CN116889528A - Water-light mask and preparation method thereof - Google Patents

Water-light mask and preparation method thereof Download PDF

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Publication number
CN116889528A
CN116889528A CN202310853358.8A CN202310853358A CN116889528A CN 116889528 A CN116889528 A CN 116889528A CN 202310853358 A CN202310853358 A CN 202310853358A CN 116889528 A CN116889528 A CN 116889528A
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extract
mask
hydrographic
skin
water
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郑帅
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Shanghai Lanzhimeiya Cosmetics Co ltd
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Shanghai Lanzhimeiya Cosmetics Co ltd
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Abstract

The invention discloses a water-light facial mask and a preparation method thereof, wherein the preparation raw materials comprise: water, moisturizer, skin conditioner, antioxidant component, plant extract, skin protectant, film forming agent, pH regulator, and antiseptic. The polypeptide combination of the invention is carnosine, acetyl hexapeptide-8, palmitoyl pentapeptide-4, tetrapeptide-4 and palmitoyl tripeptide-8, which can tighten skin and reduce wrinkles within 14 days. The plant extract and the antioxidant component are added to act together, so that the repairing effect of the mask is further improved.

Description

Water-light mask and preparation method thereof
Technical Field
The invention relates to the field of A61K8/9789, in particular to a water-light mask and a preparation method thereof.
Background
The facial mask is a kind of skin care product, and the skin is covered for a short time to temporarily isolate the external air and pollution, so that the skin cuticle is supplemented with all the moisture, humectant and nutrient in the facial mask. In recent years, because of the enhancement of the maintenance consciousness and the transition of the consumption consciousness of Chinese consumers, the consumer groups of the mask are continuously expanded, and at present, the mask becomes a heavy game in a cosmetic sales matrix because the mask bears the beauty of broad men and women consumers.
CN110559238A discloses a waxberry essence polypeptide water-light mask, which comprises a mask liquid coated on the surface of a substrate, wherein the mask liquid consists of a water solvent, a skin conditioning agent, a humectant, a thickening agent, a solubilizer and a PH regulator, the skin conditioning agent comprises poly-gamma sodium glutamate, a mixture of phycocyanin and alcohol, a cactus extract, a waxberry extract, trehalose, betaine, p-hydroxyacetophenone, hydroxyethyl cellulose, beta glucan and a polypeptide mixed liquid according to the content ratio of all raw materials, and the mask can relieve the dry and tight state of skin and nourish the skin in a water-moist manner, but the repairing function of the skin is still required to be further improved.
CN106265119B discloses a polypeptide tightening and moisturizing mask and a preparation method thereof, the components include: acetyl hexapeptide 3, trideceth 1, carnosine, aloe vera, milk yeast, butylene glycol, glycerol, sodium hyaluronate, squalane, tocopherol, yellow collagen, stearic acid, month Gui Chun polyether 3, phenoxyethanol, methylparaben, ethylparaben. The three cosmetic polypeptides of acetyl hexapeptide 3, tridecyl 1 and carnosine are important nutrition components of skin, can effectively improve facial skin relaxation, and can effectively supplement nutrition components such as amino acid and the like required by epidermal cells. However, the effect of the composition is not obtained in a short time, and the effect of tightening and removing wrinkles is still required to be further improved.
Disclosure of Invention
Aiming at the problems, the water-light facial mask provided by the invention is prepared from the following raw materials: water, moisturizer, skin conditioner, antioxidant component, plant extract, and skin protectant.
Preferably, the preparation raw materials comprise, by mass: 80-100 parts of water, 5-12 parts of humectant, 0.1-5 parts of skin conditioner, 0.0001-1 part of antioxidant component, 0.05-1 part of plant extract and 0.001-0.5 part of skin protectant.
In one embodiment, the humectant is selected from one or more of a small molecule humectant, a polymeric humectant, a closed oil.
Preferably, the humectant is a combination of a small molecular humectant and a high molecular humectant, and the mass ratio is (0.2-15): (0.01-2).
