CN115804736B - Multi-effect lip balm and preparation method thereof - Google Patents
Multi-effect lip balm and preparation method thereof Download PDFInfo
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- CN115804736B CN115804736B CN202211604906.5A CN202211604906A CN115804736B CN 115804736 B CN115804736 B CN 115804736B CN 202211604906 A CN202211604906 A CN 202211604906A CN 115804736 B CN115804736 B CN 115804736B
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- 238000002360 preparation method Methods 0.000 title abstract description 13
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- Cosmetics (AREA)
Abstract
The application discloses a multi-effect lip balm and a preparation method thereof, wherein the multi-effect lip balm comprises a low molecular weight gel, octyl dodecanol, a skin conditioner, an emollient, diisostearyl malate, a radix arnebiae extract, a calendula extract, a tea extract, white pool flower seed oil and sunflower seed oil; the preparation method of the multi-effect lip balm comprises the following steps: stirring the low molecular weight gel and octyl dodecanol to obtain a phase A preform; step two, stirring sunflower seed oil, lithospermum root extract, calendula extract, tea extract and white pond flower seed oil to obtain a phase B preform; stirring the phase A prefabricated product and the phase B prefabricated product to obtain a phase C prefabricated product; and step four, adding the emollient and the skin conditioner into the C-phase preformed product, and pouring the preformed product into a mould for cooling and forming to obtain the multi-effect lip gloss. The multifunctional lip care product has the effects of caring lips and rapidly weakening pigmentation of lips.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a multi-effect lip balm and a preparation method thereof.
Background
The mouth is one of the five sense organs of the human body, and the condition of the lips directly affects the external qi quality of the individual, so that the maintenance and modification of the lips are important. Healthy lips are ruddy and glossy, are suitable for being dried and wet, have no cracks, and can enable a human body to be exposed to natural good gas color.
Most women today choose to apply lipstick in daily life, making the lips more attractive and adding to the charm of the individual. The lipstick mainly comprises components such as wax, dye, essence and the like, contains a large number of complex chemical components, is easy to cause lip inflammation after long-term use, causes lip chapping and lip skin peeling, and seriously damages the health of lips. Meanwhile, a large amount of artificial pigments and other components contained in the lipstick can permeate into the skin of the lips, so that the pigments of the lips are deposited, and the lips are dark and blackened.
In order to better care the lips, many people choose to apply lip gloss after removal of makeup. Most lip balms on the market at present only have the effect of preserving moisture and moistening lips, and are difficult to meet the demands of people who smear lipstick for a long time on lip care, so that a lip balm capable of multiple-effect lip care is needed.
Disclosure of Invention
In order to achieve the purpose of multi-effect lip care, the application aims at the effects of the sunflower seed oil, the lithospermum root extract, the calendula extract, the tea extract and the white pool flower seed oil compounded multi-effect lip gloss after lip care research, has the unexpected effect of quickly fading lip pigmentation, and simultaneously achieves the purpose of multi-effect lip care by being assisted with the effects of the sunflower seed oil, the lithospermum root extract, the calendula extract, the tea extract and the white pool flower seed oil.
In a first aspect, the application provides a multi-effect lip balm, which adopts the following technical scheme:
a multi-effect lip balm comprises the following raw materials in percentage by mass:
In the technical scheme, the lithospermum root extract has the effects of moistening skin, relieving dryness, detumescence and relieving itching; the calendula extract is beneficial to dry or damaged skin, and can promote the rapid healing and regeneration of the skin; the tea extract is rich in tea polyphenol, so that the tea extract has the effects of relieving skin aging, resisting bacteria and diminishing inflammation; the white pond flower seed oil can repair the barrier of damaged skin and promote the metabolism of the skin.
