CN1185968C - Chinese herbal medicine additive in cigarette and its preparing mehtod and use - Google Patents
Chinese herbal medicine additive in cigarette and its preparing mehtod and use Download PDFInfo
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- CN1185968C CN1185968C CNB031402402A CN03140240A CN1185968C CN 1185968 C CN1185968 C CN 1185968C CN B031402402 A CNB031402402 A CN B031402402A CN 03140240 A CN03140240 A CN 03140240A CN 1185968 C CN1185968 C CN 1185968C
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 61
- 241000411851 herbal medicine Species 0.000 title claims abstract description 35
- 239000000654 additive Substances 0.000 title abstract description 12
- 230000000996 additive effect Effects 0.000 title abstract description 12
- 238000002360 preparation method Methods 0.000 claims abstract description 45
- 241000208125 Nicotiana Species 0.000 claims abstract description 44
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 44
- 239000000284 extract Substances 0.000 claims abstract description 34
- 108090000790 Enzymes Proteins 0.000 claims abstract description 32
- 102000004190 Enzymes Human genes 0.000 claims abstract description 32
- 235000000346 sugar Nutrition 0.000 claims abstract description 8
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 64
- 239000000203 mixture Substances 0.000 claims description 38
- 239000003674 animal food additive Substances 0.000 claims description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 238000001914 filtration Methods 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 8
- 238000001556 precipitation Methods 0.000 claims description 7
- 241001016310 Epimedium grandiflorum Species 0.000 claims description 6
- 241000521581 Millettia Species 0.000 claims description 6
- 239000004365 Protease Substances 0.000 claims description 6
- 240000004274 Sarcandra glabra Species 0.000 claims description 6
- 235000010842 Sarcandra glabra Nutrition 0.000 claims description 6
- 235000018905 epimedium Nutrition 0.000 claims description 6
- 238000009472 formulation Methods 0.000 claims description 6
- 239000008361 herbal raw material Substances 0.000 claims description 6
- 229930091371 Fructose Natural products 0.000 claims description 4
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 4
- 239000005715 Fructose Substances 0.000 claims description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 4
- 108091005804 Peptidases Proteins 0.000 claims description 4
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 4
- 240000007164 Salvia officinalis Species 0.000 claims description 4
- SRBFZHDQGSBBOR-LECHCGJUSA-N alpha-D-xylose Chemical compound O[C@@H]1CO[C@H](O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-LECHCGJUSA-N 0.000 claims description 4
- 108010019077 beta-Amylase Proteins 0.000 claims description 4
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 4
- 235000013399 edible fruits Nutrition 0.000 claims description 4
- 239000008103 glucose Substances 0.000 claims description 4
- 235000005412 red sage Nutrition 0.000 claims description 4
- 229960003487 xylose Drugs 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 2
- 235000012907 honey Nutrition 0.000 claims description 2
- 239000011148 porous material Substances 0.000 claims description 2
- 238000011084 recovery Methods 0.000 claims description 2
- 240000006766 Cornus mas Species 0.000 claims 1
- 201000010099 disease Diseases 0.000 abstract description 9
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 9
- 239000003205 fragrance Substances 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 5
- 230000008901 benefit Effects 0.000 abstract description 3
- 239000000796 flavoring agent Substances 0.000 abstract description 3
- 235000019634 flavors Nutrition 0.000 abstract description 3
- 210000004072 lung Anatomy 0.000 abstract description 2
- 230000008569 process Effects 0.000 abstract description 2
- 238000009776 industrial production Methods 0.000 abstract 1
- 229940088598 enzyme Drugs 0.000 description 22
- 235000019441 ethanol Nutrition 0.000 description 21
- 239000007787 solid Substances 0.000 description 9
- 239000000779 smoke Substances 0.000 description 7
- 230000002000 scavenging effect Effects 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 230000008859 change Effects 0.000 description 5
- 230000000391 smoking effect Effects 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 4
- 241000282414 Homo sapiens Species 0.000 description 4
- 241000209020 Cornus Species 0.000 description 3
- 239000004480 active ingredient Substances 0.000 description 3
- 238000005352 clarification Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 235000012343 cottonseed oil Nutrition 0.000 description 3
- 230000009849 deactivation Effects 0.000 description 3
- 230000006837 decompression Effects 0.000 description 3