The small molecule moisturizers include, but are not limited to, butylene glycol, polyethylene glycol, propylene glycol, hexylene glycol, 1, 2-pentanediol, glycerin, maltitol, polypropylene glycol, sorbitol, mannitol, glycerol glucoside; preferably mannitol, butanediol, glycerol, 1, 2-pentanediol and glyceroglycosides, the mass ratio is (0.1-1): (1-6): (0.5-4): (0.1-1): (0.1-1).
The high molecular humectant comprises, but is not limited to, pullulan, tremella polysaccharide, beta-glucan, carob seed polysaccharide and hydrolyzed sclerotium gum; preferably hydrolyzed sclerotium rolfsii.
In one embodiment, the skin conditioning agent is selected from one or more of acids, plant essential oils, vitamins.
Preferably, the skin conditioning agent is a combination of acid and plant essential oil, and the mass ratio is (10-30): (0.1-2).
The acids include, but are not limited to, tetrahydropyrimidine carboxylic acid, hyaluronic acid, salicylic acid, tretinoin, preferably, tetrahydropyrimidine carboxylic acid.
The plant essential oil comprises, but is not limited to, lime peel oil, lavender oil, cedar oil, rose oil, jasmine oil, tea tree essential oil and lemon essential oil, preferably the combination of lime peel oil, lavender oil and cedar oil, and the mass ratio is (1-10): (0.1-5): (0.1-5).
In one embodiment, the antioxidant component is selected from one or more of a polysaccharide, a coenzyme, a polypeptide.
Preferably, the antioxidant component is a polypeptide.
The polypeptides include, but are not limited to, carnosine, acetyl hexapeptide-8, palmitoyl pentapeptide-4, tetrapeptide-4, palmitoyl tripeptide-8, nonapeptide-1, acetyl octapeptide-3, tripeptide-1, conopeptide, oligopeptide-1, tripeptide-1 copper, decarboxylated carnosine, palmitoyl tetrapeptide-7, acetyl dipeptide-1, lysine polypeptides, myristoyl hexapeptide-5, snake venom peptides, preferably carnosine, acetyl hexapeptide-8, palmitoyl pentapeptide-4, tetrapeptide-4, combinations of palmitoyl tripeptide-8, mass ratios of (3-18): (0.1-3): (0.01-2): (0.01-2): (0.01-4).
In one embodiment, the plant extract is selected from one or more of Ecklonia CAVA (Ecklonia CAVA) extract, cyrtymenia Sparsa (HIZIKIA FUSIFORME) extract, philippine Sonchus extract (CODIUM TOMENTOSUM), philippine Gelidium herb (GELIDIUM CARTILAGINEUM) extract, herba Portulacae (Portulaca oleracea) extract, green tea (Camellia sinensis) extract, herba Saussureae Involueratae (Saussurea species) extract, aloe (ALOE VERA) extract, centella asiatica (Centella asiatica) extract, grapefruit (Citrus PARADISI MACF) extract, and radix Puerariae (PUERARIAE LOBATAE RADIX) extract.
Preferably, the plant extract is a combination of thallus laminariae extract, cyrtymenia Sparsa extract, sargassum fusiforme extract, gelidium amansii extract, and herba Portulacae extract, and the mass ratio is (2-10): (2-10): (2-10): (2-10): 1.
in one embodiment, the emulsifier is selected from one or more of an ionic emulsifier, a nonionic emulsifier, a natural emulsifier.
Preferably, the emulsifier is a nonionic emulsifier.
Further preferably, the nonionic emulsifier is a combination of PPG-13-decyl tetradecyl polyether-24, coco glucoside, hydroxyethyl cellulose, polysorbate-60 and PEG-40 hydrogenated castor oil, and the mass ratio is (4-10): (2-8): (2-8): (0.001-1): (0.1-5).
In one embodiment, the skin protectant is selected from one or more of sodium lauroyl amino acid, jojoba oil, stearyl alcohol, shea butter, VE, peony root, aloe, centella asiatica, licorice, amino acids, dextran, allantoin, sodium hyaluronate, squalane, beta-alanyl hydroxypropionyl diaminobutyric acid benzylamine.
Preferably beta-alanyl hydroxyproline diaminobutyric acid benzylamine.
