CN117357425A - Fragrance composition with long-lasting fragrance, preparation method thereof and application thereof in cosmetics - Google Patents
Fragrance composition with long-lasting fragrance, preparation method thereof and application thereof in cosmetics Download PDFInfo
- Publication number
- CN117357425A CN117357425A CN202311592568.2A CN202311592568A CN117357425A CN 117357425 A CN117357425 A CN 117357425A CN 202311592568 A CN202311592568 A CN 202311592568A CN 117357425 A CN117357425 A CN 117357425A
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- Prior art keywords
- beta
- sheet
- fibroin
- cosmetic
- fragrance
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- Pending
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 53
- 239000003205 fragrance Substances 0.000 title claims abstract description 48
- 239000002537 cosmetic Substances 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- 230000005923 long-lasting effect Effects 0.000 title claims description 7
- 108010022355 Fibroins Proteins 0.000 claims abstract description 43
- 125000003118 aryl group Chemical group 0.000 claims abstract description 40
- 239000000126 substance Substances 0.000 claims abstract description 35
- 239000000341 volatile oil Substances 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 5
- 239000003921 oil Substances 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 239000000839 emulsion Substances 0.000 claims description 3
- 239000000243 solution Substances 0.000 abstract description 27
- 239000000463 material Substances 0.000 abstract description 6
- 230000002045 lasting effect Effects 0.000 abstract description 5
- 238000013329 compounding Methods 0.000 abstract description 2
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000005728 strengthening Methods 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 24
- 239000000686 essence Substances 0.000 description 16
- 238000012360 testing method Methods 0.000 description 10
- 238000005303 weighing Methods 0.000 description 8
- 239000006071 cream Substances 0.000 description 4
- 241000021559 Dicerandra Species 0.000 description 3
- 235000010654 Melissa officinalis Nutrition 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000865 liniment Substances 0.000 description 3
- 230000014759 maintenance of location Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000002775 capsule Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000002502 liposome Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003094 microcapsule Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 210000000707 wrist Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
Abstract
The invention relates to the technical field of cosmetics, in particular to a lasting fragrance composition, a preparation method and application thereof in cosmetics, and the technical scheme is characterized by comprising the following components in percentage by mass: 10-80% of beta-sheet fibroin solution, and the balance of aromatic substances; wherein the concentration of the beta-sheet fibroin in the beta-sheet fibroin solution is 0.2-10%, and the aromatic substance comprises at least one of essence and essential oil. The aromatic substance composition is prepared by compounding the beta-sheet fibroin aqueous solution and the aromatic substances, has the advantages of strengthening aroma, prolonging the duration of the aroma, reducing the volatility of materials and being simple in preparation process, and has wide application range.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a fragrance composition capable of lasting fragrance, and preparation and application thereof in cosmetics.
Background
The essence is a mixture prepared by manual work and containing more than two or even tens of flavors (sometimes containing proper solvents or carriers), has a certain fragrance, and is widely applied to daily cosmetics such as perfumes, skin care products, washing and caring products and the like to mask the smell of the raw materials and bring pleasant feeling to consumers.
In the cosmetic field, cosmetics having pleasant smell are increasingly popular today while pursuing skin feel and efficacy. All brands strive to improve the quality of the fragrance, but the storage and transportation and high temperature conditions accelerate the volatilization of volatile components in cosmetics, so that the fragrance of the essence is weakened, and the fragrance retention time of the essence is shortened.
The prior art mainly adopts the modes of adding high molecular polymer, increasing the dosage of film forming agent, adopting microcapsule and liposome encapsulation, and the like to solve the problems, and prolonging the fragrance retention time. However, the above-described technique has the following drawbacks: the capsule and liposome preparation technology is complex, and the durability of the capsule is poor; the use amount of the film forming agent is increased, so that the problems of poor skin feel, difficult smearing and the like are easily caused.
