JP3073831B2 - Fragrance composition for hair cosmetics and hair cleansing - Google Patents
Fragrance composition for hair cosmetics and hair cleansingInfo
- Publication number
- JP3073831B2 JP3073831B2 JP04087719A JP8771992A JP3073831B2 JP 3073831 B2 JP3073831 B2 JP 3073831B2 JP 04087719 A JP04087719 A JP 04087719A JP 8771992 A JP8771992 A JP 8771992A JP 3073831 B2 JP3073831 B2 JP 3073831B2
- Authority
- JP
- Japan
- Prior art keywords
- hair
- base
- fragrance
- fragrance composition
- agarwood
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
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- Cosmetics (AREA)
- Detergent Compositions (AREA)
- Fats And Perfumes (AREA)
Description
【0001】[0001]
【産業上の利用分野】本発明は、たばこ臭の付着した頭
髪から発する悪臭のマスキング効果に優れたマスキング
剤として、更には、頭髪化粧料用及び頭髪洗浄用香料と
して有用なる頭髪化粧料用及び頭髪洗浄用香料組成物に
関する。BACKGROUND OF THE INVENTION The present invention relates to a masking agent having an excellent masking effect on malodors generated from hair to which a tobacco odor is attached, and further to a hair cosmetic which is useful as a cosmetic for hair and a fragrance for washing hair. The present invention relates to a fragrance composition for cleaning hair.
【0002】[0002]
【従来の技術および発明が解決しようとする課題】従
来、たばこ臭の付着した頭髪から発する悪臭の防止方法
としては、香料組成物によるマスキング法が用いられて
いる。しかしながら、従来のマスキング用香料組成物の
処方設計は、調香師の長年の経験と勘に頼ってきた。2. Description of the Related Art Conventionally, as a method for preventing a malodor emitted from hair to which a tobacco smell has adhered, a masking method using a fragrance composition has been used. However, the formulation design of the conventional masking fragrance composition has relied on the perfumer's many years of experience and intuition.
【0003】しかも、充分なマスキング効果を得るため
には、重く暗く非常に特徴のある強い香りを使用しなけ
ればならず、香りが強すぎてかえって不快感を与えてし
まうなどの問題点があった。Moreover, in order to obtain a sufficient masking effect, it is necessary to use a strong scent that is heavy, dark, and very distinctive, and there is a problem that the scent is too strong and gives off discomfort. Was.
【0004】また、最近は自然な軽く明るい香りが好ま
れているが、この様な自然で軽く明るい香りでは、たば
こ臭を長時間にわたってマスキングすることは不可能で
あった。特にたばこ臭の付着した頭髪から発する悪臭の
マスキングを目的とした香料は、未だ見出だされてはい
ないのが現状である。[0004] In recent years, natural light and bright scents have been preferred, but it is impossible to mask the tobacco odor over a long period of time with such natural and light scents. In particular, at present, no fragrance has been found for the purpose of masking offensive odors emitted from the hair to which a tobacco odor is attached.
【0005】本発明者らは、このような事情に鑑み、鋭
意検討を重ねた結果、後記特定の頭髪化粧料用及び頭髪
洗浄料用香料組成物が頭髪臭のマスキング効果に優れる
ことを見い出し、本発明を完成した。In view of such circumstances, the present inventors have conducted intensive studies, and as a result, have found that the following specific fragrance composition for hair cosmetics and hair cleansing is excellent in masking effect of hair odor. The present invention has been completed.
【0006】即ち、本発明の目的は、頭髪臭のマスキン
グ効果に優れた頭髪化粧料用及び頭髪洗浄料用香料組成
物を提供することにある。[0006] That is, an object of the present invention is to provide a fragrance composition for hair cosmetics and a hair cleansing agent, which has an excellent masking effect on hair odor.