The bioactive polypeptide compound has the advantages of high bioactivity, easy absorption, safety and no toxicity, and the physiological effects and biological effects of beautifying and protecting skin and resisting aging are gradually applied to the beautifying cosmetics. The polypeptide combination in the invention is carnosine, acetyl hexapeptide-8, palmitoyl pentapeptide-4, tetrapeptide-4 and palmitoyl tripeptide-8, and the mass ratio is (3-18): (0.1-3): (0.01-2): (0.01-2): (0.01-4) can tighten skin and reduce wrinkles within 14 days, and the reasons considered by the applicant are: acetyl hexapeptide-8 can block nerve transmission muscle contraction information locally, influence the nerve conduction of the leather bag, relax the machine flesh of the face, palmitoyl pentapeptide-4 can penetrate the dermis to increase collagen, reverse the skin aging process through rebuilding from inside to outside, tetrapeptide and palmitoyl tripeptide-8 can increase collagen generation of the skin and fiber generation in extracellular matrix, reduce wrinkle depth, and the four polypeptides act together, so that the skin can be well repaired from the inside, obvious effect can be visually brought, the carnosine has good antioxidant, anti-saccharification and anti-inflammatory effects, redundant free radicals in the skin are removed, skin aging is reduced, skin elasticity is increased, skin moisturizing is kept, pigmentation is reduced, and the five polypeptides are combined according to the mass part requirements, so that the formed wrinkles can be reduced, the further generation of the wrinkles can be prevented from the source, and quick response is achieved in 14 days.
However, the polypeptide is unstable, especially when multiple polypeptides are compounded and used, the properties of the polypeptide can be changed when external conditions such as pH, temperature, illumination, oxygen concentration and the like are changed, so that the related efficacy performance of the water-based facial mask is affected, and the applicant finds that the small molecular humectant is a combination of mannitol, butanediol, glycerol, 1, 2-pentanediol and glyceroglycosides according to a mass ratio of (0.1-1): (1-6): (0.5-4): (0.1-1): (0.1-1), the stability of the polypeptide can be well ensured. The applicant believes that the possible reasons are that the polyhydric alcohol and sugar alcohol in the small molecule moisturizer can enable more water molecules to surround the polypeptide, so that an isolating protective layer is formed outside the polypeptide, the adsorption, aggregation and precipitation of the surface of the polypeptide are prevented, and the skin barrier is easier to permeate in the skin care process, so that the skin can absorb the polypeptide components better.
In one embodiment, the raw materials for preparing the hydrooptical mask further comprise, in parts by mass: 0.01-1 part of film forming agent, 0.00001-0.5 part of pH regulator and 0.1-5 parts of preservative.
In one embodiment, the film former is an oil soluble film former and/or a water soluble film former.
Preferably, the film forming agent is a water-soluble film forming agent.
Further preferably, the film former is polyacrylate crosslinked polymer-6.
In one embodiment, the pH adjuster includes, but is not limited to, sodium hydroxide, potassium hydroxide, triethanolamine, citric acid, sodium citrate, succinic acid, disodium succinate, sodium dihydrogen phosphate, disodium hydrogen phosphate, preferably disodium hydrogen phosphate.
In one embodiment, the preservative includes, but is not limited to, 1, 2-hexanediol, p-hydroxyacetophenone, hexetidine, imidazolidinyl urea, sorbic acid, 2-furoic acid, captan, diglyme, hexeneglycol, benzalkonium chloride, chlorhexidine, benzoic acids, chlorocresol, cresols, nipagins, t-butanol, benzalkonium chloride, benzethonium chloride, carbomers, cetrimide, bronopol, chlorhexidine, butyl hydroxybenzene, methylparaben, propyl hydroxybenzoate, ethylparaben, p-chloro-meta-xylene, phenoxyethanol, sodium propionate, preferably 1, 2-hexanediol, p-hydroxyacetophenone, carbomer, in a mass ratio of (1-10): (0.5-8): (0.5-5).
The invention also discloses a preparation method of the water-light facial mask, which comprises the following steps: mixing the raw materials.