Sunflower seed oil is one of oils with the highest unsaturated fatty acid content, the unsaturated fatty acid content is up to 85%, the content of linoleic acid in the types of the unsaturated fatty acid is the highest, and the linoleic acid has the effects of enhancing the skin barrier function, improving the skin immunity and increasing the skin permeability; the alpha-tocopherol content in the sunflower seed oil is higher than that of common vegetable oil, and the linoleic acid and the alpha-tocopherol in the sunflower seed oil are in a balanced proportion which is just suitable for human body absorption, so that the sunflower seed oil is more convenient for human body absorption and utilization, has the effects of lubricating skin and fading lips, and has the anti-inflammatory effect of promoting skin wound healing.
According to the technical scheme, the multiple-effect lip balm compounded by the lithospermum root extract, the calendula extract, the tea extract, the white pool flower seed oil and the sunflower seed oil can obviously improve dark and blackish lips caused by pigmentation, has an obvious effect of fading pigmentation of lips, can maintain a good appearance and an odor state of the multiple-effect lip balm for a long time, ensures that the peroxide value in the multiple-effect lip balm is in a reasonable range, and overcomes the defect that the sunflower seed oil is easy to rancid and give off odor due to the fact that the unsaturated fatty acid content is too high. The effects of the five natural plant extracts are assisted, so that the purpose of caring lips from multiple angles of moistening, moisturizing, relieving, repairing and fading lips is achieved.
Preferably, the mass ratio of the lithospermum root extract to the calendula extract to the tea leaf extract to the white pool flower seed oil is 1:10:12:35.
According to the technical scheme, the multi-effect lip balm obtained according to the proportion has the effect of more rapidly fading pigment deposition of lips, and can more effectively improve dark blackening of lips.
Preferably, the low molecular weight gel is prepared from dibutyl lauroyl glutamine and dibutyl ethyl hexanoyl glutamine according to a mass ratio of 1:1, and is compounded according to the proportion.
According to the technical scheme, dibutyl lauroyl glutamine and dibutyl ethyl hexanoyl glutamine are used as low-molecular-weight gel of the multi-effect lip balm according to the proportion, and the folding resistance of the multi-effect lip balm is further enhanced on the basis of not changing the ductility of the multi-effect lip balm.
Preferably, the mass ratio of dibutyl lauroyl glutamine, dibutyl ethyl hexanoyl glutamine and octyl dodecanol is 1:1:12.
According to the technical scheme, the multi-effect lip balm prepared according to the proportion has more transparent paste and better smearing ductility, the smoothness is higher during smearing, and meanwhile, the smell of the multi-effect lip balm is blended to be proper.
Preferably, the emollient comprises at least hydrogenated castor oil dimer linoleate, phytosterol/octyldodecanol lauroyl glutamate.
In the technical scheme, the hydrogenated castor oil dimer linoleate and the phytosterin/octyl dodecanol lauroyl glutamate are high-viscosity grease, wherein the hydrogenated castor oil dimer linoleate has good skin adhesiveness, can form a long-acting moisturizing film on lips, and can maintain the humidity of lips after sunflower seed oil is moisturized; the phytosterol/octyl dodecanol lauroyl glutamate has good skin moisturizing property, can be further combined with hydrogenated castor oil dimer linoleate to form a protective film with longer moisturizing effect on lips, and can better lock oil content and prolong moisturizing time.
Preferably, the skin conditioner at least comprises bisabolol, stearyl glycyrrhetinate, wherein the mass ratio of the bisabolol to the stearyl glycyrrhetinate is 1:1.
In the technical scheme, bisabolol and stearyl glycyrrhetinate from plants are prepared by the steps of 1:1 can provide excellent anti-inflammatory effect for lips, and solve the problems of lip inflammation and allergy.
Preferably, the skin conditioning agent further comprises sodium hyaluronate.
According to the technical scheme, the sodium hyaluronate is added into the multi-effect lip balm, so that the permeability of lips is further improved, the absorption capacity of the lips to other effective components is improved, and the lip care effect of the multi-effect lip balm is further improved.