- 238000005238 degreasing Methods 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 238000000247 postprecipitation Methods 0.000 description 3
- 235000019419 proteases Nutrition 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000000967 suction filtration Methods 0.000 description 3
- 150000008163 sugars Chemical class 0.000 description 3
- 206010061218 Inflammation Diseases 0.000 description 2
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 2
- 210000003734 kidney Anatomy 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 208000023504 respiratory system disease Diseases 0.000 description 2
- 238000005728 strengthening Methods 0.000 description 2
- 108090000270 Ficain Proteins 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 108090000526 Papain Proteins 0.000 description 1
- 206010035664 Pneumonia Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000019836 ficin Nutrition 0.000 description 1
- POTUGHMKJGOKRI-UHFFFAOYSA-N ficin Chemical compound FI=CI=N POTUGHMKJGOKRI-UHFFFAOYSA-N 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000019834 papain Nutrition 0.000 description 1
- 229940055729 papain Drugs 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 208000003265 stomatitis Diseases 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention provides a Chinese herbal medicine additive for cigarettes and a preparation method of the additive. The preparation method comprises the following steps: Chinese herbal medicine extract is prepared; Chinese herbal medicine extract extractum is prepared; tobacco shred enzyme digest is prepared; then, after mixed, the Chinese herbal medicine extract extractum, reducing sugar and the tobacco shred enzyme digest are arranged in a Maillard reaction device, reaction is carried out for 15 to 45 minutes at temperature between 110 DEG C and 128 DEG C, and finally, the Chinese herbal medicine additive for cigarettes is obtained. The preparation method of the present invention has the advantages of simple process and easy industrial production. The prepared Chinese herbal medicine additive has the fragrance of flue-cured tobacco as well as has the special effect of preventing and curing diseases and can relieve damage brought to lung tissue by cigarettes. After the Chinese herbal medicine additive is added to tobacco shreds, the original tobacco flavors of cigarettes are not changed, and cigarettes are easy to accept by smokers.
Description
Technical field
The present invention relates to a kind of cigarette additive, particularly a kind of cigarette Chinese herb feed additive and preparation method thereof.
Background technology
Smoking serious harm human beings'health contains multiple poisonous and harmful substance in cigarette smoke, these materials cause the various diseases of human body easily.Therefore, alleviate smoker's suffered murder by poisoning in smoking process, merit attention as a kind of low toxicity how or few malicious cigarette.In recent years, China's tobacco business constantly proposed galenical is added in the pipe tobacco, particularly added the Chinese herb feed additive that resistance of human body was cured the disease, increased to preventable disease in cigarette, made the smoker can prevent and treat some disease in smoking.The patent No. is 91100109 Chinese invention patent " a kind of cigarette additive and preparation method thereof ", wherein disclose a kind of by hexanol be dissolved in the cigarette additive that the Herb Gynostemmae Pentaphylli extract in the ethanol is formed, this cigarette additive has the special efficacy of preventing and curing diseases, add behind the pipe tobacco this additive to explained hereafter cigarette routinely, make cigarette have some disease of control, as the function of upper respiratory disease.But, after having added this Chinese herb feed additive in the pipe tobacco, because this additive fragrance component separately is difficult to coordinate with the fragrance of pipe tobacco, makes and sneaked into new flavour of a drug in the original smoke of cigarette, thereby had a strong impact on the quality of pipe tobacco and smoker taste cigarette.
Summary of the invention
The objective of the invention is to overcome the shortcoming that prior art exists, provide a kind of and not only have the special efficacy of preventing and curing diseases but also have flue-cured tobacco fragrance, add the preparation method who does not change the cigarette Chinese herb feed additive of the original smoke of cigarette behind the pipe tobacco to.
Another object of the present invention is to provide a kind of cigarette Chinese herb feed additive by method for preparing.
A further object of the present invention is to provide a kind of application of the cigarette Chinese herb feed additive by method for preparing.
