KR102579965B1 - Perfume composition for expressing the fragrance of bugleweed clove fennel aroma tea - Google Patents

Perfume composition for expressing the fragrance of bugleweed clove fennel aroma tea Download PDF

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KR102579965B1
KR102579965B1 KR1020210015530A KR20210015530A KR102579965B1 KR 102579965 B1 KR102579965 B1 KR 102579965B1 KR 1020210015530 A KR1020210015530 A KR 1020210015530A KR 20210015530 A KR20210015530 A KR 20210015530A KR 102579965 B1 KR102579965 B1 KR 102579965B1
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weight
fragrance
composition
fragrance composition
tea
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KR20220112035A (en
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박소라
고은성
장윤미
이은혜
우창식
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한국콜마주식회사
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0061Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35Ketones, e.g. benzophenone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0007Aliphatic compounds
    • C11B9/0015Aliphatic compounds containing oxygen as the only heteroatom
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0026Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0034Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0042Essential oils; Perfumes compounds containing condensed hydrocarbon rings
    • C11B9/0046Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings

Abstract

본 발명은 어진향차의 향취를 재현한 향료 조성물에 관한 것이다.The present invention relates to a fragrance composition that reproduces the fragrance of royal tea.

Description

어진향차 향취 재현 향료 조성물{Perfume composition for expressing the fragrance of bugleweed clove fennel aroma tea}Perfume composition for expressing the fragrance of bugleweed clove fennel aroma tea}

본 발명은 향료 조성물에 관한 것으로, 보다 상세하게는 어진향차의 향취를 재현한 향료 조성물에 관한 것이다.The present invention relates to a fragrance composition, and more specifically, to a fragrance composition that reproduces the fragrance of royal tea.

식품, 의약품, 생활용품 및 화장품 등의 소비재에는 다양한 향의 향료 조성물이 첨가되고 있고, 천연 성분을 선호하는 소비자의 기호에 맞춰 천연 유래의 향료를 사용하는 경향이 증가하고 있다. 천연 향료 조성물로서 천연 물질로부터 채취된 물질을 사용하는 경우도 있으나, 천연 물질의 종류에 따라 채취량에 한계가 있으며, 향기의 강도 및 지속성이 떨어진다는 문제가 있다. 이에 화합물의 적절한 배합을 통해 천연 물질의 향취를 재현하는 조성물에 대한 연구, 개발이 활발히 진행되고 있다.Fragrance compositions with various scents are being added to consumer goods such as food, medicine, household goods, and cosmetics, and the tendency to use natural fragrances in line with the preferences of consumers who prefer natural ingredients is increasing. There are cases where materials collected from natural materials are used as natural fragrance compositions, but there is a limit to the amount collected depending on the type of natural material, and there is a problem that the intensity and sustainability of the scent is low. Accordingly, research and development on compositions that reproduce the scent of natural substances through appropriate mixing of compounds are actively underway.

한편, 체취를 마스킹하기 위한 용도로 향이 좋은 향수나 바디 제품 등의 화장품을 사용하기도 하나, 이는 근본적으로 체취를 개선하는 것이 아니라 일시적으로 체취를 가리는 방법에 지나지 않으며, 시간이 지나면 다시 체취가 날뿐더러 체취와 향취가 섞여서 더 역한 향취를 발향하는 문제가 있다. 따라서, 체취 개선에 효과적인 향료 조성물에 대한 요구가 있다. On the other hand, cosmetics such as scented perfume or body products may be used to mask body odor, but this does not fundamentally improve body odor, but is only a way to temporarily mask body odor, and over time, the body odor will return. There is a problem where body odor and dreadlocks mix, creating a more unpleasant scent. Therefore, there is a need for a fragrance composition that is effective in improving body odor.

본 발명은 어진향차의 향취를 재현한 향료 조성물을 제공한다. 또한, 본 발명은 상기 향료 조성물을 포함하는 피부 외용제 조성물 및 건강기능식품을 제공한다.The present invention provides a fragrance composition that reproduces the scent of traditional Chinese tea. Additionally, the present invention provides a composition for topical skin application and a health functional food containing the above-described fragrance composition.

