CN115386422A - Far infrared radiation essential oil - Google Patents
Far infrared radiation essential oil Download PDFInfo
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- CN115386422A CN115386422A CN202210945412.7A CN202210945412A CN115386422A CN 115386422 A CN115386422 A CN 115386422A CN 202210945412 A CN202210945412 A CN 202210945412A CN 115386422 A CN115386422 A CN 115386422A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- Chemical & Material Sciences (AREA)
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention provides far infrared radiation essential oil which comprises functional components, wherein the mass percentage of the functional components in the far infrared radiation essential oil is not more than 45%; the far infrared radiation essential oil has characteristic absorption peak in the far infrared region of 4-14 microns after being radiated by a far infrared radiation source, and the normal total emissivity is not lower than 0.70. The far infrared radiation essential oil in the scheme can resonate with a far infrared radiation source under the irradiation of the far infrared radiation source covering the wavelength in the range, so that the far infrared radiation essential oil is easier to be absorbed by a human body, the effects of all components of the far infrared radiation essential oil are better exerted, and the far infrared radiation essential oil has more excellent medical care effect.
Description
Technical Field
The invention belongs to the technical field of essential oil production, and particularly relates to far infrared radiation essential oil and a preparation method thereof.
Background
Essential oil is widely used in the fields of beauty care, skin care and the like, generally, the essential oil is plant essential oil, the plant essential oil is extracted from flowers, leaves, stems, roots, fruits and the like in plants by a specific method, and the essential oil can permeate into human blood or other tissues from human skin in the using process and plays a specific curative effect after being combined with molecules in a human body. However, the essential oils sold in the market at present, such as those for relieving muscular soreness, muscular fatigue and muscular stiffness, are generally used, cannot be well absorbed by human skin, and have certain pain relieving effect after being used for many times.
Disclosure of Invention
The invention aims to provide far infrared radiation essential oil and a preparation method thereof, so that essential oil products have quick absorption effect and quick and long-acting analgesic effect.
According to one aspect of the invention, the far infrared radiation essential oil comprises a functional component, wherein the functional component accounts for no more than 45% of the far infrared radiation essential oil by mass; the far infrared radiation essential oil has characteristic absorption peak in the far infrared region of 4-14 microns after being radiated by a far infrared radiation source, and the normal total emissivity is not lower than 0.70.
Preferably, the normal total emissivity of the far infrared radiation essential oil is not less than 0.75.
Preferably, the normal total emissivity of the far infrared radiation essential oil is not less than 0.80.
The far infrared radiation essential oil has higher normal total emissivity, so the far infrared radiation essential oil has stronger heat effect, and the good heat effect can stimulate pores on the skin to open and promote the blood circulation of a human body when in use, thereby promoting the absorption of the skin on the essential oil, leading the essential oil to exert the maximum effect, and achieving the rapid and obvious health care effect.
The essential oil in the scheme can resonate with a far infrared radiation source, and can generate certain physical change or chemical change after being radiated by the far infrared radiation source, so that the essential oil can be promoted to be absorbed by a human body, the effects of all components in the essential oil can be better played, and the essential oil has more excellent medical care effect.
Preferably, the functional component comprises thermal oil, and the thermal oil accounts for not more than 15% of the far infrared radiation essential oil by mass percent; the thermal oil contains at least one of ginger oil, chili oil, black pepper oil and peppermint oil.
Preferably, the thermal oil comprises ginger oil, chili oil, black pepper oil and mint oil, and in the thermal oil, the mass ratio of the ginger oil: chili oil: black pepper oil: 5-15 parts of peppermint oil: 5 to 15:5 to 15:5 to 15.
Preferably, the thermal oil has certain irritation, and the skin can generate thermal effect when being coated on the skin, so that the thermal oil can stimulate pores on the skin to open and promote blood circulation of a human body, further promote the full absorption of each component of the essential oil, fully exert the functional effect of each component of the essential oil, and enable the analgesic effect of the essential oil to be quicker and more effective.
Preferably, the functional component also comprises formula oil, and the mass percentage of the formula oil in the far infrared radiation essential oil is not higher than 30%; the formula oil contains at least one of juniper berry extract, holly root extract, horse-arbor lotus extract, pubescent angelica root extract, cinnamon extract, asarum extract, red perilla extract, clove basil extract, benzoin extract, centella asiatica extract, garden balsam stem extract, gastrodia elata extract, angelica sinensis extract, ligusticum wallichii extract, suberect spatholobus stem extract, ginseng extract and bighead atractylodes rhizome extract.