Purpose of the present invention is achieved through the following technical solutions: the preparation method of this cigarette Chinese herb feed additive comprises the steps---
(1) preparation Chinese herbal medicine leachate: with the herbal raw material of 100 parts of weight portions, after 500～1000 parts water, 0.01～0.2 part enzyme preparation were mixed, water logging, decoction, removal residue obtained the Chinese herbal medicine leachate; Described herbal raw material is one or more mixtures of loguat leaf, Chloranthus glaber, barrenwort, dogwood fruit, thizoma curculiginis, the red sage root, reticulate millettia;
(2) preparation extracts of Chinese herbal medicine medicinal extract: add ethanol in described Chinese herbal medicine leachate, the weight of described ethanol accounts for 60%～70% of gross weight, and alcohol precipitation, filtration, recovery ethanol, concentrated filtrate obtain extracts of Chinese herbal medicine medicinal extract then;
(3) preparation pipe tobacco enzyme hydrolyzate: with the pipe tobacco butt of 100 parts of weight portions, with after 500～1000 parts water, 0.01～0.2 part enzyme preparation are mixed, water logging, decoction, removal residue, filtering and concentrating obtain the pipe tobacco enzyme hydrolyzate;
(4) the described extracts of Chinese herbal medicine medicinal extract of 100 parts of weight portions, 10～40 parts reduced sugar, 5～10 parts described pipe tobacco enzyme hydrolyzate are mixed after, place the Maillard reaction device, under 110～128 ℃ temperature, reacted 15～45 minutes, and finally obtained the cigarette Chinese herb feed additive.
In the described step (1), various mixtures is equal in weight in the described herbal raw material.
In described step (1) and the step (3), described enzyme preparation is an AMS, or the complex enzyme formulation of AMS, beta amylase, fine little plain enzyme, protease.
In described step (1) and the step (3), described water logging is that mixture was kept under 65～95 ℃ of temperature 15～90 minutes.
In described step (1) and the step (3), described decoction is for being 1～1.5Kg/cm with the mixture pressure after the water logging
2Vapour pressure heating 5～15 minutes.
In the described step (2), the time of described alcohol precipitation is under the normal temperature 4～24 hours.
In the described step (2), the precision of described filtration is pore size filter 4～7 μ m.
In the described step (4), described reduced sugar is one or more in honey, glucose, fructose, the wood sugar.
Preparation method by above-mentioned cigarette Chinese herb feed additive prepares the cigarette Chinese herb feed additive; Prepared cigarette Chinese herb feed additive can be applicable to the production of cigarette, cigarette, pipe tobacco.
The present invention compared with prior art has following advantage and effect: the Chinese herb feed additive of (1) the present invention preparation had both had flue-cured tobacco fragrance, had the beneficial functional of preventing and curing diseases again, can alleviate the infringement of smoking to human lung tissue; (2) do not change the original smoke of cigarette after the Chinese herb feed additive of the present invention's preparation adds pipe tobacco to, make cigarette be easy to be accepted, overcome conventional plant extraction liquid and added the shortcoming that has a strong impact on the pipe tobacco local flavor in the pipe tobacco to by the smoker; (3) the inventive method step of preparation process is simple, is easy to carry out suitability for industrialized production, and economic benefit is obvious, good market prospect.
The specific embodiment
Below in conjunction with embodiment the present invention is done further detailed description, but embodiments of the present invention are not limited thereto.
Embodiment 1
Preparation method's concrete steps of cigarette Chinese herb feed additive of the present invention are as follows:
(1) preparation Chinese herbal medicine leachate: loguat leaf, Chloranthus glaber and the reticulate millettia (wherein the weight ratio of loguat leaf, Chloranthus glaber and reticulate millettia is 1: 1: 1) of 1000 grams are pulverized the back cross 30 mesh sieves, with 6500 the gram the water mixing and stirring after heat, when temperature reaches 50 ℃, in said mixture, add the complex enzyme formulation of 0.5 gram AMS, beta amylase, fine little plain enzyme, protease, continue to be heated to 90 ℃ and under this temperature, kept 40 minutes then; Then said mixture being put into pressure cooker, is 1.5Kg/cm with pressure
2Vapour pressure heating 10 minutes; With mixture centrifugal 15 minutes, remove residue after the cooling, obtain the Chinese herbal medicine leachates of 5000 grams with the 5000rpm rotating speed.
(2) preparation extracts of Chinese herbal medicine medicinal extract: add absolute ethyl alcohol in the Chinese herbal medicine leachate, wherein the weight of ethanol is 65% of gross weight, places room temperature to make its alcohol precipitation in 8 hours said mixture; Post precipitation with the clarification the ethanol scavenging solution with siphonage sucking-off gently, get transparent ethanol scavenging solution with degreasing cottonseed cake suction filtration; Reclaim ethanol 50 ℃ of following decompression distillation, vacuum is concentrated into soluble solid content and reaches 55% then, obtains about 200 gram extract medicinal extract.