본 발명에 따른 향료 조성물은 리모넨(LIMONENE), 시트럴(CITRAL), 캠퍼(CAMPHOR), 유제놀(EUGENOL), 이소유제놀(ISO EUGENOL), 리날로올(LINALOOL), 메틸 벤조에이트(METHYL BENZOATE), 베타-카리오필렌(BETA-CARYOPHYLLENE), 아네톨(ANETHOLE) 및 카르본(CARVONE)을 포함한다.The fragrance composition according to the present invention includes LIMONENE, CITRAL, CAMPHOR, EUGENOL, ISO EUGENOL, LINALOOL, and METHYL BENZOATE. ), beta-CARYOPHYLLENE, ANETHOLE and CARVONE.

본 발명에 따른 향료 조성물은 어진향차의 향취를 재현한 것으로, 체취 개선에 효과적이다. 본 발명에 따른 향료 조성물은 어진향차의 향취를 그대로 재현하는 동시에, 기호성이 좋으면서도 체취 개선에 효과적인 향료 원료를 추가로 배합할 수 있어, 더욱 효과적이고 지속적으로 체취를 개선하는 효과를 갖는다.The fragrance composition according to the present invention reproduces the fragrance of ginseng tea and is effective in improving body odor. The fragrance composition according to the present invention reproduces the scent of gin-scented tea as it is, and at the same time, it can additionally contain fragrance raw materials that are good in palatability and are effective in improving body odor, so it has the effect of improving body odor more effectively and continuously.

이하, 본 발명에 대하여 설명한다. 그러나, 하기 내용에 의해서만 한정되는 것은 아니며, 필요에 따라 각 구성요소가 다양하게 변형되거나 선택적으로 혼용될 수 있다. 따라서, 본 발명의 사상 및 기술범위에 포함되는 모든 변경, 균등물 내지 대체물을 포함하는 것으로 이해되어야 한다.Hereinafter, the present invention will be described. However, it is not limited to the following content, and each component may be variously modified or selectively mixed as needed. Accordingly, it should be understood to include all changes, equivalents, and substitutes included in the spirit and technical scope of the present invention.

본 발명에 따른 향료 조성물은 리모넨(LIMONENE), 시트럴(CITRAL), 캠퍼(CAMPHOR), 유제놀(EUGENOL), 이소유제놀(ISO EUGENOL), 리날로올(LINALOOL), 메틸 벤조에이트(METHYL BENZOATE), 베타-카리오필렌(BETA-CARYOPHYLLENE), 아네톨(ANETHOLE) 및 카르본(CARVONE)을 주요 향취 성분으로 포함한다.The fragrance composition according to the present invention includes LIMONENE, CITRAL, CAMPHOR, EUGENOL, ISO EUGENOL, LINALOOL, and METHYL BENZOATE. ), BETA-CARYOPHYLLENE, ANETHOLE and CARVONE as the main fragrance ingredients.

상기 주요 향취 성분의 함량은 특별히 제한되지 않으나, 향료 조성물 총 중량을 기준으로, 리모넨 1 내지 5 중량%, 예를 들어 1.5 내지 2.5 중량%, 시트럴 0.2 내지 5 중량%, 예를 들어 0.5 내지 1.5 중량%, 캠퍼 1 내지 10 중량%, 예를 들어 3.5 내지 4.5 중량%, 유제놀 10 내지 25 중량%, 예를 들어 15 내지 20 중량%, 이소유제놀 2 내지 20 중량%, 예를 들어 5 내지 15 중량%, 리날로올 1 내지 15 중량%, 예를 들어 3 내지 8 중량%, 메틸 벤조에이트 0.5 내지 10 중량%, 예를 들어 2 내지 6 중량%, 베타-카리오필렌 0.2 내지 1.5 중량%, 예를 들어 0.5 내지 1 중량%, 아네톨 0.05 내지 2 중량%, 예를 들어 0.2 내지 0.6 중량% 및 카르본 0.5 내지 15 중량%, 예를 들어 2 내지 10 중량%를 포함할 수 있다. 상기 주요 향취 성분이 전술한 범위로 포함되는 경우 어진향차 고유의 향취를 효과적으로 재현할 수 있으며, 전술한 범위를 벗어나는 경우 어진향차 향취와의 유사성이 낮아지면서 향취의 기호성이 저하되고, 체취 제거 효과가 저하될 수 있다.The content of the main fragrance ingredient is not particularly limited, but based on the total weight of the fragrance composition, limonene is 1 to 5% by weight, for example, 1.5 to 2.5% by weight, citral is 0.2 to 5% by weight, for example, 0.5 to 1.5%. Weight percent, camphor 1 to 10 weight percent, for example 3.5 to 4.5 weight percent, eugenol 10 to 25 weight percent, for example 15 to 20 weight percent, isoeugenol 2 to 20 weight percent, for example 5 to 20 weight percent. 15% by weight, linalool 1 to 15% by weight, such as 3 to 8% by weight, methyl benzoate 0.5 to 10% by weight, such as 2 to 6% by weight, beta-caryophyllene 0.2 to 1.5% by weight, for example 0.5 to 1% by weight, anethole 0.05 to 2% by weight, such as 0.2 to 0.6% by weight, and carvone 0.5 to 15% by weight, such as 2 to 10% by weight. If the main fragrance components are contained within the above-mentioned range, the unique fragrance of the fragrant tea can be effectively reproduced. If it is outside the above-mentioned range, the similarity with the fragrant scent of the fragrant tea is lowered, the palatability of the fragrance is lowered, and the effect of removing body odor is reduced. may deteriorate.