【0007】[0007]
【課題を解決するための手段】上記の目的は、沈香木精
油を含有することを特徴とする頭髪化粧料用及び頭髪洗
浄料用香料組成物、及び沈香木精油精油にシトラスベー
ス,ミュゲベース,ローズベース,ジャスミンベース,
ムスクベース等の明るく軽い香料成分を添加した頭髪化
粧料用及び頭髪洗浄料用香料組成物によって達成され
る。以下、本発明の構成に関して詳説する。DISCLOSURE OF THE INVENTION The object of the present invention is to provide a fragrance composition for hair cosmetics and a hair cleansing agent characterized by containing an essential oil of agarwood, and an essential oil of agarwood for citrus base, muguet base and rose. Base, jasmine base,
This is achieved by a fragrance composition for hair cosmetics and a hair cleanser to which a bright and light fragrance component such as musk base is added. Hereinafter, the configuration of the present invention will be described in detail.
【0008】本発明によって使用される沈香木とは、A
cquilaria属の倒木、枯木が土中に長年月埋没
し、その間細菌等の微生物の影響によって生成した特有
の芳香を有する黒色を呈した樹脂性物質で、東南アジア
を主たる産地とするものである。沈香木精油を得る方法
としては、沈香木を粉砕し、水蒸気蒸留法及び溶媒抽出
法(n−ヘキサン)がある(これらの方法によって得ら
れる沈香木精油をそれぞれ沈香木水蒸気蒸留物及び沈香
木溶媒抽出物と称する。)。また、超臨界炭酸ガス抽出
によっても得ることができる(この精油を沈香木超臨界
炭酸ガス抽出物と称する。)。これらの精油は褐色から
黒色の芳香を有する液体である。特に好ましくは沈香木
超臨界炭酸ガス抽出物である。The agarwood used in the present invention is A
A fallen tree or dead tree of the genus cquilaria has been buried in the soil for many years in the soil, during which time it is a black colored resinous substance with a unique aroma generated under the influence of microorganisms such as bacteria, and it is mainly produced in Southeast Asia. As a method for obtaining an agarwood essential oil, there is a steam distillation method and a solvent extraction method (n-hexane) by pulverizing an agarwood tree (the agarwood essential oil obtained by these methods is used for the agarwood steam distillate and the agarwood solvent, respectively). Extracts). It can also be obtained by supercritical carbon dioxide extraction (this essential oil is referred to as agarwood supercritical carbon dioxide extract). These essential oils are liquids having a brown to black aroma. Particularly preferred is an agarwood supercritical carbon dioxide extract.
【0009】本発明に用いる沈香木超臨界炭酸ガス抽出
物は、特願平3−98317号公報に記載の方法に準じ
て得られるものである。The supercritical carbon dioxide extract of agarwood used in the present invention is obtained according to the method described in Japanese Patent Application No. 3-98317.
【0010】沈香木精油の含有量は、香料組成物を基準
として、0.01重量%〜50重量%(以下wt%と略
記する)、好ましくは0.1wt%〜5wt%である。
0.01wt%未満の場合は、たばこ臭の付着した頭髪
から発する悪臭のマスキング効果が不十分になる傾向が
みられ、50wt%を超えると、芳香性が低下するの
で、好ましくない。[0010] The content of the agarwood essential oil is 0.01 to 50% by weight (hereinafter abbreviated as wt%), preferably 0.1 to 5% by weight, based on the perfume composition.
If the amount is less than 0.01 wt%, the masking effect of the malodor emitted from the hair to which a tobacco smell adheres tends to be insufficient, and if it exceeds 50 wt%, the fragrance is undesirably reduced.
【0011】本発明の頭髪化粧料用及び頭髪洗浄料用香
料組成物に配合される香料成分としては、シトラスベー
ス,ミュゲベース,ローズベース,ジャスミンベース,
ムスクベース等の明るく軽い香料成分が好ましいものと
して挙げられ、いずれも公知で、汎用される香料成分を
含有する。例えばシトラスベースはリモネン,シトラー
ル,リナロール,リナリルアセテート等からなり、ミュ
ゲベースはハイドロキシシトロネラール,リラール,リ
リアール等からなり、ローズベースはフェニルエチルア
ルコール,シトロネロール,ゲラニオール等からなり、
ジャスミンベースはベンジルアセテート,メチルディハ
イドロジャスモネート,ヘキシルシンナミックアルデヒ
ド等からなり、ムスクベースはギャラクソリッド,ムス
クケトン,シクロペンタデカノライド等からなるがこれ
らに限定されるものではない。The fragrance component to be added to the fragrance composition for hair cosmetics and hair cleansing composition of the present invention includes citrus base, mugue base, rose base, jasmine base, and the like.