(3) preparation pipe tobacco enzyme hydrolyzate: add 5000 gram water in 1000 gram pipe tobacco butts, the complex enzyme formulation of 0.2 gram AMS, beta amylase, fine little plain enzyme, protease is modulated into mixture; This mixture is kept 90 ℃ temperature 40 minutes, leach the active ingredient in the raw material; Then mixture being put into pressure cooker, is 1.5Kg/cm with pressure
2Vapour pressure heating 10 minutes, make enzyme deactivation; Again mixture is cooled off rapidly, with the 5000rpm rotating speed centrifugal 15 minutes, remove residue; It is 45% that the filtration final vacuum is concentrated into solid content, must about 150 milliliters of pipe tobacco hydrolyzates.
(4) adding 50 gram reduced sugars (weight ratio of wood sugar and glucose is 1: 1) and 15 in 200 gram extracts of Chinese herbal medicine medicinal extract, to restrain solid contents be 45% pipe tobacco hydrolyzate, stir and be placed in the Maillard reaction device, reacted 30 minutes down at 121 ℃, obtain about 250 grams at last and have fire-cured tobacco type fragrance, be rich in the cigarette Chinese herb feed additive of effective ingredients in plant.
Prepared cigarette Chinese herb feed additive is sprayed at behind the pipe tobacco explained hereafter cigarette routinely, effect with degraded cigarette toxin, anti-inflammation, symptoms such as, pneumonia many for the upper respiratory disease that causes because of smoking such as stomatitis, phlegm have special efficacy, and do not change the original smoke of cigarette, make cigarette be easy to be accepted by the smoker.
Embodiment 2
Preparation method's concrete steps of cigarette Chinese herb feed additive of the present invention are as follows:
(1) preparation Chinese herbal medicine leachate: barrenwort, dogwood fruit, thizoma curculiginis, the red sage root (wherein the weight of barrenwort, dogwood fruit, thizoma curculiginis, the red sage root is 250 grams) of 1000 grams are pulverized the back and crossed 30 mesh sieves, with 7500 the gram the water mixing and stirring after heat, when temperature reaches 50 ℃, in said mixture, add 0.5 gram AMS, continue to be heated to 90 ℃ and under this temperature, kept 40 minutes then; Then said mixture being put into pressure cooker, is 1.2Kg/cm with pressure
2Vapour pressure heating 10 minutes; With mixture centrifugal 15 minutes, remove residue after the cooling, obtain the Chinese herbal medicine leachates of 6000 grams with the 5000rpm rotating speed.
(2) preparation extracts of Chinese herbal medicine medicinal extract: add absolute ethyl alcohol in the Chinese herbal medicine leachate, wherein the weight of ethanol is 60% of gross weight, places room temperature to make its alcohol precipitation in 8 hours said mixture; Post precipitation with the clarification the ethanol scavenging solution with siphonage sucking-off gently, get transparent ethanol scavenging solution with degreasing cottonseed cake suction filtration; Reclaim ethanol 50 ℃ of following decompression distillation, vacuum is concentrated into soluble solid content and reaches 55% then, obtains about 220 gram extract medicinal extract.
(3) preparation pipe tobacco enzyme hydrolyzate: add 5000 gram water in 1000 gram pipe tobacco butts, 0.2 gram AMS and 0.1 gram papain are modulated into mixture; This mixture is kept 70 ℃ temperature 40 minutes, leach the active ingredient in the raw material; Then mixture being put into pressure cooker, is 1.0Kg/cm with pressure
2Vapour pressure heating 10 minutes, make enzyme deactivation; Again mixture is cooled off rapidly, with the 5000rpm rotating speed centrifugal 15 minutes, remove residue; It is 45% that the filtration final vacuum is concentrated into solid content, must about 150 milliliters of pipe tobacco hydrolyzates.
(4) adding 50 gram reduced sugars (weight ratio of fructose and glucose is 1: 1) and 15 in 200 gram extracts of Chinese herbal medicine medicinal extract, to restrain solid contents be 45% pipe tobacco hydrolyzate, stir and be placed in the Maillard reaction device, reacted 40 minutes down at 115 ℃, obtain about 250 grams at last and have fire-cured tobacco type fragrance, be rich in the cigarette Chinese herb feed additive of effective ingredients in plant.