Disclosure of Invention
Aiming at the defects existing in the prior art, the invention aims to provide a fragrance composition capable of lasting fragrance, and preparation and application thereof in cosmetics, and the fragrance composition has the advantages of reducing material volatility and prolonging fragrance duration.
The technical aim of the invention is achieved by the following technical scheme, namely a fragrance composition capable of lasting fragrance, which comprises the following components: 10-80% of beta-sheet fibroin solution, and the balance of aromatic substances;
wherein the concentration of the beta-sheet fibroin in the beta-sheet fibroin solution is 0.2-10%, and the aromatic substance comprises at least one of essence and essential oil.
In one embodiment, the beta-sheet fibroin has a length of 20-4000nm and a diameter of 5-30nm.
In one embodiment, the beta-sheet content of the beta-sheet fibroin is greater than or equal to 30%.
In one embodiment, the beta-sheet fibroin solution is 11-67% by mass.
The preparation method of the aromatic substance composition comprises the following steps: and (3) obtaining a beta-sheet fibroin solution and aromatic substances, adding the aromatic substances into the beta-sheet fibroin solution, and uniformly stirring and mixing to obtain a target product.
The use of the above fragrance composition in the preparation of cosmetics.
A cosmetic comprises the above aromatic composition.
In one embodiment, the cosmetic is an emulsified cosmetic comprising any one of an oil-in-water structure, a water-in-oil structure, and a multiple emulsion structure.
In one embodiment, the fragrance composition is present in the cosmetic in an amount of 0.01 to 20% by mass.
In one embodiment, the fragrance composition is present in the cosmetic in an amount of 0.1 to 10% by mass.
The fragrance composition capable of lasting fragrance and the preparation and application thereof in cosmetics have the following beneficial effects:
firstly, the beta-sheet fibroin solution and aromatic substances are compounded to prepare the aromatic substance composition, so that the fragrance can be enhanced and the duration of the fragrance can be prolonged;
secondly, the invention utilizes the beta-sheet structure of the beta-sheet fibroin to absorb and slowly release aromatic substances, thereby further reducing the volatility of materials and improving the experience of users;
thirdly, the preparation process is simple, the beta-sheet fibroin solution and the aromatic substances are uniformly mixed to be applied to the cosmetic base stock, and the preparation process does not involve complex preparation processes and has wide application range.
Drawings
FIG. 1 is a graph showing the volatilization quality of application example 1 and comparative example 1;
fig. 2 is a graph of volatilization quality of application example 2 and comparative example 2.
Detailed Description
The present invention will be described in further detail with reference to the following examples, which are intended to facilitate the understanding of the present invention without any limitation thereto. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. In case of conflict, the present specification, definitions, will control.
The term "prepared from …" as used herein is synonymous with "comprising". The terms "comprising," "including," "having," "containing," or any other variation thereof, as used herein, are intended to cover a non-exclusive inclusion. For example, a composition, step, method, article, or apparatus that comprises a list of elements is not necessarily limited to only those elements but may include other elements not expressly listed or inherent to such composition, step, method, article, or apparatus.
The conjunction "consisting of …" excludes any unspecified element, step or component. If used in a claim, such phrase will cause the claim to be closed, such that it does not include materials other than those described, except for conventional impurities associated therewith. When the phrase "consisting of …" appears in a clause of the claim body, rather than immediately following the subject, it is limited to only the elements described in that clause; other elements are not excluded from the stated claims as a whole.
When an equivalent, concentration, or other value or parameter is expressed as a range, preferred range, or a range bounded by a list of upper preferable values and lower preferable values, this is to be understood as specifically disclosing all ranges formed from any pair of any upper range limit or preferred value and any lower range limit or preferred value, regardless of whether ranges are separately disclosed. For example, when ranges of "1 to 5" are disclosed, the described ranges should be construed to include ranges of "1 to 4", "1 to 3", "1 to 2 and 4 to 5", "1 to 3 and 5", and the like. When a numerical range is described herein, unless otherwise indicated, the range is intended to include its endpoints and all integers and fractions within the range.