일례로, 본 발명에 따른 향료 조성물은 메틸 차비콜(ETHYL CHAVICOL), 아밀 신남알(AMYL CINNAMAL) 및 파네졸(FARNESOL) 중 1종 이상을 더 포함할 수 있다. 상기 성분을 더 포함할 경우, 어진향차 향취와의 유사도 및 향취에 대한 기호도가 개선될 수 있다.For example, the fragrance composition according to the present invention may further include one or more of methyl chavicol (ETHYL CHAVICOL), amyl cinnamal (AMYL CINNAMAL), and farnesol (FARNESOL). When the above ingredients are further included, the similarity with the scent of euphorbia tea and the preference for the scent can be improved.

상기 추가 성분의 함량은 특별히 제한되지 않으나, 향료 조성물 총 중량을 기준으로, 메틸 차비콜 0.5 내지 3 중량%, 예를 들어 1 내지 2 중량%, 아밀 신남알 0.5 내지 5 중량%, 예를 들어 2 내지 3 중량% 및 파네졸 0.1 내지 3 중량%, 예를 들어 0.2 내지 1 중량%를 포함할 수 있다. 상기 추가 성분의 함량이 전술한 범위를 만족하는 경우, 어진향차 고유 향취에 대한 유사성 및 기호성을 향상시킬 수 있다.The content of the additional ingredients is not particularly limited, but based on the total weight of the fragrance composition, methyl chavicol 0.5 to 3% by weight, for example 1 to 2% by weight, amyl cinnamal 0.5 to 5% by weight, for example 2 to 3% by weight and farnesol 0.1 to 3% by weight, for example 0.2 to 1% by weight. When the content of the additional ingredient satisfies the above-mentioned range, the similarity and palatability of the unique flavor of the Eojin-flavored tea can be improved.

일례로, 본 발명에 따른 향료 조성물은 신나믹 알데하이드(CINNAMIC ALDEHYDE), 아니스 알데하이드(ANISE ALDEHYDE), 이소플라본(ISOFLAVONE) 및 크로만(CHROMANE) 중 1종 이상을 더 포함할 수 있다. 상기 성분은 악취를 발생하는 성분과 결합하기에 효과적인 구조를 갖는 것으로서, 상기 성분을 더 포함할 경우 체취 개선 효과를 극대화할 수 있다. For example, the fragrance composition according to the present invention may further include one or more of cinnamic aldehyde, anis aldehyde, isoflavone, and chromane. The ingredient has an effective structure for binding to ingredients that generate odor, and if the ingredient is further included, the effect of improving body odor can be maximized.