Preferably, the formula oil contains at least three of juniper berry extract, wintergreen extract, arborvitae extract, pubescent angelica root extract, cinnamon extract, asarum extract, red perilla extract, clove basil extract, benzoin extract, centella asiatica extract, garden balsam stem extract, gastrodia elata extract, angelica sinensis extract, ligusticum wallichii extract, caulis spatholobi extract, ginseng extract and bighead atractylodes rhizome extract.
Preferably, 2 to 10 parts of juniper berry extract, 2 to 10 parts of holly extract, 2 to 10 parts of horse-lily extract, 2 to 10 parts of pubescent angelica root extract, 2 to 10 parts of cinnamon extract, 2 to 10 parts of asarum extract, 2 to 10 parts of red perilla extract, 2 to 10 parts of clove basil extract, 2 to 10 parts of benzoin extract, 2 to 10 parts of centella extract, 3 to 10 parts of garden balsam stem extract, 3 to 10 parts of gastrodia tuber extract, 3 to 10 parts of angelica extract, 3 to 10 parts of ligusticum wallichii extract, 3 to 10 parts of suberect spatholobus stem extract, 3 to 10 parts of ginseng extract and 3 to 10 parts of largehead atractylodes rhizome extract.
The addition of the formula oil enables the pain relieving effect of the essential oil to be more obvious, and in addition, the essential oil with different health care effects according to actual needs can be prepared by adopting different components and proportions in the formula oil.
Preferably, the far infrared radiation essential oil further comprises a base oil component, and the base oil component accounts for not less than 55% by mass of the far infrared radiation essential oil.
Preferably, the base oil component contains at least one of grape seed oil and coconut oil.
On one hand, the base oil can play a role in diluting the thermal effect oil and the formula oil, so that the problems of burns and the like caused by overhigh concentrations of the thermal effect oil and the formula oil to the skin of a human body are prevented; on the other hand, the addition of the base oil can greatly reduce the manufacturing cost of the essential oil, and has greater economic benefit.
The proportion of each component in the essential oil formula is reasonably adjusted, so that the effects of each component in the essential oil can be exerted to the best effect, and the components in the essential oil can mutually act synergistically, so that the essential oil has better far infrared radiation characteristic, is easier to be absorbed by the skin of a human body after being radiated by a far infrared radiation source, and has more obvious quick pain relieving and antibacterial effects.
According to another aspect of the present invention, there is provided a method for preparing far infrared radiation essential oil, comprising the operations of: all the raw materials for preparing the far infrared radiation essential oil are mixed, the material formed by the raw materials is taken as a precursor mixture, and the far infrared radiation source is utilized to provide 4-14 mu m of far infrared radiation for the precursor mixture at the temperature of 50-70 ℃.
When the far infrared radiation source is used for carrying out radiation processing on the essential oil, the far infrared radiation source in the scheme can realize a good radiation effect on the essential oil at 50-70 ℃, and compared with the far infrared radiation source which needs high-temperature heating, the far infrared radiation source in the scheme can obviously reduce processing energy consumption, and has lower energy cost and higher economic benefit.
Preferably, the heating temperature of the precursor mixture is 60 ℃.
Preferably, the irradiation time is 2 to 5 hours.
Preferably, the irradiation time is 3 hours.
Preferably, the reactants are continuously stirred during the far infrared ray irradiation.
Preferably, the far infrared radiation source comprises far infrared ceramic powder and epoxy resin, and the mass ratio of the far infrared ceramic powder to the epoxy resin is 40-50.
Preferably, the far infrared ceramic powder comprises, by mass, 10% -20% of praseodymium-neodymium oxide, 5% -15% of zirconium oxide, 10% -15% of iron oxide, 5% -15% of lanthanum oxide, 3% -5% of palladium oxide and the balance tourmaline.
Preferably, the far infrared radiation source is prepared as follows:
s1, fully mixing far infrared ceramic powder with epoxy resin to form a mixture;
s2, sintering and forming the mixture in the S1 at the temperature of 200-220 ℃ to obtain the far infrared radiation source.