The present invention will be described in detail below with reference to the accompanying drawings and examples.
A long lasting fragrance composition comprising: 10-80% of beta-sheet fibroin solution, and the balance of aromatic substances;
wherein the concentration of beta-sheet fibroin in the beta-sheet fibroin solution is 0.2-10%, and the aromatic substance comprises at least one of essence and essential oil.
In practical application, when the concentration of the solution of the beta-pleated silk protein is equal to or more than 2%, the solution is gel, and the aromatic substance can be single essence, single essential oil, a mixture of multiple essences, a mixture of multiple essential oils or a mixture of the essences and the essential oils. The invention prepares the aromatic substance composition by compounding the beta-sheet fibroin solution and the aromatic substances, and can strengthen the fragrance and increase the duration of the fragrance; in addition, the invention utilizes the beta-sheet structure of the beta-sheet fibroin to absorb and slowly release aromatic substances, thereby further reducing the volatility of materials and improving the experience of users.
Specifically, the length of the beta-sheet fibroin is 20-4000nm, and the diameter is 5-30nm.
Further, the beta-sheet content of the beta-sheet fibroin is greater than or equal to 30%.
Further, the mass percentage of the beta-sheet fibroin solution is 11-67%.
A method of preparing a fragrance composition comprising the steps of: and (3) obtaining a beta-sheet fibroin solution and aromatic substances, adding the aromatic substances into the beta-sheet fibroin solution, and uniformly stirring and mixing to obtain a target product.
In actual production, the two raw materials are mixed according to different proportions at normal temperature to obtain a uniform mixture, namely the target product. Depending on the mixing ratio, the mixture exhibits a translucent or opaque appearance. The preparation process of the aromatic substance composition is simple, the aromatic substance composition is obtained by uniformly mixing the beta-sheet fibroin solution and the aromatic substances, the complex preparation process is not involved, and the popularization is convenient.
Use of a fragrance composition in the preparation of a cosmetic. After the cosmetic base stock is prepared, the aromatic substance composition is added into the cosmetic base stock at normal temperature, and the steps of flavoring and mixing are completed after the aromatic substance composition is stirred and mixed uniformly, so that the method does not involve a complex adding process and has wide application range.
A cosmetic comprises the above aromatic composition.
Specifically, the cosmetic is an emulsified cosmetic comprising any one of an oil-in-water structure, a water-in-oil structure and a multiple emulsion structure.
Specifically, the aromatic composition is contained in the cosmetic in an amount of 0.01-20% by mass.
Further, the aromatic composition is contained in the cosmetic in an amount of 0.1-10% by mass.
Example 1
The present example provides a fragrance composition comprising 50% beta-sheet fibroin solution and 50% daily flavor, wherein the concentration of the beta-sheet fibroin solution is 0.5%.
The preparation method of this example is as follows: weighing beta-sheet fibroin solution and daily essence according to a proportion, adding the daily essence into the beta-sheet fibroin solution, and stirring for 3min at 25 ℃ and a rotating speed of 3000r/min to obtain a semitransparent mixture, namely the aromatic substance composition.
Example 2
The present example provides a fragrance composition comprising 50% beta-sheet fibroin solution and 50% daily flavor, wherein the concentration of the beta-sheet fibroin solution is 2%.
The preparation method of this example is the same as that of example 1.
Example 3
The embodiment provides an aromatic substance composition, which comprises 20% of beta-sheet fibroin solution and 80% of daily essence, wherein the concentration of the beta-sheet fibroin solution is 0.5%.
The preparation method of this example is the same as that of example 1.