상기 추가 성분의 함량은 특별히 제한되지 않으나, 향료 조성물 총 중량을 기준으로, 신나믹 알데하이드 0.5 내지 10 중량%, 예를 들어 2 내지 6 중량%, 아니스 알데하이드 0.5 내지 7 중량%, 예를 들어 1 내지 4 중량%, 이소플라본 0.5 내지 7 중량%, 예를 들어 1 내지 3 중량% 및 크로만 0.2 내지 3 중량%, 예를 들어 0.5 내지 1.5 중량%를 포함할 수 있다. 상기 추가 성분의 함량이 전술한 범위를 만족하는 경우, 어진향차 고유 향취에 대한 유사성 및 기호성을 유지하는 동시에, 체취 개선 효과를 향상시킬 수 있다.The content of the additional ingredient is not particularly limited, but based on the total weight of the fragrance composition, cinnamic aldehyde is 0.5 to 10% by weight, for example, 2 to 6% by weight, anis aldehyde is 0.5 to 7% by weight, for example, 1 to 1%. 4% by weight, isoflavones 0.5 to 7% by weight, such as 1 to 3% by weight, and chromane 0.2 to 3% by weight, such as 0.5 to 1.5% by weight. When the content of the additional ingredient satisfies the above-mentioned range, the similarity and palatability of the unique fragrance of the ginseng tea can be maintained while simultaneously improving the body odor improvement effect.

본 발명에 따른 향료 조성물은 상기 향취 성분들의 분산성 및 조성물의 제형 안정성을 증가시키기 위해, 용매를 추가적으로 더 포함할 수 있다. 상기 용매로는 향료 조성물 분야에서 사용되는 통상적인 용매를 특별한 제한 없이 사용할 수 있으며, 예를 들어 이소프로판올, 에틸 카보네이트, 에틸 아세테이트, 벤질 알콜, 벤질 벤조에이트, 프로필렌 글리콜, 디프로필렌 글리콜, 1,3-부틸글리콜 오일, 글리세롤 지방족 에스테르, 폴리에틸렌 글리콜 또는 소르비탄의 지방산 에스테르 등을 사용할 수 있다.The fragrance composition according to the present invention may further include a solvent in order to increase the dispersibility of the fragrance ingredients and the formulation stability of the composition. The solvent may be any conventional solvent used in the field of perfume compositions without particular limitation, for example, isopropanol, ethyl carbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, propylene glycol, dipropylene glycol, 1,3- Butyl glycol oil, glycerol aliphatic ester, polyethylene glycol, or sorbitan fatty acid ester can be used.

상기 용매의 함량은 향료 조성물의 총 중량(100 중량%)을 만족시키는 잔량일 수 있으며, 예를 들어 향료 조성물 총 중량을 기준으로, 10 내지 60 중량%, 예를 들어 30 내지 55 중량%일 수 있다. 용매의 함량이 전술한 범위에 해당될 경우 향취 성분이 조성물 내에서 균일하게 분산될 수 있다.The content of the solvent may be a residual amount that satisfies the total weight of the fragrance composition (100% by weight), for example, 10 to 60% by weight, for example, 30 to 55% by weight, based on the total weight of the fragrance composition. there is. When the content of the solvent falls within the above-mentioned range, the fragrance component can be uniformly dispersed within the composition.

본 발명의 향료 조성물은 피부 외용제 조성물, 화장료 조성물, 퍼스널 케어 조성물, 홈 케어 조성물 등에 배합될 수 있고, 배합량은 당업계에 통상적인 기술에 따라 목적하는 효과를 이루기 위해 적절하게 선택할 수 있다.The fragrance composition of the present invention can be mixed into external skin compositions, cosmetic compositions, personal care compositions, home care compositions, etc., and the mixing amount can be appropriately selected to achieve the desired effect according to techniques common in the art.

상기 피부 외용제 조성물은 크림, 젤, 패취, 분무제, 연고제, 경고제, 로션제, 리니멘트제, 파스타제 또는 카타플라스마제의 피부 외용제 형태의 의약품 또는 의약외품으로 제조하여 사용할 수 있으나, 이에 제한되지 않는다. 상기 화장료 조성물은 크림, 폼, 유액, 오일, 유탁액, 스프레이 제형의 화장품 또는 향수에 사용될 수 있으나, 이에 제한되지 않는다. 상기 퍼스널 케어 조성물은 샴푸, 바디 워시(body wash), 비누, 세안제, 헤어 컨디셔너, 샴푸, 제모용 제품, 입욕제 등의 퍼스널 케어 제품에 사용될 수 있으나, 이에 제한되지 않는다. 상기 홈 케어 조성물은 주방 세제, 세탁 세제, 청소 세제 등의 홈 케어 제품에 사용될 수 있으나, 이에 제한되지 않는다.The composition for external use for skin can be manufactured and used as a drug or quasi-drug in the form of a cream, gel, patch, spray, ointment, warning agent, lotion, liniment, paste agent, or cataplasma agent, but is not limited thereto. . The cosmetic composition may be used in cream, foam, emulsion, oil, emulsion, spray formulation cosmetics or perfume, but is not limited thereto. The personal care composition may be used in personal care products such as shampoo, body wash, soap, face wash, hair conditioner, shampoo, hair removal product, and bath agent, but is not limited thereto. The home care composition may be used in home care products such as kitchen detergent, laundry detergent, and cleaning detergent, but is not limited thereto.

