CN115678291B - 抗脱落剂及其制备方法和应用 - Google Patents
抗脱落剂及其制备方法和应用 Download PDFInfo
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- CN115678291B CN115678291B CN202110847288.6A CN202110847288A CN115678291B CN 115678291 B CN115678291 B CN 115678291B CN 202110847288 A CN202110847288 A CN 202110847288A CN 115678291 B CN115678291 B CN 115678291B
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- 238000002360 preparation method Methods 0.000 title claims abstract description 14
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- -1 nitrogen-containing aromatic compound Chemical class 0.000 claims abstract description 59
- 238000002156 mixing Methods 0.000 claims abstract description 34
- 229920005989 resin Polymers 0.000 claims abstract description 21
- 239000011347 resin Substances 0.000 claims abstract description 21
- 239000007822 coupling agent Substances 0.000 claims abstract description 17
- FACXGONDLDSNOE-UHFFFAOYSA-N buta-1,3-diene;styrene Chemical compound C=CC=C.C=CC1=CC=CC=C1.C=CC1=CC=CC=C1 FACXGONDLDSNOE-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000463 material Substances 0.000 claims abstract description 16
- 229920000468 styrene butadiene styrene block copolymer Polymers 0.000 claims abstract description 16
- 239000005038 ethylene vinyl acetate Substances 0.000 claims abstract description 15
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- 238000001125 extrusion Methods 0.000 claims description 10
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- 239000000203 mixture Substances 0.000 claims description 8
- JUJWROOIHBZHMG-UHFFFAOYSA-N pyridine Substances C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 8
- IANQTJSKSUMEQM-UHFFFAOYSA-N 1-benzofuran Chemical compound C1=CC=C2OC=CC2=C1 IANQTJSKSUMEQM-UHFFFAOYSA-N 0.000 claims description 6
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims description 6
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims description 6
- 239000010692 aromatic oil Substances 0.000 claims description 5
- 150000002734 metacrylic acid derivatives Chemical class 0.000 claims description 5
- ZRMMVODKVLXCBB-UHFFFAOYSA-N 1-n-cyclohexyl-4-n-phenylbenzene-1,4-diamine Chemical compound C1CCCCC1NC(C=C1)=CC=C1NC1=CC=CC=C1 ZRMMVODKVLXCBB-UHFFFAOYSA-N 0.000 claims description 4
- WDQMWEYDKDCEHT-UHFFFAOYSA-N 2-ethylhexyl 2-methylprop-2-enoate Chemical compound CCCCC(CC)COC(=O)C(C)=C WDQMWEYDKDCEHT-UHFFFAOYSA-N 0.000 claims description 4
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- MVZWLBUGTZKZMN-UHFFFAOYSA-N pyrimidine-4,6-diamine;hydrochloride Chemical compound Cl.NC1=CC(N)=NC=N1 MVZWLBUGTZKZMN-UHFFFAOYSA-N 0.000 claims description 4
- VHMLWEBEDKTKOQ-UHFFFAOYSA-N 5,6-diamino-1h-pyrimidine-2,4-dione;hydrochloride Chemical compound Cl.NC=1NC(=O)NC(=O)C=1N VHMLWEBEDKTKOQ-UHFFFAOYSA-N 0.000 claims description 3
- WOBHKFSMXKNTIM-UHFFFAOYSA-N Hydroxyethyl methacrylate Chemical compound CC(=C)C(=O)OCCO WOBHKFSMXKNTIM-UHFFFAOYSA-N 0.000 claims description 3
- UTGQNNCQYDRXCH-UHFFFAOYSA-N N,N'-diphenyl-1,4-phenylenediamine Chemical compound C=1C=C(NC=2C=CC=CC=2)C=CC=1NC1=CC=CC=C1 UTGQNNCQYDRXCH-UHFFFAOYSA-N 0.000 claims description 3