Preferred are bright and light fragrance ingredients such as musk bases, all of which contain known and widely used fragrance ingredients. For example, citrus base is composed of limonene, citral, linalool, linalyl acetate, etc., muguet base is composed of hydroxycitronellal, liral, lilial, etc., rose base is composed of phenylethyl alcohol, citronellol, geraniol, etc.
The jasmine base is composed of benzyl acetate, methyl dihydrojasmonate, hexylcinnamic aldehyde and the like, and the musk base is composed of galact solid, musk ketone, cyclopentadecanolide and the like, but is not limited thereto.
【0012】これらの香料成分は、本発明の香料組成物
に保留性やこくを与え、また、トップノート,ボディノ
ート,ラストノートをうまく組み合わせることによっ
て、経時的にも魅力のある香りにすることができる。[0012] These fragrance components give the fragrance composition of the present invention a retention property and a body, and also make the fragrance attractive over time by combining top notes, body notes and last notes. Can be.
【0013】また、本発明の香料組成物には、香料成分
の組成比の調整のために、ジエチルフタレート等の希釈
剤を配合することもできる。The fragrance composition of the present invention may also contain a diluent such as diethyl phthalate for adjusting the composition ratio of the fragrance component.
【0014】本発明の頭髪化粧料用及び頭髪洗浄料用香
料組成物に配合される香料成分の含有量は、香料組成物
を基準として、0.01重量%〜50重量%(以下wt
%と略記する)、好ましくは0.1wt%〜5wt%で
ある。0.01wt%未満の場合は、芳香性が低下する
傾向がみられ、50wt%を超えると、特有の芳香性が
強くなるので、好ましくない。The content of the fragrance component contained in the fragrance composition for hair cosmetics and hair cleansing composition of the present invention is 0.01% by weight to 50% by weight (hereinafter referred to as wt.) Based on the fragrance composition.
%), Preferably 0.1 wt% to 5 wt%. When the content is less than 0.01 wt%, the fragrance tends to decrease.
【0015】本発明の香料組成物は、本発明の沈香木精
油が少量で長時間頭髪臭のマスキング効果を発揮する
為、従来のマスキング香料に見られた重く、暗く、力強
い香りとは異なる、弱い香り(自然で軽く、明るい香
り)、例えば、ローズカーネーションジャスミン等のシ
ングルフローラル,フローラルブーケ,フローラルアル
デヒド,フローラルグリーン,シプレー,オリエンタ
ル,シトラス等でも処方を組めるという利点を有してい
る。The fragrance composition of the present invention is different from the heavy, dark and powerful scent found in conventional masking fragrances because the agarwood essential oil of the present invention exerts a masking effect on hair odor for a long time in a small amount. There is an advantage that a formulation can be formulated even for a weak scent (natural, light and bright scent), for example, single floral such as rose carnation jasmine, floral bouquet, floral aldehyde, floral green, shipley, oriental, citrus, and the like.
【0016】本発明の香料組成物は、頭髪用デオドラン
トコロン等のフレグランス製品、ヘアートニック,ヘア
ーリクイド,ヘアーローション,ヘアースプレー,ヘア
ーセッティングフォーム,ヘアークリーム,ヘアーミル
ク,ヘアーブローローション,ヘアーブロースプレー,
ヘアーセッティングジェル,ヘアースティック,リン
ス,ヘアーコンディショナー,ヘアートリートメント,
ヘアーエッセンス,ヘアーパック等の頭髪化粧品料やシ
ャンプー等の頭髪洗浄料等に利用される。The fragrance composition of the present invention includes fragrance products such as deodorant colon for hair, hair tonic, hair liquid, hair lotion, hair spray, hair setting foam, hair cream, hair milk, hair blow lotion, hair blow spray,
Hair setting gel, hair stick, rinse, hair conditioner, hair tree Tome cement,
It is used for hair cosmetics such as hair essences and hair packs, and hair cleaning materials such as shampoos.
