CN1171198A - 0.08% matrine aqua - Google Patents
0.08% matrine aqua Download PDFInfo
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- CN1171198A CN1171198A CN 97105935 CN97105935A CN1171198A CN 1171198 A CN1171198 A CN 1171198A CN 97105935 CN97105935 CN 97105935 CN 97105935 A CN97105935 A CN 97105935A CN 1171198 A CN1171198 A CN 1171198A
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- kuh
- hop
- tobacco
- fructus zanthoxyli
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Abstract
A 0.08% matrine aqua belonging to a plant protecting agent for preventing and eliminating pests in lepidoptera, Hemiptera, Vaginata and Homoptera is prepared from 9 natural plants such as flavescent sophora root, chinaberry, tobacco, trifoliate jawelvine, common threewingnut, etc. through breaking, extraction, concentration, alcohol deposition, reflux and mixing, and features high effect, low poison, no residue and no environmental pollution.
Description
The invention belongs to a kind of plant protecting liquid.
Though agricultural chemicals is a key factor of guaranteeing agricultural year, stable yields, but the present chemical pesticide that uses, not only environment is caused severe contamination, and can in using the grain of chemical pesticide, vegetables, fruit and other edible economic crops, leave a large amount of residual hazards, directly damage the people's physical and mental health.A large amount of uses of chemical pesticide also are one of key factors of current cancer patient's increase.
The agricultural chemicals of China's use at present, great majority belong to the bigger agricultural chemicals of toxicity, and are therefore just more serious to the pollution of environment and crop, just bigger to China people's physical and mental health harm.In addition,, also cause the minimizing of agricultural byproducts outlet, cause very big economic loss to country because residue of pesticide exceed standard.
Purpose of the present invention is the problems referred to above that exist at chemical pesticide, provides a kind of efficient, low toxicity, noresidue, production not to have the aqueous matrine solution of the three wastes.
Purpose of the present invention adopts following technical proposals to realize, that is:
0.08% aqueous matrine solution, be utilize pure natural plant kuh-seng, China tree, tobacco, trifoliate jewelvine, thunder godvine, maple willow, hop, rule grass, Fructus Zanthoxyli Plansipini through extraction, concentrate, alcohol precipitation, return to stay and make.
China utilizes the characteristic of plant, promptly utilizes its some contained composition, and the control diseases and pests of agronomic crop is ancient, and oneself has it.According to record, just oneself waits pest control through the agent of appliable plant insects as crotons before 1800.Just once mentioning plants such as the tuber of stemona, black false hellebore, the root of langdu, kuh-seng has insecticidal properties in 1892 kinds of medicines that the Compendium of Material Medica that the Ming Dynasty 24 years Wanli year (1596) Li Shizhen (1518-1593 A.D.) is write is narrated.
We utilize natural plants to kill the experience of plant insect, inspiration and theory of traditional Chinese medical science according to the Ancient Times in China scientist; we have selected a collection ofly to have insecticidal function and person poultry harmless's natural plants is mixed with plant protecting liquid; through extensive, long-term test; comprise the large tracts of land field trial; the kind of medicinal plant and compatibility carried out repeatedly revising, succeeded in developing the high and low poison of insecticidal effect, noresidue, 0.08% aqueous matrine solution free from environmental pollution finally.
The compatibility of 0.08% aqueous matrine solution is:
Kuh-seng 5-30%, China tree 15-30%, tobacco 6-20%, trifoliate jewelvine 4-20%, thunder godvine 5-20%, maple willow 4-10%, hop 4-10%, restrain careless 3-5%, Fructus Zanthoxyli Plansipini 9-10%.
0.08% aqueous matrine solution is to extract to have the natural components Banlangen of killing plant insect effectiveness from above-mentioned natural plants, through being processed into.The demarcation composition of the present invention's and quantitative analysis qualitative as it with matrine is with reference to the related standards now of kuh-seng bar in the Pharmacopoeia of the People's Republic of China (95).
Kuh-seng (SOphorafLavesensAit) belongs to leguminous plant.The structural formula with matrine (Matrine) of killing plant insect effectiveness that extracts from radix sophorae is
Empirical formula is: C
15H
24N
2O.The effective content of matrine 〉=0.08%.Outward appearance is the dark brown homogeneous liquid, does not have visible suspension and sediment, and density is 995kg/m
3, acidity is (with H
2SO
4Meter)≤1.0, stability of emulsion (extension rate) 800,1000,1200, storage at normal temperature stability is for to store under shady and cool lucifuge condition, and the shelf-life is 2 years, can use with chrysanthemum lipid and acid agrichemical.