In a second aspect, the application provides a preparation method of a multi-effect lip balm, which adopts the following technical scheme:
A preparation method of a multi-effect lip balm comprises the following steps:
1) Uniformly stirring the low molecular weight gel and octyl dodecanol at the temperature of between 90 and 100 ℃ to obtain a phase A preform;
2) Uniformly stirring sunflower seed oil, lithospermum root extract, calendula extract, tea extract and white pond flower seed oil at 70-80 ℃ to obtain a phase B preform;
3) Mixing the phase A preform and the phase B preform at 70-80 ℃ and fully and uniformly stirring at 30-40 r/min to obtain a phase C preform;
4) Adding the emollient and the skin conditioner into the phase C preform, and uniformly stirring at 70-75 ℃ to obtain a phase D preform;
5) And pouring the D-phase preform into a specific mold, and cooling and forming to obtain the multi-effect lip balm.
According to the technical scheme, the multi-effect lip balm prepared by the preparation method maintains the performances of all raw materials to the maximum extent, and meanwhile, the prepared multi-effect lip balm has clear and transparent paste, good moistening degree and high melting point.
Preferably, the preparation method of the B-phase preform in the step 2) comprises the following steps: uniformly stirring sunflower seed oil, lithospermum root extract, calendula extract, tea extract and white pond flower seed oil at 70-80 ℃, and standing at 75-80 ℃ for 0.2-0.5 h to obtain a phase B preform.
According to the technical scheme, the sunflower seed oil, the lithospermum root extract, the calendula extract, the tea extract and the white pool flower seed oil are kept stand for 0.2-0.5 h at the temperature of 75-80 ℃, so that fusion of the lithospermum root extract, the calendula extract, the tea extract, the white pool flower seed oil and the sunflower seed oil can be further promoted, and the sunflower seed oil has an excellent effect of preventing rancidity.
Preferably, the preparation method of the D-phase preform in the step 4) comprises the following steps: adding the emollient and the skin conditioner into the phase C preform, stirring uniformly at 70-75 ℃, and sieving with a 300-mesh sieve to obtain the phase D preform.
According to the technical scheme, the D-phase preformed product is sieved by a 300-mesh sieve, so that impurities in the lipstick preparation process can be further filtered, the impurities in the prepared multi-effect lip balm are further reduced, and the prepared multi-effect lip balm is provided with a cleaner paste.
In summary, the present application includes at least one of the following beneficial technical effects:
1. according to the technical scheme, the multi-effect lip balm added with sunflower seed oil, lithospermum root extract, calendula extract, tea leaf extract and white pond flower seed oil can obviously improve dark blackening of lips caused by melanin precipitation, has an obvious effect of fading pigment deposition of lips, and achieves the purpose of multi-angle lip care from moistening, moisturizing, relieving, repairing and fading lips by being supplemented with the effects of the five natural plant extracts.
2. The mass ratio of dibutyl lauroyl glutamine to dibutyl ethyl caproyl glutamine to octyl dodecanol is 1:1:12, the anti-folding capability of the multi-effect lip balm can be further enhanced, meanwhile, the multi-effect lip balm has more transparent paste and better smearing ductility, and the smell of the multi-effect lip balm is blended to be proper.
3. Hydrogenated castor oil dimer linoleate and phytosterol/octyldodecanol lauroyl glutamate are both high viscosity oils, wherein the hydrogenated castor oil dimer linoleate has good skin adhesion, can form a long-acting moisturizing film on lips, and can maintain the humidity of lips after sunflower seed oil is moisturized; the phytosterol/octyl dodecanol lauroyl glutamate has good skin moisturizing property, can be further combined with hydrogenated castor oil dimer linoleate to form a protective film with longer moisturizing effect on lips, and can better lock oil content and prolong moisturizing time.
Detailed Description
The materials in the following examples and comparative examples were all commercially available.
Examples 1 to 3
A multi-effect lip balm is composed of the following raw materials:
low molecular weight gels, emollients, skin conditioning agents, octyldodecanol, diisostearyl malate, radix Arnebiae extract, calendula extract, tea extract, white pool seed oil, sunflower seed oil.
Wherein the low molecular weight gel is compounded by dibutyl lauroyl glutamine and dibutyl lauroyl glutamine.