Far infrared radiation source has been widely studied in recent years because of its high far infrared radiance, and far infrared that infrared radiation material emitted far away can produce the resonance effect with being in the material of the wavelength range of far infrared radiation material, makes the material that is radiated produce certain physics or chemical change, and then makes the material that is radiated have some special properties. The far infrared radiation source prepared by adopting the specific materials and the material proportion thereof has excellent radiation performance, and the effect of the essential oil can be more remarkable when the far infrared radiation source is applied to essential oil processing. The far infrared radiation source prepared by adopting specific materials in a specific proportion has the normal total emissivity of over 0.85 at the radiation wavelength of 4-14 mu m, and has excellent far infrared radiation effect. The radiation wavelength of the far infrared radiation source covers the wavelength of the essential oil in the scheme, so that when the essential oil is radiated by the far infrared radiation source, on one hand, material molecules in the essential oil can resonate with the far infrared radiation source, so that molecular chains of the material molecules in the essential oil are broken under the warming effect of a certain time, and finally, the formed essential oil mixture has smaller molecular weight and activity, and is easier to absorb by a human body; on the other hand, after being absorbed by a human body, the essential oil radiated by far infrared rays can resonate with water molecules in the human body and activate the water molecules, so that the binding force of the essential oil and macromolecules in the human body can be enhanced, proteins and other biological macromolecules in the human body are activated, cells of the human body are in a high vibration energy level, capillary vessels of the human body are expanded, blood circulation and metabolism in the human body are promoted, the effects of all components of the essential oil are further exerted, and the purpose of relieving pain more obviously, quickly and effectively is achieved.
Drawings
FIG. 1 is a report of the detection of the total normal emissivity of far infrared radiation essential oil in example 1 of the present invention.
Detailed Description
In order to make the technical solutions of the present invention better understood by those skilled in the art, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments.
Example 1
The essential oil formula adopted in the embodiment is as follows according to the mass parts: 6 parts of ginger oil, 6 parts of chili oil, 6 parts of black pepper oil, 5 parts of peppermint oil, 3 parts of juniper berry extract, 5 parts of wintergreen extract, 2 parts of horse lotus extract, 2 parts of radix angelicae pubescentis extract, 3 parts of cinnamon extract, 2 parts of asarum extract, 3 parts of red perilla extract, 2 parts of clove basil extract, 2 parts of benzoin extract, 2 parts of centella extract, 3 parts of speranskia herb extract, 3 parts of gastrodia tuber extract, 3 parts of angelica extract, 3 parts of ligusticum wallichii extract, 3 parts of caulis spatholobi extract, 2 parts of ginseng extract, 2 parts of bighead atractylodes rhizome extract, 40 parts of grape seed oil and 50 parts of coconut oil.
The method for preparing the far infrared radiation essential oil in the embodiment is as follows: mixing all the raw materials for preparing the far infrared radiation essential oil in a reaction kettle, irradiating the mixture for 3 hours at 60 ℃ by using a far infrared radiation source, stirring the mixture in the irradiation process, cooling and discharging the mixture out of the kettle to obtain the far infrared radiation essential oil.
The method of making the far infrared radiation source of this example is as follows: according to the mass ratio, fully mixing the far infrared ceramic powder and the epoxy resin according to the mixture ratio of 45. The formula of the far infrared ceramic powder in the embodiment is as follows according to the mass ratio: 10% of praseodymium-neodymium oxide, 5% of zirconium oxide, 15% of iron oxide, 15% of lanthanum oxide, 5% of palladium oxide and 50% of tourmaline.
Example 2
The thermal efficiency oil adopted in the essential oil formula adopted in the embodiment is single-component thermal efficiency oil, and the essential oil formula adopted in the embodiment is as follows according to the mass parts: 20 parts of ginger oil, 3 parts of juniper berry extract, 5 parts of holly root extract, 2 parts of horse-lily extract, 2 parts of radix angelicae pubescentis extract, 3 parts of cinnamon extract, 2 parts of asarum extract, 3 parts of red perilla extract, 2 parts of clove basil extract, 2 parts of benzoin extract, 2 parts of centella asiatica extract, 3 parts of garden balsam stem extract, 3 parts of gastrodia elata extract, 3 parts of angelica extract, 3 parts of ligusticum wallichii extract, 3 parts of caulis spatholobi extract, 2 parts of ginseng extract, 2 parts of bighead atractylodes rhizome extract, 40 parts of grape seed oil and 50 parts of coconut oil.