0.08% aqueous matrine solution has following advantage:
1, has efficient, broad spectrum activity
0.08% aqueous matrine solution is to Lepidoptera, the Semiptera of vegetables, fruit tree, flowers, forest, field crop, stick up various pests such as wing order, Homoptera, diptera and Acarina and have and significantly kill and preventive effect.
2, has hypotoxicity
Chemical pesticide generally all has the characteristic of severe toxicity, though it can kill the insect of damage to crops effectively, people and animals is waited to constitute the danger side of body simultaneously.And 0.08% aqueous matrine solution, be that pure natural plant is made, estimate the toxicity test conclusion that carry out at the supervision and inspection center, all belong to " low toxicity " through toxicological test and the Ministry of Chemical Industry's chemistry security of Tianjin labour health occupation disease precaution﹠china institution, people and animals are not had the danger of poisoning, belong to a kind of safe agricultural chemicals.0.08% aqueous matrine solution is after the detection and test of units such as Japanese plate shell garden Co., Ltd., american agriculture research institute, the Chinese Academy of Agricultural Sciences, Jiangsu Province's plant protection master station, Liaoning Province's agricultural research institute, academy of agricultural sciences, Liaoning Province, the Temple of Heaven, Beijing, being subjected to consistent favorable comment and abundant affirmation, is the desirable regeneration product of existing agricultural chemicals.
3, non-environmental-pollution problem
(1), noresidue
Another drawback of general chemical pesticide is exactly the toxic residue problem, and residual periodicity is long, damaging range is wide, some agricultural chemicals even can in organisms such as people and animals, precipitate and accumulate, scientist has unexpectedly found the molecule of hexachlorcyclohexane in the last penguin body of living on not by the region of large-scale development on this sheet earth of the South Pole, this harmfulness of chemical pesticide can have been seen, and 0.08% aqueous matrine solution is a kind of low toxicity product that utilizes multiple pure natural plant to handle through scientific technology, there is not the toxic residue problem in tracking test, to the greatest extent ecotopes such as people and animals is not constituted any danger side of body yet.
(2), produce the no three wastes
No matter chemical pesticide factory where is existing and produce the pollution problem of the three wastes to surrounding environment more or less all, expended great amount of manpower for this reason, financial resources and material resources are not fundamentally reversed this passive situation yet, there is not the problem of producing the three wastes and produce 0.08% aqueous matrine solution: 1. produce remaining waste residue and can be used for fermenting, the biogas that fermentation is produced can be used as a kind of good energy and is used, the remaining fermentation dregs of a decoction through with other fertilizer by a certain percentage after the proportioning, make genseng fertilizer, first-class fertilizer such as grape fertilizer have good development prospect and vast market; 2. the industrial water after using is after simple process, and recycling again can also be as the dipping water, for the health of human body is made due contribution.3. there is not waste gas.
4, raw material sources are extensive, and are cheap
Kuh-seng, China tree, tobacco, trifoliate jewelvine, thunder godvine, maple willow, hop, rule grass, these raw materials of Fructus Zanthoxyli Plansipini all are easy to get, particularly radix sophorae in China northeast, all there is growth the mountain area and the hilly country in most of area, North China, spring, Qiu Erji can excavate.
5, extraction and preparation process are easy, are easy to form large-scale production
If produce with a kind of product, and your production technology is quite complicated, and specification requirement is very high again, will influence the large-scale production and the exploitation of this product in various degree, also can increase this production cost of products, thus make product the competitiveness on the market relatively a little less than.The production technology of 0.08% aqueous matrine solution is also uncomplicated, and equipment needed thereby also has only extractor, inspissator, recovery tower, triple effect machine etc., and production procedure is simple and clear, clear.Its technological process is: raw material → cleaning → pulverizing → extraction → concentrate → alcohol precipitation → return and heat up in a steamer → mix → canned → warehouse-in, this has just increased the feasibility of large-scale production and exploitation greatly.In fact this technology belongs to conventional herb liquid extraction process.
Embodiment one
Aqueous matrine solution, by kuh-seng, China tree, tobacco, trifoliate jewelvine, thunder godvine, maple willow, hop, rule grass, Fructus Zanthoxyli Plansipini, through cleaning, pulverize, extraction, concentrating, alcohol precipitation, return and heat up in a steamer, be mixed and made into, the compatibility of its kuh-seng, China tree, tobacco, trifoliate jewelvine, thunder godvine, maple willow, hop, rule grass, Fructus Zanthoxyli Plansipini is: kuh-seng 20%, China tree 20%, tobacco 10%, trifoliate jewelvine 5%, thunder godvine 5%, maple willow 20%, hop 6%, rule grass 4%, Fructus Zanthoxyli Plansipini 10%.