Wherein, the emollient is compounded by hydrogenated castor oil dimer linoleate, phytosterol/octyl dodecanol lauroyl glutamate.
Wherein the skin conditioner is compounded by bisabolol, stearyl glycyrrhetinate and sodium hyaluronate.
Wherein, radix Arnebiae extract is purchased from Guangzhou teno Biotechnology Co., ltd (D430 radix Lithospermi oil HL-045).
Wherein the calendula extract was purchased from the biotechnology company, jia Chuan, guangzhou (oil-soluble calendula extract-J).
Among them, tea leaf extract was purchased from the biotechnology company of Jia Chuan, guangzhou (oil-soluble Linzhi tea extract-Z).
Wherein, the white pool flower seed oil is purchased from Guangzhou Zhongbo New Material Co.
Among them, sunflower seed oil was purchased from baobao limited (BV 80).
Wherein, the bisabolol, stearyl glycyrrhetinate is purchased from Guangzhou He vast Biotechnology Co.
The example discloses a multi-effect lip balm, the proportion of each raw material is shown in table 1:
table 1 examples 1-3A Multi-effect lip balm raw Material formulation
The embodiment also discloses a preparation method of the multi-effect lip balm, which comprises the following steps:
Step 1), stirring low molecular weight gel and octyl dodecanol for 30min at 100 ℃ to obtain a phase A preform;
Step 2) stirring sunflower seed oil, radix arnebiae root extract, calendula extract, tea extract and white pond flower seed oil at 80 ℃ for 20min to obtain a phase B preform;
step 3) mixing the A-phase preform and the B-phase preform at 80 ℃ and stirring at 40r/min for 30min to obtain a C-phase preform;
step 4) adding an emollient and a skin conditioner into the phase C preform, and stirring at 75 ℃ for 20min at 35r/min to obtain a phase D preform;
And 5) pouring the D-phase preform into a mould, and cooling and forming to obtain the multi-effect lip balm.
Example 4
In a multi-effect lip balm, the amount of dibutyl lauroyl glutamine was 3kg, the amount of dibutyl ethyl hexanoyl glutamine was 3kg, and the amount of octyl dodecanol was 36kg, unlike example 1.
Example 5
Unlike example 1, in a preparation method of a multi-effect lip balm, step 2 becomes: stirring sunflower seed oil, radix Arnebiae extract, herba Sidae Rhombifoliae extract, folium Camelliae sinensis extract, and BAIHUA seed oil at 80deg.C for 20min, and standing at 75deg.C for 0.5 hr to obtain phase B preform.
Step 4 becomes: adding emollient and skin conditioner into the phase C preform, stirring at 75deg.C for 20min at 35r/min, and sieving with 300 mesh sieve to obtain phase D preform.
Comparative example 1
Unlike example 1, the arnebia root extract was replaced with aloe extract in equal amounts.
The aloe extract is commercially available and is prepared by a water extraction method, and the proportion of aloe extract is 1:10.
Comparative example 2
The difference from example 1 is that the calendula extract is replaced by kapok extract in equal amounts.
Kapok extract is commercially available and is prepared by a water extraction method, and the proportion of the kapok extract is 1:10.
Comparative example 3
The difference from example 1 is that the tea extract is replaced by the jasmine extract in equal amount.
The jasmine flower extract is commercially available and is prepared by a water extraction method, and the proportion of the jasmine flower extract is 1:10.
Comparative example 4
Unlike example 1, the white pool seed oil was replaced with jojoba oil in equal amounts.
Comparative example 5
Unlike example 1, sunflower seed oil was replaced by olive oil in equal amounts.
Comparative example 6
Unlike example 1, the arnebia root extract, calendula extract, tea extract, and white pool seed oil were replaced with sunflower seed oil in equal amounts.
Experiment 1
The appearance and the smell of the multi-effect lip balm are detected by adopting a sensory experiment, and the peroxide value of the multi-effect lip balm is detected by adopting a GBT26513-2011 detection method.