The method for preparing the far infrared radiation essential oil in the embodiment is the same as that of the embodiment 1, and the method for preparing the far infrared radiation source, the ratio of the far infrared ceramic powder to the epoxy resin and the formula of the far infrared ceramic powder are also the same as those of the embodiment 1.
Example 3
The thermal efficiency oil adopted in the essential oil formula adopted in the embodiment contains two different types of thermal efficiency oil, and the essential oil formula adopted in the embodiment is calculated according to the mass parts: 12 parts of black pepper oil, 13 parts of peppermint oil, 3 parts of juniper berry extract, 5 parts of holly extract, 2 parts of horse-lily extract, 2 parts of radix angelicae pubescentis extract, 3 parts of cinnamon extract, 2 parts of asarum extract, 3 parts of red perilla extract, 2 parts of clove basil extract, 2 parts of benzoin extract, 2 parts of centella extract, 3 parts of garden balsam stem extract, 3 parts of gastrodia elata extract, 3 parts of angelica extract, 3 parts of ligusticum wallichii extract, 3 parts of caulis spatholobi extract, 2 parts of ginseng extract, 2 parts of bighead atractylodes rhizome extract, 50 parts of grape seed oil and 50 parts of coconut oil.
The method for preparing the far infrared radiation essential oil in the embodiment is the same as that of the embodiment 1, and the method for preparing the far infrared radiation source, the ratio of the far infrared ceramic powder to the epoxy resin and the formula of the far infrared ceramic powder are also the same as those of the embodiment 1.
Example 4
The essential oil formula adopted in the embodiment contains three different types of formula oil, and the essential oil formula adopted in the embodiment is as follows according to the mass parts: 6 parts of ginger oil, 6 parts of chili oil, 6 parts of black pepper oil, 5 parts of peppermint oil, 20 parts of juniper berry extract, 10 parts of wintergreen extract, 10 parts of horse-tree-lotus extract, 45 parts of grape seed oil and 50 parts of coconut oil.
The method for preparing the far infrared radiation essential oil in the embodiment is the same as that of the embodiment 1, and the method for preparing the far infrared radiation source, the ratio of the far infrared ceramic powder to the epoxy resin and the formula of the far infrared ceramic powder are also the same as those of the embodiment 1.
Example 5
The essential oil formula adopted in the embodiment contains three different types of formula oils, and the essential oil formula adopted in the embodiment is calculated according to the mass parts: 8 parts of ginger oil, 6 parts of chili oil, 6 parts of black pepper oil, 5 parts of peppermint oil, 15 parts of radix angelicae pubescentis extract, 13 parts of asarum extract, 20 parts of clove basil extract, 50 parts of grape seed oil and 50 parts of coconut oil.
The method for preparing the far infrared radiation essential oil in the embodiment is the same as that in the embodiment 1, and the method for preparing the far infrared radiation source, the ratio of the far infrared ceramic powder to the epoxy resin and the formula of the far infrared ceramic powder are also the same as those in the embodiment 1.
Example 6
The essential oil formulation adopted in this example is the same as that in example 1, and the method for preparing the far infrared radiation essential oil and the ratio of the far infrared ceramic powder to the epoxy resin in this example are also the same as those in example 1. The difference between this example and example 1 is that the formulation of the far infrared ceramic powder used is not consistent. The formula of the far infrared ceramic powder in this embodiment is as follows according to the mass ratio: 20% of praseodymium-neodymium oxide, 15% of zirconium oxide, 10% of iron oxide, 5% of lanthanum oxide, 3% of palladium oxide and 47% of tourmaline.
Example 7
The essential oil formulation adopted in this example is the same as that in example 1, and the method for preparing the far infrared radiation essential oil and the ratio of the far infrared ceramic powder to the epoxy resin in this example are also the same as those in example 1. The difference between this example and example 1 is that the formulation of the far infrared ceramic powder used is not consistent. The formula of the far infrared ceramic powder in this embodiment is as follows according to the mass ratio: 10% of praseodymium-neodymium oxide, 5% of zirconium oxide, 10% of iron oxide, 5% of lanthanum oxide, 3% of palladium oxide and 67% of tourmaline.