Prepared cigarette Chinese herb feed additive is sprayed at behind the pipe tobacco explained hereafter cigarette routinely, has the effect of tonifying kidney and strengthening yang, and do not change the original smoke of cigarette, make cigarette be easy to be accepted by the smoker.
Embodiment 3
Preparation method's concrete steps of cigarette Chinese herb feed additive of the present invention are as follows:
(1) preparation Chinese herbal medicine leachate: loguat leaf, Chloranthus glaber, reticulate millettia and the barrenwort (wherein the weight of loguat leaf, Chloranthus glaber, reticulate millettia and barrenwort is 250 grams) of 1000 grams are pulverized the back cross 30 mesh sieves, with 6000 the gram the water mixing and stirring after heat, when temperature reaches 50 ℃, in said mixture, add the complex enzyme formulation of 0.5 gram AMS and the fine little plain enzyme of 0.1 gram, continue to be heated to 80 ℃ and under this temperature, kept 40 minutes then; Then said mixture being put into pressure cooker, is 1.5Kg/cm with pressure
2Vapour pressure heating 5 minutes; With mixture centrifugal 15 minutes, remove residue after the cooling, obtain the Chinese herbal medicine leachates of 4500 grams with the 5000rpm rotating speed.
(2) preparation extracts of Chinese herbal medicine medicinal extract: add absolute ethyl alcohol in the Chinese herbal medicine leachate, wherein the weight of ethanol is 60% of gross weight, places room temperature to make its alcohol precipitation in 8 hours said mixture; Post precipitation with the clarification the ethanol scavenging solution with siphonage sucking-off gently, get transparent ethanol scavenging solution with degreasing cottonseed cake suction filtration; Reclaim ethanol 50 ℃ of following decompression distillation, vacuum is concentrated into soluble solid content and reaches 55% then, obtains about 190 gram extract medicinal extract.
(3) preparation pipe tobacco enzyme hydrolyzate: add 5000 gram water in 1000 gram pipe tobacco butts, the complex enzyme formulation of 0.2 gram AMS, the fine little plain enzyme of 0.1 gram and 0.1 gram ficin is modulated into mixture; This mixture is kept 65 ℃ temperature 40 minutes, leach the active ingredient in the raw material; Then mixture being put into pressure cooker, is 1.5Kg/cm with pressure
2Vapour pressure heating 5 minutes, make enzyme deactivation; Again mixture is cooled off rapidly, with the 5000rpm rotating speed centrifugal 15 minutes, remove residue; It is 45% that the filtration final vacuum is concentrated into solid content, must about 150 milliliters of pipe tobacco hydrolyzates.
(4) adding 50 gram reduced sugars (weight ratio of wood sugar and fructose is 1: 2) and 15 in 200 gram extracts of Chinese herbal medicine medicinal extract, to restrain solid contents be 45% pipe tobacco hydrolyzate, stir and be placed in the Maillard reaction device, reacted 25 minutes down at 125 ℃, obtain about 250 grams at last and have fire-cured tobacco type fragrance, be rich in the cigarette Chinese herb feed additive of effective ingredients in plant.
Prepared cigarette Chinese herb feed additive is sprayed at behind the pipe tobacco explained hereafter cigarette routinely, has the effect of anti-inflammation and tonifying kidney and strengthening yang, and do not change the original smoke of cigarette, make cigarette be easy to be accepted by the smoker.
Claims (9)
1, a kind of preparation method of cigarette Chinese herb feed additive is characterized in that comprising the steps:
(1) preparation Chinese herbal medicine leachate: with the herbal raw material of 100 parts of weight portions, after 500～1000 parts water, 0.01～0.2 part enzyme preparation were mixed, water logging, decoction, removal residue obtained the Chinese herbal medicine leachate; Described herbal raw material is one or more mixtures of loguat leaf, Chloranthus glaber, barrenwort, dogwood fruit, thizoma curculiginis, the red sage root, reticulate millettia;
(2) preparation extracts of Chinese herbal medicine medicinal extract: add ethanol in described Chinese herbal medicine leachate, the weight of described ethanol accounts for 60%～70% of gross weight, and alcohol precipitation, filtration, recovery ethanol, concentrated filtrate obtain extracts of Chinese herbal medicine medicinal extract then;
(3) preparation pipe tobacco enzyme hydrolyzate: with the pipe tobacco butt of 100 parts of weight portions, with after 500～1000 parts water, 0.01～0.2 part enzyme preparation are mixed, water logging, decoction, removal residue, filtering and concentrating obtain the pipe tobacco enzyme hydrolyzate;
(4) the described extracts of Chinese herbal medicine medicinal extract of 100 parts of weight portions, 10～40 parts reduced sugar, 5～10 parts described pipe tobacco enzyme hydrolyzate are mixed after, place the Maillard reaction device, under 110～128 ℃ temperature, reacted 15～45 minutes, and obtained the cigarette Chinese herb feed additive.