Specifically, the method comprises the following steps:
(1) In a main emulsifying pot, 80% of the total water is taken, then one half of butanediol, one third of glycerol, hydrolyzed small sclerotium gum, polyacrylate crosslinked polymer-6, carbomer, hydroxyethyl cellulose, disodium hydrogen phosphate and polysorbate-60 are sequentially added, stirring and homogenizing are started for 1-2min until no particles exist, heating is carried out to 80-85 ℃, and heat preservation is carried out for 25-30 min.
(2) Dissolving five sixths of 1, 2-hexanediol and p-hydroxyacetophenone in a container at 60-70 ℃ for standby application.
(3) Uniformly mixing PEG-40 hydrogenated castor oil, lime peel oil, lavender oil and cedar wood oil for later use.
(4) Cooling the main emulsifying pot to 60-70 ℃, adding the solution uniformly mixed in the step (2), and uniformly stirring.
(5) Cooling to 40-45 ℃, adding the rest raw materials, stirring uniformly, adding the solution uniformly mixed in the step (3), and stirring uniformly.
Advantageous effects
1. The polypeptide combination of the invention is carnosine, acetyl hexapeptide-8, palmitoyl pentapeptide-4, tetrapeptide-4 and palmitoyl tripeptide-8, which can tighten skin and reduce wrinkles within 14 days.
2. Beta-alanyl hydroxy prolyl diaminobutyric acid benzylamine is used as a skin protective agent, can promote proliferation of fibroblasts and horny layer cells, improve cell viscosity, increase synthesis of type I collagen, reduce expression of elastase, and endow skin with better compactness, so that the compacting effect is further improved.
3. The humectant is a combination of a small molecular humectant and a high molecular humectant, so that the mask has good moisture retention and is easier to continuously absorb beneficial components.
4. The plant extract and the antioxidant component are added to act together, so that the repairing effect of the mask is further improved.
5. The mask liquid is stable and has long shelf life by compounding a plurality of nonionic emulsifiers, so that the beneficial components can play a role.
Detailed Description
Example 1
The hydrolyzed ringlet gum was purchased from Shanghai Hui Biotechnology Co. The carnosine is purchased from Shenzhen Viqi technologies Inc.
The carbomers were purchased from road-blogging management (Shanghai) Inc. The polyacrylate crosslinked polymer-6 was purchased from SEPPIC s.a. The sargassum fusiforme extract is purchased from Guangzhou Bai Hao chemical industry Co. The Pinus sylvestris extract was purchased from Fangzhou Bai Hao chemical Co.
The thallus laminariae extract is purchased from Guangzhou Bai Hao chemical industry Co. The gelonin extract was purchased from chemical industry limited, baobao, guangzhou.
The PPG-13-decyl tetradecyl polyether-24 is available from Ashland LLC.
The coco glucoside was purchased from basf (china) limited.
The hydroxyethyl cellulose was purchased from taiwan technical ja refinement trade limited.
The purslane extract was purchased from BioSpectrum, inc.
The beta-alanyl hydroxypropionyl diaminobutyric acid benzylamine was purchased from Vichi technologies Inc. of Shenzhen.
The PEG-40 hydrogenated castor oil was purchased from Basiff (China) Inc.
The acetyl hexapeptide-8 is purchased from Shenzhen Vichi technologies Co.
The palmitoyl pentapeptide-4 is purchased from Shenzhen Vichi technologies Inc.
The lime peel oil was purchased from pure elegant fragrance essence limited.
The lavender oil was purchased from pure elegant fragrance essence limited.
The tetrapeptide-4 is purchased from Shenzhen Vichi technologies Inc.
The cedar wood oil was purchased from pure elegant fragrance and essence limited.
The palmitoyl tripeptide-8 is purchased from Shenzhen Vichi technologies Co., ltd.
The polysorbate-60 is available from Shenzhen Vichi technologies Inc.
The preparation method of the water-light facial mask comprises the following steps:
(1) In a main emulsifying pot, 80% of the total water is taken, then one half of butanediol, one third of glycerol, hydrolyzed small sclerotium gum, polyacrylate crosslinked polymer-6, carbomer, hydroxyethyl cellulose, disodium hydrogen phosphate and polysorbate-60 are sequentially added, stirring and homogenizing are started for 1-2min until no particles exist, heating is carried out to 80 ℃, and the temperature is kept for 30 min.