Example 8
The essential oil formulation adopted in this example is the same as that in example 1, and the method for preparing the far infrared radiation essential oil and the ratio of the far infrared ceramic powder to the epoxy resin in this example are also the same as those in example 1. The difference between this example and example 1 is that the formulation of the far infrared ceramic powder used is not consistent. The formula of the far infrared ceramic powder in this embodiment is as follows according to the mass ratio: 20% of praseodymium-neodymium oxide, 15% of zirconium oxide, 15% of iron oxide, 15% of lanthanum oxide, 5% of palladium oxide and 30% of tourmaline.
Example 9
The essential oil formulation adopted in this example is the same as that in example 1, and the method for preparing the far infrared radiation essential oil and the ratio of the far infrared ceramic powder to the epoxy resin in this example are also the same as those in example 1. The difference between this example and example 1 is that the formulation of the far infrared ceramic powder used is not consistent. The formula of the far infrared ceramic powder in this embodiment is as follows according to the mass ratio: 15% of praseodymium-neodymium oxide, 10% of zirconium oxide, 12% of iron oxide, 10% of lanthanum oxide, 4% of palladium oxide and 59% of tourmaline.
Comparative example 1
The essential oil formula adopted in the comparative example does not contain formula oil, and the essential oil formula adopted in the comparative example is calculated according to the mass parts: 6 parts of ginger oil, 6 parts of chili oil, 6 parts of black pepper oil, 5 parts of peppermint oil, 60 parts of grape seed oil and 75 parts of coconut oil.
The method for preparing the far infrared radiation essential oil in this comparative example was the same as in example 1, and the method for preparing the far infrared radiation source, the ratio of the far infrared ceramic powder to the epoxy resin, and the formulation of the far infrared ceramic powder were also the same as in example 1.
Comparative example 2
The essential oil formula adopted in the comparative example does not contain thermal effect oil, and the essential oil formula adopted in the comparative example is calculated according to the mass parts: 3 parts of juniper berry extract, 5 parts of wintergreen extract, 2 parts of horse-buckwheat extract, 2 parts of radix angelicae pubescentis extract, 3 parts of cinnamon extract, 2 parts of asarum extract, 3 parts of red perilla extract, 2 parts of clove basil extract, 2 parts of benzoin extract, 2 parts of centella extract, 3 parts of garden balsam stem extract, 3 parts of gastrodia elata extract, 3 parts of angelica extract, 3 parts of ligusticum wallichii extract, 3 parts of caulis spatholobi extract, 2 parts of ginseng extract, 2 parts of bighead atractylodes rhizome extract, 50 parts of grape seed oil and 63 parts of coconut oil.
The method for preparing the far infrared radiation essential oil in the comparative example is the same as that of example 1, and the method for preparing the far infrared radiation source, the ratio of the far infrared ceramic powder to the epoxy resin, and the formula of the far infrared ceramic powder are also the same as those of example 1.
Comparative example 3
The content of the thermal effect oil in the essential oil formula adopted in the comparative example is about 5% by mass of the essential oil, and the essential oil formula adopted in the comparative example is as follows according to parts by mass: 3 parts of ginger oil, 4 parts of chili oil, 3 parts of juniper berry extract, 5 parts of wintergreen extract, 2 parts of horse-lily extract, 2 parts of radix angelicae pubescentis extract, 3 parts of cinnamon extract, 2 parts of asarum extract, 3 parts of red perilla extract, 2 parts of clove basil extract, 2 parts of benzoin extract, 2 parts of centella asiatica extract, 3 parts of garden balsam stem extract, 3 parts of gastrodia elata extract, 3 parts of angelica extract, 3 parts of ligusticum wallichii extract, 3 parts of caulis spatholobi extract, 2 parts of ginseng extract, 2 parts of bighead atractylodes rhizome extract, 40 parts of grape seed oil and 50 parts of coconut oil.
The method for preparing the far infrared radiation essential oil in the comparative example is the same as that of example 1, and the method for preparing the far infrared radiation source, the ratio of the far infrared ceramic powder to the epoxy resin, and the formula of the far infrared ceramic powder are also the same as those of example 1.
Comparative example 4
The essential oil formula in the comparative example only contains base oil, and the essential oil formula adopted in the comparative example is as follows according to parts by mass: 40 parts of grape seed oil and 50 parts of coconut oil.