【0017】これらの製品への該香料組成物の配合量
は、製品形態によっても異なるが、製品総量を基準とし
てフレグランス製品には0.5wt%〜30wt%,ヘ
アートニック,シャンプー等のヘアケア製品には0.1
wt%〜1.0wt%配合される。 The amount of the fragrance composition in these products varies depending on the product form. However, based on the total amount of the product, the fragrance product is used in an amount of 0.5% to 30% by weight, and the fragrance product is used in hair care products such as hair tonic and shampoo. Is 0.1
wt% to 1.0 wt% .
【0018】[0018]
【実施例】以下、実施例及び比較例によって本発明を詳
説するが、本発明は実施例の記載に限定されるものでは
ない。EXAMPLES The present invention will be described below in detail with reference to examples and comparative examples, but the present invention is not limited to the description of the examples.
【0019】実施例、及び応用例に先立ち、評価方法に
ついて述べる。Prior to the embodiment and the application example, an evaluation method will be described.
【0020】実施例の評価方法Evaluation method of the embodiment
【0021】(1)マスキング効果評価試験方法 毎分10リットルの空気を循環させた20リットルのガ
ラス製の容器内に、着火した市販紙巻き煙草を一本入
れ、煙草は10分ごとに交換しこれを煙室とした。この
煙室内に、充分に洗浄を行った頭髪束5グラムを20分
間さらし、取り出した後30分経過したものにエチルア
ルコールで0.3%に希釈した頭髪化粧料用及び頭髪洗
浄料用香料組成物を噴霧する。(1回の噴霧量約0.1
グラム)この香料組成物の噴霧より5分後,30分後,
1時間後に頭髪束から発する悪臭がマスキングされてい
るかどうかを、5名の調香師が判断し、下記の規準で評
価した。(1) Masking Effect Evaluation Test Method One ignited commercial cigarette is placed in a 20-liter glass container circulating 10 liters of air per minute, and the cigarette is replaced every 10 minutes. Was designated as a smoke room. 5 g of a thoroughly washed hair bundle was exposed to the smoke chamber for 20 minutes, and after 30 minutes from the removal, the hair bundle was diluted to 0.3% with ethyl alcohol and used as a fragrance composition for hair cosmetics and hair cleansing. Spray things. (Approximately 0.1 spray amount
G) 5 minutes and 30 minutes after spraying of the perfume composition,
One hour later, five perfumers determined whether or not the odor emitted from the hair bundle was masked, and evaluated according to the following criteria.
【0022】 [0022]
【0023】5名の得点の合計を、下記の基準で評価し
た。 The total of the scores of the five persons was evaluated according to the following criteria.
【0024】(2)香りの官能評価試験方法 (1)のマスキング効果評価試験方法と同様にして5分
後,30分後,1時間後に、20名のパネルが頭髪束の
においを官能的に判断し、下記の基準で評価した。(2) Sensory evaluation test method for fragrance In the same manner as in the test method for evaluating the masking effect of (1), after 5 minutes, 30 minutes, and 1 hour, a panel of 20 persons sensuously sensed the smell of the hair bundle. It was judged and evaluated according to the following criteria.
【0025】 [0025]
【0026】応用例の評価方法Evaluation method of application example
【0027】(1)マスキング効果評価試験方法 煙草の煙を充満させた容積約70立方メートルの部屋
に、女性パネラーを30分間入室させた後、調製した頭
髪化粧料及び頭髪洗浄料を、通常の使用方法にしたがっ
て使用し、使用直後,1時間後,3時間後の頭髪から発
する臭いがマスキングされているかどうかを、5名の調
香師が判断し、実施例と同様の基準で評価した。(1) Masking Effect Evaluation Test Method After a female panelist was allowed to enter a room filled with tobacco smoke and having a volume of about 70 cubic meters for 30 minutes, the prepared hair cosmetics and hair cleansing agent were used under normal conditions. It was used according to the method, and five perfumers judged whether the odor emitted from the hair immediately after use, 1 hour after, and 3 hours after was masked, and evaluated based on the same criteria as in the examples.