또한, 본 발명의 향료 조성물은 건강기능식품에 배합될 수 있고, 배합량은 당업계에 통상적인 기술에 따라 목적하는 효과를 이루기 위해 적절하게 선택할 수 있다.In addition, the flavor composition of the present invention can be mixed into health functional foods, and the mixing amount can be appropriately selected to achieve the desired effect according to techniques common in the art.

이하, 실시예를 통하여 본 발명을 보다 구체적으로 설명한다. 그러나 하기 실시예는 본 발명의 이해를 돕기 위한 것일 뿐, 어떠한 의미로든 본 발명의 범위가 실시예로 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail through examples. However, the following examples are only intended to aid understanding of the present invention, and the scope of the present invention is not limited to the examples in any way.

[어진향차 향취 분석][Analysis of scent of Eojin-scented tea]

회향, 곽향 및 정향을 1:1:1의 중량비로 혼합하여 끓는 물에 10분간 우려낸 후, 80 ℃에서 30분간 우려내어 어진향차를 제조하였다. GC-MS 분석을 수행하여 향취 성분을 분석하였으며 그 결과를 하기 표 1에 나타내었다.Fennel, fennel, and cloves were mixed at a weight ratio of 1:1:1, steeped in boiling water for 10 minutes, and then steeped at 80°C for 30 minutes to prepare Eojin-scented tea. GC-MS analysis was performed to analyze fragrance components, and the results are shown in Table 1 below.

GC-MS 분석 조건GC-MS analysis conditions

- 분석기기: HP 5890 II GC- Analysis instrument: HP 5890 II GC

- 컬럼: DB-1(60 m X 0.25 mm, 0.25 ㎛)- Column: DB-1 (60 m

- 이동상 기체: He- Mobile phase gas: He

- 주입온도: 250 ℃- Injection temperature: 250 ℃

- 검출온도: 270 ℃- Detection temperature: 270 ℃

- 오븐온도: 50 내지 220 ℃ (10 ℃/min)- Oven temperature: 50 to 220 ℃ (10 ℃/min)

상기 표 1에 나타난 바와 같이, 어진향차의 향취를 구성하는 전체 성분 중, 리모넨, 시트럴, 캠퍼, 유제놀, 이소유제놀, 리날로올, 메틸 벤조에이트, 베타-카리오필렌, 아네톨 및 카르본의 10가지 성분이 주 성분에 해당함을 확인하였다.As shown in Table 1, among all the ingredients that make up the fragrance of Eojin-scented tea, limonene, citral, camphor, eugenol, isoeugenol, linalool, methyl benzoate, beta-caryophyllene, anethole, and carboxylic acid. It was confirmed that the 10 ingredients of the product correspond to the main ingredients.

[실시예 1-4][Example 1-4]

하기 표 2에 기재된 조성에 따라 향취 성분 및 용매를 혼합하여 실시예 1-4의 향료 조성물을 제조하였다.The fragrance compositions of Examples 1-4 were prepared by mixing fragrance ingredients and solvents according to the composition shown in Table 2 below.