The experimental method comprises the following steps: the detection period of appearance, smell and peroxide value is 180 days, the lip balms in the examples and the comparative examples are taken out uniformly at random daily time points in the 180 days, the paste of the lip balm is kept stand for 10min in an indoor environment with the temperature of 36 ℃ and the humidity of 99%, and the lip balm is respectively stored in a lip balm shell at normal temperature for the rest time.
The above-mentioned indexes were detected by 10 testers on days 1 and 180 for the multi-effect lip balms of the above examples and comparative examples, respectively, sensory evaluation criteria are shown in table 2, experimental results are shown in table 3, the experimental results are averaged, and a change rate (%) of the detection results is calculated, the change rate (%) = [ (180-1) 1/100%.
TABLE 2 sensory evaluation criteria
TABLE 3 detection results of appearance, smell and peroxide value of Multi-effect lip balm
Table 3 shows that the multi-effect lip balms of examples 1-5 can maintain good appearance and smell for a long time in the use state, and the peroxide value of the lip balms can always meet the requirement that the peroxide value (%) in GBT26513-2011 is less than or equal to 0.2.
The comparison of the example 1 and the comparative examples 1-6 shows that only the auxiliary agent compounded by simultaneously adding the radix arnebiae extract, the calendula extract, the tea extract and the white pool seed oil can obviously improve the defects that the multi-effect lip balm taking sunflower seed oil as the main raw material is easy to deteriorate and emits peculiar smell.
Experiment 2
The skin melanin tester (Mexameter) tests the effect of the multi-effect lip gloss on lightening the lip color, and when the test data is less than or equal to 35, the lip color is restored to the normal state.
The experimental object: 110 healthy people between 30 and 40 years old are selected, and the raw materials in the above examples and comparative examples have no allergic history, no cheilitis, long-term lipstick smearing and dark and black lips.
The experimental method comprises the following steps:
Volunteers were divided into 11 groups of 10 persons each, after face cleaning in the morning and evening, lip balms in the above examples and comparative examples were uniformly applied to lips (in order to prevent deterioration of lip balms in use, lip balms of each comparative example were replaced once every week), and skin melanin test was performed every two weeks for 4 weeks continuously, the detected part was the middle part of the lip of the lower lip, test data was recorded, average values were taken for each group, and a fade rate (%) was calculated, and the calculation method: desalination rate (%) = [ (pre-use test data-post-use test data)/pre-use test data ] ×100% and experimental results are shown in table 4.
TABLE 4 multiple effect lip gloss lightening effect
Table 4 shows that the multi-effect lip balms of examples 1-5 have excellent and rapid effects of improving darkening of the lips.
Experiment 3
Sensory evaluation tests the extensibility, adhesive force, moistening degree and sense of transparency of the multi-effect lip balm.
The experimental object: 110 healthy people between 30 and 40 years old are selected, and the raw materials in the above examples and comparative examples have no allergic history, no cheilitis, long-term lipstick smearing and dark and black lips.
The experimental method comprises the following steps: volunteers were divided into 11 groups of 10 persons each, and after face washing at night, lip balms in the above examples and comparative examples were evenly applied to lips for satisfaction scoring: very satisfactory was 4 points, satisfactory was 3 points, generally 2 points, the difference was 1 point, the evaluation results of each group were averaged, and the experimental results are shown in Table 5.
