876B2 (enExample) * | 1973-07-19 | 1978-10-12 | ||
| JPS60260574A (ja) * | 1984-04-10 | 1985-12-23 | ユニオン・カ−バイド・コ−ポレ−シヨン | １−アザビシクロ〔２．２．２〕オクタン又は１，４−ジアザビシクロ〔２．２．２〕オクタンの合成 |
| US4804758A (en) * | 1986-10-08 | 1989-02-14 | Basf Aktiengesellschaft | Preparation of 1,4-diazabicyclo[2.2.2]octanes |
| DE3735214A1 (de) * | 1987-10-17 | 1989-04-27 | Huels Chemische Werke Ag | Verfahren zur herstellung von 1,4-diazabicyclo(2.2.2)-octan aus piperazin |
| US5731449A (en) * | 1996-09-23 | 1998-03-24 | Air Products And Chemicals, Inc. | Triethylendiamine synthesis with base-treated zeolites as catalysts |
| US5741906A (en) * | 1996-11-15 | 1998-04-21 | Air Products And Chemicals, Inc. | Production of triethylenediamine using surface acidity deactivated zeolite catalysts |
| US6084096A (en) * | 1998-04-09 | 2000-07-04 | Air Products And Chemicals, Inc. | Triethylenediamine and piperazine synthesis using zeolite catalysts modified with a silicon-containing compound |
-
2001
- 2001-07-05 DE DE10132499A patent/DE10132499A1/de not_active Withdrawn
-
2002
- 2002-07-04 JP JP2003510666A patent/JP5073914B2/ja not_active Expired - Fee Related
- 2002-07-04 ES ES02782456T patent/ES2272786T3/es not_active Expired - Lifetime
- 2002-07-04 WO PCT/EP2002/007430 patent/WO2003004499A1/de not_active Ceased
- 2002-07-04 KR KR10-2004-7000036A patent/KR20040023639A/ko not_active Withdrawn
- 2002-07-04 EP EP02782456A patent/EP1406904B1/de not_active Expired - Lifetime
- 2002-07-04 AT AT02782456T patent/ATE341551T1/de not_active IP Right Cessation
- 2002-07-04 DE DE50208348T patent/DE50208348D1/de not_active Expired - Lifetime
- 2002-07-04 CN CNB028135210A patent/CN1228339C/zh not_active Expired - Lifetime
- 2002-07-04 US US10/482,644 patent/US6958397B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1228339C (zh) | 2005-11-23 |
| US6958397B2 (en) | 2005-10-25 |
| DE10132499A1 (de) | 2003-01-23 |
| ES2272786T3 (es) | 2007-05-01 |
| JP2005500324A (ja) | 2005-01-06 |
| EP1406904B1 (de) | 2006-10-04 |
| KR20040023639A (ko) | 2004-03-18 |
| EP1406904A1 (de) | 2004-04-14 |
| US20040236106A1 (en) | 2004-11-25 |
| DE50208348D1 (de) | 2006-11-16 |
| WO2003004499A1 (de) | 2003-01-16 |
| JP5073914B2 (ja) | 2012-11-14 |
| CN1524083A (zh) | 2004-08-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| REN | Ceased due to non-payment of the annual fee |