체취 마스킹 목적으로 향수를 사용해본 경험이 있는 20 내지 39세의 남녀 20명을 대상으로, 상기 실시예 1-4에 따라 제조된 향료 조성물이 10% 적용된 향수에 대한 관능 평가를 실시하였다. 일주일 동안 각 실시예의 향수를 손목 및 귀 밑(맥박이 뛰는 곳)에 아침, 저녁 각 1회씩 분사하고, 알코올이 충분히 휘발된 3분 후의 향취를 확인하였고, 그 결과를 하기 표 3 및 표 4에 나타내었다.Sensory evaluation was conducted on 20 men and women aged 20 to 39 who had experience using perfume for body odor masking, to which 10% of the perfume composition prepared according to Examples 1-4 was applied. For a week, the perfume of each example was sprayed on the wrist and under the ear (pulse point) once in the morning and once in the evening, and the fragrance was checked 3 minutes after the alcohol had sufficiently volatilized. The results are shown in Tables 3 and 4 below. indicated.

표 3는 각 실시예 조성물의 향취 선호도를 평가한 것이고, 표 4는 각 실시예 조성물의 어진향차 향취와의 유사성을 평가한 것이다. 선호도는 매우 좋은 경우 7점, 전혀 좋지 않은 경우 1점을 기준으로 평가하였으며, 유사성은 매우 유사한 경우 7점, 전혀 유사하지 않은 경우 1점을 기준으로 평가하였다.Table 3 evaluates the scent preference of each example composition, and Table 4 evaluates the similarity of each example composition to the scent of the traditional Chinese tea. Preference was evaluated based on 7 points if very good and 1 point if not good at all, and similarity was evaluated based on 7 points if very similar and 1 point if not similar at all.

상기 표 3의 결과로부터, 10종의 주 성분 외에 메틸 차비콜, 아밀 신남알 및 파네졸 중 1종 이상의 추가 성분을 더 포함하는 경우, 특히, 메틸 차비콜, 아밀 신남알 및 파네졸의 3종을 더 포함하는 경우, 향취에 대한 선호도가 더욱 증가한 것을 확인할 수 있다. From the results in Table 3 above, in the case where, in addition to the 10 main ingredients, one or more additional ingredients among methyl chavicol, amyl cinnamal, and farnesol are further included, in particular, 3 types of methyl chavicol, amyl cinnamal, and farnesol When further included, it can be seen that the preference for fragrance has further increased.

상기 표 4의 결과로부터, 10종의 주 성분 외에 메틸 차비콜, 아밀 신남알 및 파네졸 중 1종 이상의 추가 성분을 더 포함하는 경우, 특히, 메틸 차비콜, 아밀 신남알 및 파네졸의 3종을 더 포함하는 경우, 어진향차 향취에 대한 유사성이 더욱 증가한 것을 확인할 수 있다. From the results in Table 4 above, in addition to the 10 main ingredients, if one or more additional ingredients among methyl chavicol, amyl cinnamal, and farnesol are further included, in particular, 3 types of methyl chavicol, amyl cinnamal, and farnesol When further included, it can be seen that the similarity to the scent of the Eoji-flavored tea has further increased.

[실시예 5-8][Example 5-8]

하기 표 5에 기재된 조성에 따라 향취 성분 및 용매를 혼합하여 실시예 5-8의 향료 조성물을 제조하였다. The fragrance compositions of Examples 5-8 were prepared by mixing fragrance ingredients and solvents according to the compositions shown in Table 5 below.

체취 마스킹 목적으로 향수를 사용해본 경험이 있는 20 내지 39세의 남녀 20명을 대상으로, 상기 실시예 5-8에 따라 제조된 향료 조성물이 10% 적용된 향수에 대한 관능 평가를 실시하였다. 일주일 동안 각 실시예의 향수를 손목 및 귀 밑(맥박이 뛰는 곳)에 아침, 저녁 각 1회씩 분사하고, 알코올이 충분히 휘발된 3분 후 체취 개선도를 확인하였다. 하기 표 6의 결과는 실시예 4에 따른 향수를 적용한 경우와 대비하여 체취의 개선된 정도를 비교 평가한 것이다. 체취 개선도는 매우 좋은 경우 7점, 전혀 좋지 않은 경우 1점을 기준으로 평가하였다.Sensory evaluation was conducted on 20 men and women aged 20 to 39 who had experience using perfume for body odor masking, to which 10% of the perfume composition prepared according to Examples 5-8 was applied. For a week, the perfume of each example was sprayed on the wrist and under the ear (where the pulse beats) once in the morning and once in the evening, and the degree of improvement in body odor was confirmed after 3 minutes when the alcohol had sufficiently volatilized. The results in Table 6 below compare and evaluate the degree of improvement in body odor compared to the case where the perfume according to Example 4 was applied. The degree of improvement in body odor was evaluated based on 7 points for very good and 1 point for not good at all.