- OUBMGJOQLXMSNT-UHFFFAOYSA-N N-isopropyl-N'-phenyl-p-phenylenediamine Chemical compound C1=CC(NC(C)C)=CC=C1NC1=CC=CC=C1 OUBMGJOQLXMSNT-UHFFFAOYSA-N 0.000 claims description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 3
- 150000004645 aluminates Chemical class 0.000 claims description 3
- SUPCQIBBMFXVTL-UHFFFAOYSA-N ethyl 2-methylprop-2-enoate Chemical compound CCOC(=O)C(C)=C SUPCQIBBMFXVTL-UHFFFAOYSA-N 0.000 claims description 3
- 229920006122 polyamide resin Polymers 0.000 claims description 3
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims description 3
- 150000003505 terpenes Chemical class 0.000 claims description 3
- 235000007586 terpenes Nutrition 0.000 claims description 3
- IIVYOQGIZSPVFZ-UHFFFAOYSA-N 2,5-diamino-4-hydroxy-1h-pyrimidin-6-one;hydrochloride Chemical compound Cl.NC1=NC(O)=C(N)C(=O)N1 IIVYOQGIZSPVFZ-UHFFFAOYSA-N 0.000 claims description 2
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 2
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 2
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 2
- 238000002844 melting Methods 0.000 claims description 2
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- 229920001568 phenolic resin Polymers 0.000 claims description 2
- 239000005011 phenolic resin Substances 0.000 claims description 2
- 229920001225 polyester resin Polymers 0.000 claims description 2
- 239000004645 polyester resin Substances 0.000 claims description 2
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 2
- RJCJNXXYYTWFCM-UHFFFAOYSA-N 2,4-diaminopyrimidin-5-ol dihydrochloride Chemical compound Cl.Cl.Nc1ncc(O)c(N)n1 RJCJNXXYYTWFCM-UHFFFAOYSA-N 0.000 claims 1
- YGBLNCKLYAIPQB-UHFFFAOYSA-N 2-tert-butyl-4-(2,2-dimethylpropyl)phenol Chemical compound CC(C)(C)CC1=CC=C(O)C(C(C)(C)C)=C1 YGBLNCKLYAIPQB-UHFFFAOYSA-N 0.000 claims 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 claims 1
- GLDOVTGHNKAZLK-UHFFFAOYSA-N n-octadecyl alcohol Natural products CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims 1
- 235000011837 pasties Nutrition 0.000 abstract description 5
- 238000004088 simulation Methods 0.000 description 14
- 238000002474 experimental method Methods 0.000 description 13
- 239000011384 asphalt concrete Substances 0.000 description 10
- 238000000605 extraction Methods 0.000 description 6
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 5
- 230000035515 penetration Effects 0.000 description 5
- 229910000831 Steel Inorganic materials 0.000 description 4
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- 239000010959 steel Substances 0.000 description 4
- 238000007664 blowing Methods 0.000 description 3
- 238000004523 catalytic cracking Methods 0.000 description 3
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- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
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- 240000000059 Vitex cofassus Species 0.000 description 1
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- 235000009347 chasteberry Nutrition 0.000 description 1
- 239000004567 concrete Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
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- 230000005484 gravity Effects 0.000 description 1
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- 239000003999 initiator Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- SSDSCDGVMJFTEQ-UHFFFAOYSA-N octadecyl 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 SSDSCDGVMJFTEQ-UHFFFAOYSA-N 0.000 description 1