(2) Five sixths of 1, 2-hexanediol and p-hydroxyacetophenone are heated and dissolved in a container at 65 ℃ for standby.
(3) Uniformly mixing PEG-40 hydrogenated castor oil, lime peel oil, lavender oil and cedar wood oil for later use.
(4) Cooling the main emulsifying pot to 65 ℃, adding the solution uniformly mixed in the step (2), and uniformly stirring.
(5) Cooling to 40 ℃, adding the rest raw materials, stirring uniformly, adding the solution uniformly mixed in the step (3), and stirring uniformly.
Performance testing
1. Stability test: the water light mask liquid prepared in the example 1 is placed in a 50 ℃ incubator for 24 hours, and then taken out, and the product is observed to be not layered, not crystallized and good in stability.
2. Cosmetic tightening and anti-wrinkle efficacy test: according to QB/T4256-2011 cosmetic moisturizing efficacy evaluation guidelines; T/ZHCA003-2018 cosmetic affects the transepidermal water loss test method; T/TDCA003-2021 cosmetic tightening efficacy test method; a clinical evaluation method for improving the canthus line efficacy of a T/SHRH018-2019 cosmetic; liu Weiyi. Zhou Lin. Zhao Hua cosmetic efficacy evaluation (XII) -consumer use test [ J ] daily chemical industry, 2021, 51 (06): 485-490.
The detection method comprises the following steps:
healthy, dry facial skin, lack of moisture, poor skin barrier function, loose skin and lack of elasticity, fine lines or wrinkles in the corners of the eyes, 31 subjects in chinese healthy men/women according to classification 2 to 5 of SKINAGEINGATLAS, aged range 25-60 years. The moisture content of the stratum corneum, skin elasticity of the subject were measured and a partial photograph was taken before using the test product, continuously using the product of example 1 for 14 days, and for 28 days, respectively, using the method of the front and rear controls. The evaluation results before and after the product is used are compared by a statistical test method so as to judge whether the statistical difference exists.
Detection part:
(1) Skin stratum corneum moisture content-cheek;
(2) Skin elasticity R2-cheek;
(3) Primos-CR corner of eye wrinkle length-corner of eye;
(4) Primos-CR canthus wrinkle volume-canthus;
(5) Primos-CR canthus wrinkle count-canthus;
(6) Self-assessment-full face.
Detection result:
sample completion: group 31 subjects were enrolled, 30 subjects were eventually counted, and subjects numbered VT022 were enrolled for personal reasons, with 2 men, 28 women, ages 28 to 55 years, and average ages 44.77±1.42 years. After the face is cleaned, the mask of the embodiment 1 is aligned to eyes, lips are applied to dry the face, the mask cloth is attached, after 15 minutes, the mask is taken down, the skin of the face is gently massaged, and after the massage is finished, the face is cleaned by clear water for 1 time every other day.
Product usage and tolerability feedback conditions: each subject used the test sample as required within the prescribed time, and showed no adverse reaction according to the adverse reaction recording results according to 2015 edition of cosmetic safety technical Specification.