【0028】(2)香りの官能評価試験方法 煙草の煙を充満させた容積約70立方メートルの部屋
に、女性パネラーを30分間入室させた後、調整した頭
髪化粧料及び頭髪洗浄料を、通常の使用方法にしたがっ
て使用し、使用直後,1時間後,3時間後の頭髪から発
する臭いを、20名のパネルが官能的に判断し、実施例
と同様の基準で評価した。(2) Sensory evaluation test method of fragrance After a female panelist was allowed to enter a room filled with tobacco smoke and having a volume of about 70 cubic meters for 30 minutes, the adjusted hair cosmetics and hair cleansing were applied to a normal room. The panel was used according to the method of use, and a panel of 20 persons sensually judged the odor emitted from the hair immediately after use, 1 hour after, and 3 hours after, and evaluated according to the same criteria as in the examples.
【0029】実施例には沈香木精油の他に、香料成分と
しては、リモネン,シトラール,リナロール,リナリル
アセテートからなるシトラスベース及び、ハイドロキシ
シトロネラール,リラール,リリアーからなるミュゲベ
ース及び、フェニルエチルアルコール,シトロネロー
ル,ゲラオールからなるローズベース及び、ベンジルア
セテート,メチルディハイドロジャスモネート,ヘキシ
ルシンナミックアルデヒドからなるジャスミンベース及
び、ギャラクソライド,ムスクケトン,シクロペンタデ
カノライドからなるムスクベースを用いた。In the examples, in addition to the agarwood essential oil, the fragrance components include citrus base consisting of limonene, citral, linalool, linalyl acetate and mugue base consisting of hydroxycitronellal, linal, and lilia, phenylethyl alcohol, A rose base composed of citronellol and geraol, a jasmine base composed of benzyl acetate, methyldihydrojasmonate, and hexylcinnamic aldehyde, and a musk base composed of galaxolide, musk ketone, and cyclopentadecanolide were used.
【0030】実施例1〜3,比較例1〜3 (頭髪化粧料用及び頭髪洗浄料用香料組成物) 調製方法 表1及び表2の処方に示した成分を混合し、頭髪化粧料
用及び頭髪洗浄料用香料組成物を調製し、評価結果を表
1及び表2に示した。Examples 1 to 3 and Comparative Examples 1 to 3 (Fragrance compositions for hair cosmetics and hair cleansers) Preparation method The ingredients shown in the formulations of Tables 1 and 2 were mixed and used for hair cosmetics and A fragrance composition for hair washes was prepared, and the evaluation results are shown in Tables 1 and 2.
【0031】[0031]
【表1】 [Table 1]
【0032】[0032]
【表2】 [Table 2]
【0033】表1及び表2から分かるように、本発明の
香料組成物を含有する頭髪化粧料用及び頭髪洗浄料用香
料組成物は、比較例の香料組成物と比較して、良好なマ
スキング効果及び官能特性に優れることが分かった。As can be seen from Tables 1 and 2, the fragrance composition for hair cosmetics and hair cleansing containing the fragrance composition of the present invention has better masking than the fragrance composition of Comparative Example. It was found to be excellent in effect and sensory characteristics.
【0034】応用例1〜3,比較応用例1〜3 (ヘアートニック) 調製方法 表3の処方に示した成分を混合し、ヘアートニックを調
製し、評価結果を表3に示した。Application Examples 1 to 3 and Comparative Application Examples 1 to 3 (Heart Tonic) Preparation Method The ingredients shown in Table 3 were mixed to prepare a hair tonic, and the evaluation results are shown in Table 3.