- 150000004989 p-phenylenediamines Chemical class 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000011342 resin composition Substances 0.000 description 1
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- 230000035882 stress Effects 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 238000003878 thermal aging Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Abstract
Description
物料重量/kg | 实施例1 | 实施例2 | 实施例3 | 实施例4 |
苯乙烯-丁二烯-苯乙烯共聚物 | 31.0 | 65.0 | 42.0 | 88.0 |
乙烯-醋酸乙烯共聚物 | 31.0 | 55.0 | 42.0 | 68.0 |
树脂 | 71.0 | 105.0 | 72.0 | 130.0 |
含氮芳香族化合物 | 31.0 | 55.0 | 42.0 | 68.0 |
对苯二胺类化合物 | 21.0 | 40.0 | 32.0 | 48.0 |
偶联剂 | 6.1 | 8.0 | 7.2 | 8.8 |
受阻酚类化合物 | 6.1 | 8.0 | 7.2 | 8.8 |
甲基丙烯酸酯类化合物 | 41.0 | 60.0 | 52.0 | 68.0 |
芳烃油 | 31.0 | 105.0 | 42.0 | 160.0 |
黏附强度/ psi | 实施例5 | 实施例6 | 实施例7 | 实施例8 | 比较例1 | 比较例2 |
未进行模拟实验 | 478 | 498 | 493 | 508 | 380 | 439 |
模拟实验后 | 498 | 523 | 511 | 537 | 308 | 314 |
Claims (15)
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CN115677267B (zh) * | 2021-07-27 | 2023-10-10 | 中国石油化工股份有限公司 | 抗脱落剂、抗脱落驱鸟沥青混合料及其制备方法 |
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WO2008002869A2 (en) * | 2006-06-26 | 2008-01-03 | Sabic Innovative Plastics Ip B.V. | Compositions and methods for polymer composites |
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CN107383907A (zh) * | 2017-08-22 | 2017-11-24 | 江苏中路交通科学技术有限公司 | 一种温拌高模量沥青改性剂、制备方法及其应用 |
CN111748211A (zh) * | 2020-08-06 | 2020-10-09 | 上海缤德新材料科技有限公司 | 一种自粘性改性沥青及其制备方法 |
CN113004708A (zh) * | 2019-12-20 | 2021-06-22 | 常州利尔德通新材料科技有限公司 | 一种沥青抗剥落剂及其制备方法 |
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- 2021-07-27 CN CN202110847288.6A patent/CN115678291B/zh active Active
Patent Citations (11)
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WO2008002869A2 (en) * | 2006-06-26 | 2008-01-03 | Sabic Innovative Plastics Ip B.V. | Compositions and methods for polymer composites |
WO2008002868A2 (en) * | 2006-06-26 | 2008-01-03 | Sabic Innovative Plastics Ip B.V. | Pyridinium salts for polymer composites and methods for their preparation |
WO2008002890A2 (en) * | 2006-06-26 | 2008-01-03 | Sabic Innovative Plastics Ip B.V. | Compositions and methods for polymer composites |
CN102660059A (zh) * | 2012-05-15 | 2012-09-12 | 福建师范大学 | 一种阻燃聚烯烃复合物的制备方法 |
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CN106633947A (zh) * | 2015-11-02 | 2017-05-10 | 中国石油化工股份有限公司 | 一种温拌聚合物改性沥青及其制备方法 |
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CN106189290A (zh) * | 2016-07-12 | 2016-12-07 | 同济大学 | 用于机场路面的改性沥青材料、其制备方法及应用 |
CN107383907A (zh) * | 2017-08-22 | 2017-11-24 | 江苏中路交通科学技术有限公司 | 一种温拌高模量沥青改性剂、制备方法及其应用 |
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Effective date of registration: 20231228 Address after: 100728 No. 22 North Main Street, Chaoyang District, Beijing, Chaoyangmen Patentee after: CHINA PETROLEUM & CHEMICAL Corp. Patentee after: Sinopec (Dalian) Petrochemical Research Institute Co.,Ltd. Address before: 100728 No. 22 North Main Street, Chaoyang District, Beijing, Chaoyangmen Patentee before: CHINA PETROLEUM & CHEMICAL Corp. Patentee before: DALIAN RESEARCH INSTITUTE OF PETROLEUM AND PETROCHEMICALS, SINOPEC Corp. |