2, the preparation method of cigarette Chinese herb feed additive according to claim 1 is characterized in that: in the described step (1), various mixtures is equal in weight in the described herbal raw material.
3, the preparation method of cigarette Chinese herb feed additive according to claim 1, it is characterized in that: in described step (1) and the step (3), described enzyme preparation is an AMS, or the complex enzyme formulation of AMS, beta amylase, fine little plain enzyme, protease.
4, the preparation method of cigarette Chinese herb feed additive according to claim 1 is characterized in that: in described step (1) and the step (3), described water logging is that mixture was kept under 65～95 ℃ of temperature 15～90 minutes.
5, the preparation method of cigarette Chinese herb feed additive according to claim 1 is characterized in that: in described step (1) and the step (3), described decoction is for being 1～1.5Kg/cm with the mixture pressure after the water logging
2Vapour pressure heating 5～15 minutes.
6, the preparation method of cigarette Chinese herb feed additive according to claim 1 is characterized in that: in the described step (2), the time of described alcohol precipitation is under the normal temperature 4～24 hours.
7, the preparation method of cigarette Chinese herb feed additive according to claim 1 is characterized in that: in the described step (2), the precision of described filtration is pore size filter 4～7 μ m.
8, the preparation method of cigarette Chinese herb feed additive according to claim 1 is characterized in that: in the described step (4), described reduced sugar is one or more in honey, glucose, fructose, the wood sugar.
9, a kind of cigarette Chinese herb feed additive that adopts each described method preparation of claim 1～8.
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| CNB031402402A CN1185968C (en) | 2003-08-22 | 2003-08-22 | Chinese herbal medicine additive in cigarette and its preparing mehtod and use |
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| CNB031402402A CN1185968C (en) | 2003-08-22 | 2003-08-22 | Chinese herbal medicine additive in cigarette and its preparing mehtod and use |
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| CN1491596A CN1491596A (en) | 2004-04-28 |
| CN1185968C true CN1185968C (en) | 2005-01-26 |
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Cited By (1)
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| CN101579146B (en) * | 2008-05-12 | 2012-07-04 | 湖北中烟工业有限责任公司 | Method for preparing tobacco flavor by Maillard reaction of nitrogen source and sugar source |
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| CN103113989B (en) * | 2013-03-07 | 2014-02-26 | 华宝食用香精香料（上海）有限公司 | Tobacco essence capable of improving cigarette taste and aroma |
| CN104419522A (en) * | 2013-08-28 | 2015-03-18 | 江西中烟工业有限责任公司 | Preparation method of Maillard reaction flavor for cigarettes with medicinal herb fragrance characteristics |
| CN104498184A (en) * | 2014-11-20 | 2015-04-08 | 湖北中烟工业有限责任公司 | Preparation method for tobacco flavor by utilizing fragrant honey in Maillard reaction |
| CN108158030B (en) * | 2017-12-28 | 2020-06-02 | 江西中烟工业有限责任公司 | Extraction method of compound traditional Chinese medicine extract and application of compound traditional Chinese medicine extract in cigarettes |
| CN110791387A (en) * | 2019-11-12 | 2020-02-14 | 四川中烟工业有限责任公司 | Maillard reactant of bamboo fungus for cigarettes as well as preparation method and application of Maillard reactant |
-
2003
- 2003-08-22 CN CNB031402402A patent/CN1185968C/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101579146B (en) * | 2008-05-12 | 2012-07-04 | 湖北中烟工业有限责任公司 | Method for preparing tobacco flavor by Maillard reaction of nitrogen source and sugar source |
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