The moisture content of the skin horny layer is shown in the following table:
TABLE 1 moisture content of the stratum corneum of skin
Product(s) Basic value The product is used for 14 days The product is used for 28 days
Example 1 44.71±2.46 75.46±1.52 72.01±1.31
TABLE 2 moisture content improvement Rate of skin stratum corneum
Skin elasticity R2 is shown in the following table:
TABLE 3 skin elasticity R2 test results
Product(s) Basic value The product is used for 14 days The product is used for 28 days
Example 1 57.63±1.16 66.67±1.38 64.25±1.18
TABLE 4 skin elasticity R2 improvement Rate
Product(s) The product is used for 14 days The product is used for 28 days
Example 1 15.68％ 11.48％
Primos-CR canthus wrinkle count is shown in the following Table:
TABLE 5 Primos-CR canthus wrinkle count
Product(s) Basic value The product is used for 14 days The product is used for 28 days
Example 1 5.00±0.12 3.50±0.17 3.10±0.21
TABLE 6 Primos-CR canthus wrinkle improvement Rate
Product(s) The product is used for 14 days The product is used for 28 days
Example 1 30.00％ 38.00％
Primos-CR canthus wrinkle volumes are shown in the following table:
TABLE 7 Primos-CR canthus wrinkle volumes
Product(s) Basic value The product is used for 14 days The product is used for 28 days
Example 1 8.19±0.43 7.18±0.49 6.52±0.52
TABLE 8 Primos-CR canthus wrinkle volume improvement Rate
Product(s) The product is used for 14 days The product is used for 28 days
Example 1 12.23％ 20.38％
Primos-CR canthus wrinkle lengths are shown in the following Table:
TABLE 9 Primos-CR canthus wrinkle Length
Product(s) Basic value The product is used for 14 days The product is used for 28 days
Example 1 40.43±2.51 36.67±2.11 35.87±2.35
TABLE 10 Primos-CR canthus wrinkle Length improvement Rate
Product(s) The product is used for 14 days The product is used for 28 days
Example 1 9.32％ 11.29％
For 28 days of continuous use of the test product, 96.67% of subjects felt the product to have a tightening effect after use; 86.67% of the subjects feel anti-wrinkle efficacy after use of the product; 100.00% of subjects feel the product has moisturizing effect after using, 90.00% of subjects feel the product can improve the compactness of facial skin after using; 96.67% of subjects feel the product to be used, the facial skin elasticity can be enhanced, 86.67% of subjects feel the product to be used, and the effect of reducing wrinkles is achieved; 93.33% of subjects feel the product improved skin smoothness after use; 100.00% of the subject sensory products can achieve the effect of moisturizing the skin, 96.67% of the subject sensory products are easy to absorb; 90.00% of subjects feel the product as good in skin feel; 100.00% of subjects considered the product to be mild and non-irritating; 100.00% of the subjects were satisfied with the overall product.

Claims (10)

1. The water-light facial mask is characterized by comprising the following preparation raw materials: water, moisturizer, skin conditioner, antioxidant component, plant extract, and skin protectant.
2. The hydrographic mask of claim 1, wherein the moisturizer is selected from one or more of a small molecule moisturizer, a high molecule moisturizer, and a occlusive oil.
3. The water-light facial mask according to claim 2, wherein the humectant is a combination of a small molecular humectant and a high molecular humectant, and the mass ratio is (0.2-15): (0.01-2).
4. The hydrographic mask of claim 1, wherein the skin conditioning agent is selected from one or more of acids, plant essential oils, vitamins.
5. The hydrographic mask of claim 1, wherein the antioxidant component is selected from one or more of a polysaccharide, a coenzyme, a polypeptide.
6. The hydrographic mask of claim 5, wherein the polypeptide is a combination of carnosine, acetyl hexapeptide-8, palmitoyl pentapeptide-4, tetrapeptide-4, palmitoyl tripeptide-8, in a mass ratio of (3-18): (0.1-3): (0.01-2): (0.01-2): (0.01-4).
7. The hydrographic mask of claim 1, wherein the plant extract is selected from one or more of kelp extract, sargassum fusiforme extract, pinus maladsura extract, gelonin extract, purslane extract, green tea extract, saussurea involucrata extract, aloe extract, centella extract, grapefruit extract, kudzuvine root extract.
8. The hydrographic mask of claim 1, wherein the emulsifier is selected from one or more of an ionic emulsifier, a nonionic emulsifier, a natural emulsifier.
9. The hydrographic mask according to any one of claims 1-8, wherein the hydrographic mask further comprises: film forming agent, pH regulator and antiseptic.
10. A method of preparing a hydrographic mask according to claim 9, comprising the steps of: mixing the raw materials.
CN202310853358.8A 2023-07-12 2023-07-12 Water-light mask and preparation method thereof Pending CN116889528A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117357450A (en) * 2023-12-08 2024-01-09 珠海金肽生物科技有限公司 Composition for improving skin aging relaxation and preparation method and application thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117357450A (en) * 2023-12-08 2024-01-09 珠海金肽生物科技有限公司 Composition for improving skin aging relaxation and preparation method and application thereof
CN117357450B (en) * 2023-12-08 2024-04-16 珠海金肽生物科技有限公司 Composition for improving skin aging relaxation and preparation method and application thereof

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