상기 표 6의 결과로부터, 실시예 4의 조성 외에 악취를 발생하는 성분과 결합하여 이를 제거하는 화합물을 1종 이상 더 포함하는 경우, 특히, 신나믹 알데하이드, 아니스 알데하이드, 이소플라본 및 크로만의 4종을 더 포함하는 경우, 체취 개선 효과가 더욱 증가한 것을 확인할 수 있다. From the results of Table 6, it can be seen that, in addition to the composition of Example 4, if one or more compounds that bind to and remove odor-generating components are further included, especially cinnamic aldehyde, anis aldehyde, isoflavone, and chroman 4. When more species are included, it can be seen that the effect of improving body odor is further increased.

Claims (10)

향료 조성물 총 중량을 기준으로, 리모넨 1 내지 5 중량%, 시트럴 0.2 내지 5 중량%, 캠퍼 1 내지 10 중량%, 유제놀 10 내지 25 중량%, 이소유제놀 2 내지 20 중량%, 리날로올 1 내지 15 중량%, 메틸 벤조에이트 0.5 내지 10 중량%, 베타-카리오필렌 0.2 내지 1.5 중량%, 아네톨 0.05 내지 2 중량%, 카르본 0.5 내지 15 중량%, 메틸 차비콜 0.5 내지 3 중량%, 아밀 신남알 0.5 내지 5 중량% 및 파네졸 0.1 내지 3 중량%를 포함하는 어진향차 향취 재현 향료 조성물.Based on the total weight of the fragrance composition, 1 to 5% by weight of limonene, 0.2 to 5% by weight of citral, 1 to 10% by weight of camphor, 10 to 25% by weight of eugenol, 2 to 20% by weight of isoeugenol, linalool. 1 to 15% by weight, methyl benzoate 0.5 to 10% by weight, beta-caryophyllene 0.2 to 1.5% by weight, anethole 0.05 to 2% by weight, carvone 0.5 to 15% by weight, methyl chavicol 0.5 to 3% by weight, A fragrance composition that reproduces the scent of Eojin-scented tea, comprising 0.5 to 5% by weight of amyl cinnamal and 0.1 to 3% by weight of farnesol. 삭제delete 삭제delete 삭제delete 제1항에 있어서, 신나믹 알데하이드(CINNAMIC ALDEHYDE), 아니스 알데하이드(ANISE ALDEHYDE), 이소플라본(ISOFLAVONE) 및 크로만(CHROMANE) 중 1종 이상을 더 포함하는 어진향차 향취 재현 향료 조성물.The fragrance composition of claim 1, further comprising at least one of cinnamic aldehyde, anise aldehyde, isoflavone, and chromane. 삭제delete 제5항에 있어서, 향료 조성물 총 중량을 기준으로, 신나믹 알데하이드 0.5 내지 10 중량%, 아니스 알데하이드 0.5 내지 7 중량%, 이소플라본 0.5 내지 7 중량% 및 크로만 0.2 내지 3 중량%를 포함하는 어진향차 향취 재현 향료 조성물.The method of claim 5, based on the total weight of the fragrance composition, 0.5 to 10% by weight of cinnamic aldehyde, 0.5 to 7% by weight of anis aldehyde, 0.5 to 7% by weight of isoflavone, and 0.2 to 3% by weight of chroman. Fragrance composition for reproducing the scent of fragrant tea. 제1항, 제5항 및 제7항 중 어느 한 항에 따른 향료 조성물을 포함하는 피부 외용제 조성물.A composition for external application to the skin comprising the fragrance composition according to any one of claims 1, 5, and 7. 제1항, 제5항 및 제7항 중 어느 한 항에 따른 향료 조성물을 포함하는 화장료 조성물.A cosmetic composition comprising the fragrance composition according to any one of claims 1, 5, and 7. 제1항, 제5항 및 제7항 중 어느 한 항에 따른 향료 조성물을 포함하는 건강기능식품.A health functional food containing the flavor composition according to any one of claims 1, 5, and 7.
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