【0035】[0035]
【表3】 [Table 3]
【0036】表3からもわかるように、本発明の香料組
成物を含有するヘアートニックは、それを含有しないも
のと比べて、頭髪臭のマスキング効果及び官能特性に優
れ、しかもその効果の持続時間も長かった。As can be seen from Table 3, the hair tonic containing the fragrance composition of the present invention is superior in the masking effect and sensual properties of the hair odor and the duration of the effect, as compared with those not containing it. Was also long.
【0037】応用例4〜6,比較応用例4〜6 (シャンプー)Application Examples 4 to 6, Comparative Application Examples 4 to 6 (Shampoo)
【0038】表4の処方に示した成分を混合し、シャン
プーを調製した。評価結果を表4に示した。The components shown in Table 4 were mixed to prepare a shampoo. Table 4 shows the evaluation results.
【0039】[0039]
【表4】 [Table 4]
【0040】表4からもわかるように、本発明の香料組
成物を含有するシャンプーは、それを含有しないものと
比べて、頭髪臭のマスキング効果及び官能特性に優れ、
しかもその効果の持続時間も長かった。As can be seen from Table 4, the shampoo containing the fragrance composition of the present invention is superior to the shampoo containing no shampoo in masking effect of hair odor and sensory characteristics.
And the duration of the effect was long.
【0041】[0041]
【発明の効果】本発明は、たばこ臭の付着した頭髪から
発する悪臭のマスキング効果に優れた頭髪化粧料用及び
頭髪洗浄料用香料組成物を提供することは明らかであ
る。It is apparent that the present invention provides a fragrance composition for hair cosmetics and a hair cleansing agent which has an excellent masking effect of malodors generated from hair to which a tobacco odor is attached.
Claims (4)
を特徴とするたばこ臭マスキング頭髪化粧料用香料組成
物。1. A fragrance composition for tobacco odor masking hair cosmetics, comprising an essential oil obtained from agarwood.
を特徴とするたばこ臭マスキング頭髪洗浄料用香料組成
物。2. A fragrance composition for tobacco odor masking hair cleansing, comprising an essential oil obtained from agarwood.
ース,ミュゲベース,ローズベース,ジャスミンベー
ス,ムスクベースの香料成分とを含有することを特徴と
するたばこ臭マスキング頭髪化粧料用香料組成物。3. A fragrance composition for tobacco odor masking hair cosmetics, comprising an essential oil obtained from agarwood and fragrance components of citrus base, mugge base, rose base, jasmine base and musk base.
ース,ミュゲベース,ローズベース,ジャスミンベー
ス,ムスクベースの香料成分とを含有することを特徴と
するたばこ臭マスキング頭髪洗浄料用香料組成物。4. A fragrance composition for tobacco odor masking hair cleansers, comprising an essential oil obtained from agarwood and fragrance components of citrus base, mugge base, rose base, jasmine base and musk base.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP04087719A JP3073831B2 (en) | 1992-03-10 | 1992-03-10 | Fragrance composition for hair cosmetics and hair cleansing |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP04087719A JP3073831B2 (en) | 1992-03-10 | 1992-03-10 | Fragrance composition for hair cosmetics and hair cleansing |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH05255059A JPH05255059A (en) | 1993-10-05 |
JP3073831B2 true JP3073831B2 (en) | 2000-08-07 |
Family
ID=13922720
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP04087719A Expired - Fee Related JP3073831B2 (en) | 1992-03-10 | 1992-03-10 | Fragrance composition for hair cosmetics and hair cleansing |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP3073831B2 (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001007002A1 (en) | 1999-07-26 | 2001-02-01 | Kao Corporation | Deodorants |
GB0104094D0 (en) * | 2001-02-20 | 2001-04-04 | Quest Int | Macrocyclic musks for malodour prevention and counteraction |
GB2484359A (en) * | 2011-02-07 | 2012-04-11 | Robina Martha Bananuka | Hair-freshener composition containing essential oils |
-
1992
- 1992-03-10 JP JP04087719A patent/JP3073831B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
JPH05255059A (en) | 1993-10-05 |
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