Application example 1 and comparative example 1
Application example 1 and comparative example 1 respectively provide an oil-in-water type cream comprising the components in mass percentages shown in the following table, and application example 1 differs from comparative example 1 in that: application example 1 used a fragrance composition having 2% of example 1, and comparative example 1 used a daily essence having 1%, and the daily essence in example 1 was the same essence as that in comparative example 1, and the actual amounts of the daily essences in application example 1 and comparative example 1 were the same.
TABLE 1
The preparation steps of application example 1 and comparative example 1 are:
s1, weighing the phase A according to a proportion, stirring to dissolve raw materials, and heating to 75 ℃ for later use;
s2, weighing the phase B according to a proportion, uniformly mixing, and heating to 75 ℃ for later use;
s3, weighing the phase C according to a proportion, uniformly mixing, heating to 75 ℃, adding the standby phase A and phase B into the phase C, and homogenizing for 8min under the condition of 5000 rpm;
s4, weighing the phase D in proportion, adding the phase D into the mixture obtained in the step S3, and homogenizing for 2min under the condition of 5000 rpm;
s5, cooling the mixed solution obtained in the step S4 to 30-35 ℃, adding the E phase, and uniformly mixing to obtain a target product.
Application example 2 and comparative example 2
Example 2 and comparative example 2 each provide a water-in-oil type balm comprising the components in the mass percentages shown in the following table, the difference between application example 2 and comparative example 2 being that: application example 2 used a fragrance composition having 9.8% of example 3, whereas comparative example 2 used a daily fragrance having 7.84%, and the daily fragrance of example 3 was the same fragrance as that of comparative example 2, and the actual amounts of the daily fragrances of application example 2 and comparative example 2 were the same.
TABLE 2
The preparation steps of application example 2 and comparative example 2 are:
s1, weighing the phase A according to a proportion, and uniformly mixing for later use;
s2, weighing the phase B according to a proportion, adding the phase B into the phase A, and uniformly mixing;
s3, weighing the phase C according to a proportion, adding the phase C into the mixture obtained in the step S2, and continuously and uniformly mixing to obtain a target product.
Test 1: volatilization test
The testing method comprises the following steps: the creams of application example 1 and comparative example 1 were taken at 6g each, the balms of application example 2 and comparative example 2 were taken at 5g each, and the resultant was tested in an oven at 50℃for 12 hours in synchronization, and the mass volatilization was measured every 2 hours, and the results were recorded and plotted.
Test results: as shown in fig. 1 and 2, the black line of fig. 1 is a comparative example 1 test sample, and the gray line is an application example 1 test sample; the black lines in fig. 2 are comparative example 2 test samples, and the gray lines are application example 2 test samples. Under the condition that the actual content of the daily essence is the same, the quality loss of the cosmetics added with the aromatic substance composition is less, which indicates that the beta-sheet fibroin solution is helpful for reducing the volatilization of materials.
Test 2: volatilization test
The creams of the same amount of application example 1 and comparative example 1 were taken and respectively coated on the positions where the two sides of the arm are not easy to contact, and the comparison was performed after 2 hours. The cream of application example 1 was more aromatic, and was longer in fragrance retention time and more skin-friendly than comparative example 1.
The balms of application example 2 and comparative example 2 were taken in equal amounts, respectively applied to both sides of the wrist, and compared after 2 hours. Compared with comparative example 2, the fragrance of application example 2 is more obvious, the touch feeling is smoother, and the fragrance is more durable.
The foregoing examples illustrate only a few embodiments of the invention and are described in detail herein without thereby limiting the scope of the invention. It should be noted that it will be apparent to those skilled in the art that several variations and modifications can be made without departing from the spirit of the invention, which are all within the scope of the invention. Accordingly, the scope of protection of the present invention is to be determined by the appended claims.
Claims (10)
1. A long lasting fragrance composition, comprising the following components in mass percent: 10-80% of beta-sheet fibroin solution, and the balance of aromatic substances;
wherein the concentration of the beta-sheet fibroin in the beta-sheet fibroin solution is 0.2-10%, and the aromatic substance comprises at least one of essence and essential oil.