Its process is:
1, get kuh-seng, China tree, tobacco, trifoliate jewelvine, thunder godvine, maple willow, hop, rule grass, Fructus Zanthoxyli Plansipini by above-mentioned compatibility respectively, and washing respectively, after the drying and crushing, sieve with 20 mesh sieve;
2, use chloroform (also can adopt hexyl acetate) extraction respectively, the water reduction, concentrate again, alcohol precipitation (employing ethanol), return and to stay, at last extract is mixed, make to comprise matrine 0.08%, nicotine 0.3%, China tree alkali 0.6%, wilfordine 0.4%, rotenone 0.1% in the extract.
This agricultural chemicals all has tangible control efficiency to the various pests such as Lepidoptera, Semiptera, Homoptera, diptera and Acarina of vegetables, fruit tree, flowers, forest, field crop.See annex 1 for details
The suitable concentration of controlling object and spray droplets: table 1
| Crop | Controlling object | The control phase | Extension rate |
| Greengrocery | Cabbage caterpillar | Emergence period | ????1000-1200 |
| Vegetable aphid | ???????″ | ????1000-1200 | |
| Oeobia undalis | ???????″ | ????1000-1200 | |
| Trialeurodes vaporariorum | ???????″ | ????1000-1200 | |
| Thrips | ???????″ | ????1000-1200 | |
| The 28 stars worm of wafing | ???????″ | ????1000-1200 | |
| Fruit tree kind | The pears aphid | ???????″ | ????800-1000 |
| Tent caterpillar | ???????″ | ????1000-1200 | |
| The boat-shaped caterpillar | ???????″ | ????1000-1200 | |
| The star caterpillar | ???????″ | ????1000-1200 | |
| Grape owlet moth | ???????″ | ????1000-1200 | |
| Slug moth | ???????″ | ????1000-1200 | |
| Looper | ???????″ | ????1000-1200 | |
| The poison caterpillar | ???????″ | ????1000-1200 | |
| The land for growing field crops | Mythimna separata | ???????″ | ????1000-1200 |
| Wheat aphid | ???????″ | ????1000-1200 | |
| Chinese herbal medicine | Aphid | ???????″ | ????1000-1200 |
| Defoliator | ???????″ | ????1000-1200 | |
| Locust | ???????″ | ????1000-1200 | |
| Beet | Beet webworm | ???????″ | ????800-1000 |
Embodiment two
Second kind of material combination making 0.08% aqueous matrine solution is: kuh-seng 10%, China tree 20%, tobacco 20%, trifoliate jewelvine 20%, thunder godvine 5%, maple willow 5%, hop 4%, rule grass 5%, Fructus Zanthoxyli Plansipini 9%.
This agricultural chemicals has special efficacy to aphid.
Embodiment three
The third material combination of making 0.08% aqueous matrine solution is: kuh-seng 5%, China tree 30%, tobacco 10%, trifoliate jewelvine 5%, thunder godvine 20%, maple willow 4%, hop 10%, rule grass 6%, Fructus Zanthoxyli Plansipini 10%.
This agricultural chemicals has special efficacy to insect.The production technology of embodiment two, three is identical with embodiment one.
Claims (2)
1,0.08% aqueous matrine solution, by pure natural plant through cleaning respectively, pulverize, extract, concentrate, alcohol precipitation, returning and to be mixed and made into after heating up in a steamer, it is characterized in that described pure natural plant is kuh-seng, China tree, trifoliate jewelvine, thunder godvine, maple willow, hop, rule grass, Fructus Zanthoxyli Plansipini, its compatibility is: kuh-seng 5-30%, China tree 15-30%, tobacco 6-20%, trifoliate jewelvine 4-20%, thunder godvine 5-20%, maple willow 4-10%, hop 4-10%, restrain careless 3-5%, Fructus Zanthoxyli Plansipini 9-10%.