TABLE 5 evaluation results of extensibility, adhesion, moisturization, and clear feel of Multi-effect lip balm
| Group of | Ductility | Adhesion force | Degree of moistening | Clear sense of penetration | Total score |
| Example 1 | 3.5 | 3.7 | 3.6 | 3.4 | 14.2 |
| Example 2 | 3.6 | 3.8 | 3.7 | 3.3 | 14.4 |
| Example 3 | 3.7 | 3.8 | 3.8 | 3.5 | 14.8 |
| Example 4 | 3.9 | 3.7 | 3.9 | 3.4 | 14.9 |
| Example 5 | 4.0 | 3.7 | 3.6 | 4.0 | 15.3 |
| Comparative example 1 | 3.1 | 3.4 | 3.3 | 2.2 | 12.0 |
| Comparative example 2 | 2.9 | 3.5 | 3.6 | 2.4 | 12.4 |
| Comparative example 3 | 3.2 | 3.3 | 3.5 | 2.5 | 12.5 |
| Comparative example 4 | 2.7 | 3.6 | 3.4 | 2.6 | 12.3 |
| Comparative example 5 | 2.4 | 3.5 | 3.8 | 2.5 | 12.2 |
| Comparative example 6 | 2.8 | 3.8 | 3.7 | 2.1 | 12.4 |
Table 5 shows that the multi-effect lip balms of examples 1-6 have good extensibility, adhesion, moisturization and feel of clarity.
The present embodiment is only for explanation of the present application and is not to be construed as limiting the present application, and modifications to the present embodiment, which may not creatively contribute to the present application as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present application.
Claims (4)
1. A multi-effect lip balm is characterized by comprising the following raw materials in percentage by mass:
Low molecular weight gelling agent: 4% -8%;
Octyl dodecanol: 35% -40%;
Skin conditioning agent: 0.5% -1%;
diisostearyl malate: 8% -12%;
radix Arnebiae extract: 0.1% -0.3%;
calendula extract: 1% -2%;
tea extract: 1% -1.5%;
White pond flower seed oil: 3% -4%;
sunflower seed oil: 25% -28%;
the emollient is the rest;
The low molecular weight gel is compounded by dibutyl lauroyl glutamine and dibutyl ethyl caproyl glutamine;
The emollient is compounded by hydrogenated castor oil dimer linoleate, phytosterol/octyl dodecanol lauroyl glutamate;
the skin conditioner is prepared by compounding bisabolol, stearyl glycyrrhetinate and sodium hyaluronate.
2. The multi-effect lip balm according to claim 1, wherein the mass ratio of the lithospermum extract, the calendula extract, the tea extract and the white pool seed oil is 1:10:12:35.
3. The multi-effect lip balm according to claim 1, wherein the low molecular weight gel is prepared from dibutyl lauroyl glutamine, dibutyl ethyl hexanoyl glutamine in a mass ratio of 1:1, and is compounded according to the proportion.
4. A multi-effect lip balm according to claim 3, characterized in that said dibutyl lauroyl glutamine, dibutyl ethyl caproyl glutamine, octyl dodecanol have a mass ratio of 1:1:12.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1328813A (en) * | 2000-06-20 | 2002-01-02 | 协和发酵工业株式会社 | Cosmetics |
| CN109394573A (en) * | 2018-12-27 | 2019-03-01 | 唯客乐化妆品(杭州)有限公司 | A kind of transparent lipstick and its preparation process |
| CN109875928A (en) * | 2019-02-27 | 2019-06-14 | 广州尚姿化妆品有限公司 | A kind of rich lip lip gloss and preparation method thereof |
| CN115089536A (en) * | 2022-07-21 | 2022-09-23 | 大疆(天津)国际贸易有限公司 | Moisturizing cream with anti-aging effect strengthening effect and preparation method thereof |
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| RU2727039C2 (en) * | 2014-08-20 | 2020-07-17 | СЭМЬЮМЕД, ЭлЭлСи | Gamma-diketones for treating and preventing skin aging and wrinkles |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1328813A (en) * | 2000-06-20 | 2002-01-02 | 协和发酵工业株式会社 | Cosmetics |
| CN109394573A (en) * | 2018-12-27 | 2019-03-01 | 唯客乐化妆品(杭州)有限公司 | A kind of transparent lipstick and its preparation process |
| CN109875928A (en) * | 2019-02-27 | 2019-06-14 | 广州尚姿化妆品有限公司 | A kind of rich lip lip gloss and preparation method thereof |
| CN115089536A (en) * | 2022-07-21 | 2022-09-23 | 大疆(天津)国际贸易有限公司 | Moisturizing cream with anti-aging effect strengthening effect and preparation method thereof |
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