2. A long lasting fragrance composition according to claim 1, wherein: the length of the beta-folded fibroin is 20-4000nm, and the diameter is 5-30nm.
3. A long lasting fragrance composition according to claim 2, wherein: the content of beta-sheet in the beta-sheet fibroin is more than or equal to 30%.
4. A long lasting fragrance composition according to claim 3, wherein: the mass percentage of the beta-sheet fibroin solution is 11-67%.
5. A method of preparing a fragrance composition according to any one of claims 1 to 4, comprising the steps of: and (3) obtaining a beta-sheet fibroin solution and aromatic substances, adding the aromatic substances into the beta-sheet fibroin solution, and uniformly stirring and mixing to obtain a target product.
6. Use of a fragrance composition according to any one of claims 1 to 4 for the preparation of a cosmetic product.
7. A cosmetic product, characterized in that it comprises the fragrance composition according to any one of claims 1 to 4.
8. The cosmetic according to claim 7, wherein the cosmetic is an emulsified cosmetic comprising any one of an oil-in-water structure, a water-in-oil structure, and a multiple emulsion structure.
9. The cosmetic product according to claim 7, wherein: the aromatic substance composition accounts for 0.01-20wt% of the cosmetic.
10. The cosmetic product according to claim 9, characterized in that: the aromatic substance composition accounts for 0.1-10wt% of the cosmetic.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311592568.2A CN117357425A (en) | 2023-11-27 | 2023-11-27 | Fragrance composition with long-lasting fragrance, preparation method thereof and application thereof in cosmetics |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311592568.2A CN117357425A (en) | 2023-11-27 | 2023-11-27 | Fragrance composition with long-lasting fragrance, preparation method thereof and application thereof in cosmetics |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN117357425A true CN117357425A (en) | 2024-01-09 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202311592568.2A Pending CN117357425A (en) | 2023-11-27 | 2023-11-27 | Fragrance composition with long-lasting fragrance, preparation method thereof and application thereof in cosmetics |
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| CN113749977A (en) * | 2021-09-24 | 2021-12-07 | 安徽华业香料合肥有限公司 | A hair treatment perfume composition with lasting fragrance |
| CN116919845A (en) * | 2023-08-30 | 2023-10-24 | 美尚(广州)化妆品股份有限公司 | Fibroin sun cream and preparation method thereof |
| CN116942553A (en) * | 2023-08-30 | 2023-10-27 | 美尚(广州)化妆品股份有限公司 | Make-up composition containing beta-folded fibroin |
| CN117064784A (en) * | 2023-08-30 | 2023-11-17 | 美尚(广州)化妆品股份有限公司 | Anhydrous cosmetic containing beta-folded fibroin and preparation method thereof |
| CN117084931A (en) * | 2023-08-30 | 2023-11-21 | 美尚(广州)化妆品股份有限公司 | Fibroin-containing powder composition and preparation method thereof |
-
2023
- 2023-11-27 CN CN202311592568.2A patent/CN117357425A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113749977A (en) * | 2021-09-24 | 2021-12-07 | 安徽华业香料合肥有限公司 | A hair treatment perfume composition with lasting fragrance |
| CN116919845A (en) * | 2023-08-30 | 2023-10-24 | 美尚(广州)化妆品股份有限公司 | Fibroin sun cream and preparation method thereof |
| CN116942553A (en) * | 2023-08-30 | 2023-10-27 | 美尚(广州)化妆品股份有限公司 | Make-up composition containing beta-folded fibroin |
| CN117064784A (en) * | 2023-08-30 | 2023-11-17 | 美尚(广州)化妆品股份有限公司 | Anhydrous cosmetic containing beta-folded fibroin and preparation method thereof |
| CN117084931A (en) * | 2023-08-30 | 2023-11-21 | 美尚(广州)化妆品股份有限公司 | Fibroin-containing powder composition and preparation method thereof |
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