2,0.08% aqueous matrine solution according to claim 1, it is characterized in that described kuh-seng, China tree, tobacco, trifoliate jewelvine, thunder godvine, the maple willow, hop, the rule grass, the compatibility of Fructus Zanthoxyli Plansipini can be kuh-seng 20%, China tree 20%, tobacco 10%, trifoliate jewelvine 5%, thunder godvine 5%, maple willow 20%, hop 6%, rule grass 4%, Fructus Zanthoxyli Plansipini 10%, also can be kuh-seng 10%, China tree 20%, tobacco 20%, trifoliate jewelvine 20%, thunder godvine 5%, maple willow 5%, hop 4%, rule grass 5%, Fructus Zanthoxyli Plansipini 9% also can be kuh-seng 5%, China tree 30%, tobacco 10%, trifoliate jewelvine 5%, thunder godvine 20%, maple willow 4%, hop 10%, rule grass 6%, Fructus Zanthoxyli Plansipini 10%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 97105935 CN1171198A (en) | 1997-06-25 | 1997-06-25 | 0.08% matrine aqua |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 97105935 CN1171198A (en) | 1997-06-25 | 1997-06-25 | 0.08% matrine aqua |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1171198A true CN1171198A (en) | 1998-01-28 |
Family
ID=5168222
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 97105935 Pending CN1171198A (en) | 1997-06-25 | 1997-06-25 | 0.08% matrine aqua |
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|---|---|
| CN (1) | CN1171198A (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101300986B (en) * | 2008-07-07 | 2010-06-02 | 石天文 | Biological insecticide |
| CN104322328A (en) * | 2014-09-26 | 2015-02-04 | 广东省昆虫研究所 | Orange pest ecological control method using predatory mites as basis |
| CN105010426A (en) * | 2015-06-30 | 2015-11-04 | 韩淑红 | High-efficiency nontoxic dichocrocis punctiferalis controlling pesticide |
| CN105265497A (en) * | 2015-11-06 | 2016-01-27 | 广西南宁胜祺安科技开发有限公司 | Preparation method for fertilizer-mixing biological disinsection additive |
| CN105265496A (en) * | 2015-11-06 | 2016-01-27 | 广西南宁胜祺安科技开发有限公司 | Preparation method of plant source insecticidal additives capable of preventing and controlling underground harmful insects |
| CN105394090A (en) * | 2015-12-24 | 2016-03-16 | 青岛百瑞吉生物工程有限公司 | Natural bactericide for controlling persimmon fruit moth of persimmon trees and preparation method thereof |
| CN105410054A (en) * | 2015-11-06 | 2016-03-23 | 广西南宁胜祺安科技开发有限公司 | Method for preparing medicines with underground insect pest prevention and treatment functions |
| CN105660727A (en) * | 2015-12-18 | 2016-06-15 | 信宜市四海永丰现代种养场 | Preparation method of biological disease and pest prevention medicine used for melon and fruit vegetables |
| CN110338196A (en) * | 2019-06-29 | 2019-10-18 | 中国农业科学院兰州兽医研究所 | A kind of compound botanical preparation for killing tick |
-
1997
- 1997-06-25 CN CN 97105935 patent/CN1171198A/en active Pending
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101300986B (en) * | 2008-07-07 | 2010-06-02 | 石天文 | Biological insecticide |
| CN104322328A (en) * | 2014-09-26 | 2015-02-04 | 广东省昆虫研究所 | Orange pest ecological control method using predatory mites as basis |
| CN105010426A (en) * | 2015-06-30 | 2015-11-04 | 韩淑红 | High-efficiency nontoxic dichocrocis punctiferalis controlling pesticide |
| CN105010426B (en) * | 2015-06-30 | 2018-01-23 | 李晓亮 | A kind of dichocrocis punctiferalis preventing and treating agricultural chemicals of high effect nontoxic |
| CN105010426B8 (en) * | 2015-06-30 | 2018-03-27 | 黑龙江中医药大学 | A kind of dichocrocis punctiferalis preventing and treating agricultural chemicals of high effect nontoxic |
| CN105265497A (en) * | 2015-11-06 | 2016-01-27 | 广西南宁胜祺安科技开发有限公司 | Preparation method for fertilizer-mixing biological disinsection additive |
| CN105265496A (en) * | 2015-11-06 | 2016-01-27 | 广西南宁胜祺安科技开发有限公司 | Preparation method of plant source insecticidal additives capable of preventing and controlling underground harmful insects |
| CN105410054A (en) * | 2015-11-06 | 2016-03-23 | 广西南宁胜祺安科技开发有限公司 | Method for preparing medicines with underground insect pest prevention and treatment functions |
| CN105660727A (en) * | 2015-12-18 | 2016-06-15 | 信宜市四海永丰现代种养场 | Preparation method of biological disease and pest prevention medicine used for melon and fruit vegetables |
| CN105394090A (en) * | 2015-12-24 | 2016-03-16 | 青岛百瑞吉生物工程有限公司 | Natural bactericide for controlling persimmon fruit moth of persimmon trees and preparation method thereof |
| CN110338196A (en) * | 2019-06-29 | 2019-10-18 | 中国农业科学院兰州兽医研究所 | A kind of compound botanical preparation for killing tick |
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