The method for preparing the far infrared radiation essential oil in the comparative example is the same as that of example 1, and the method for preparing the far infrared radiation source, the ratio of the far infrared ceramic powder to the epoxy resin, and the formula of the far infrared ceramic powder are also the same as those of example 1.
Comparative example 5
The essential oil formulation used in this comparative example was identical to that of example 1.
The procedure for preparing the essential oil of this comparative example was as follows: mixing all raw materials for preparing the essential oil in a reaction kettle, stirring the mixture for 3 hours at the temperature of 60 ℃, cooling and taking out of the kettle to obtain the essential oil. In the comparative example, far infrared radiation source is not adopted to irradiate the essential oil in the process of preparing the essential oil.
Comparative example 6
The essential oil formulation used in this comparative example was identical to that of example 1. And the method of preparing the far infrared radiation essential oil and the formulation of the far infrared ceramic powder in this comparative example were also the same as in example 1. The difference between the comparative example and the example 1 is that the ratio of the far infrared ceramic powder to the epoxy resin is not consistent. According to the mass ratio, in the comparative example, the ratio of the far infrared ceramic powder to the epoxy resin is 30.
Comparative example 7
The formula of the essential oil adopted in the comparative example is the same as that of the example 1, and the method for preparing the far infrared radiation essential oil and the ratio of the far infrared ceramic powder to the epoxy resin in the comparative example are also the same as those of the example 1. The comparative example is different from example 1 in that the formulation of the far infrared ceramic powder used is not identical. The formula of the far infrared ceramic powder in the comparative example is as follows according to the mass ratio: 5% of praseodymium-neodymium oxide, 7% of zirconium oxide, 10% of iron oxide, 5% of lanthanum oxide, 3% of palladium oxide and 70% of tourmaline. Wherein, the mass percentage of the praseodymium-neodymium oxide in the far infrared ceramic powder in the comparative example is only 5%.
Comparative example 8
The formula of the essential oil adopted in the comparative example is the same as that of the example 1, and the method for preparing the far infrared radiation essential oil and the ratio of the far infrared ceramic powder to the epoxy resin in the comparative example are also the same as those of the example 1. The comparative example is different from example 1 in that the formulation of the far infrared ceramic powder used is not identical. The formula of the far infrared ceramic powder in the comparative example is as follows according to the mass ratio: 15% of praseodymium-neodymium oxide, 7% of zirconium oxide, 10% of iron oxide, 2% of lanthanum oxide, 5% of palladium oxide and 61% of tourmaline. Wherein, the mass percentage of the lanthanum oxide in the far infrared ceramic powder in the comparative example is only 2%.
Comparative example 9
The formula of the essential oil adopted in the comparative example is the same as that of the example 1, and the method for preparing the far infrared radiation essential oil and the ratio of the far infrared ceramic powder to the epoxy resin in the comparative example are also the same as those of the example 1. The comparative example is different from example 1 in that the formulation of the far infrared ceramic powder used is not identical. The formula of the far infrared ceramic powder in the comparative example is as follows according to the mass ratio: 15% of praseodymium-neodymium oxide, 15% of zirconium oxide, 10% of iron oxide, 10% of lanthanum oxide and 60% of tourmaline. Among them, the far infrared ceramic powder in this comparative example does not contain palladium oxide.
Test example
1. Experimental construction mode
(1) Far infrared radiation characteristic characterization was performed on the essential oils prepared in examples 1 to 9 and comparative examples 1 to 9.
(2) The essential oils prepared in examples 1 to 9 and comparative examples 1 to 9 were characterized for skin irritation.
(3) The antibacterial properties of the essential oils prepared in examples 1 to 9 and comparative examples 1 to 9 were characterized. This experiment measured the total number of bacterial colonies for examples 1-9 and comparative examples 1-9 using the cosmetic hygiene code 2007.
(4) The essential oils prepared in examples 1 to 9 and comparative examples 1 to 9 were subjected to skin feel property characterization, which is mainly skin absorption effect and skin burning sensation appearance characterization.
2. Results of the experiment
(1) Characterization of far infrared radiation characteristics
Far infrared radiation characteristic characterization was performed on the essential oils of examples 1 to 9 and comparative examples 1 to 9.
Table 1 far infrared radiation characteristic test results of essential oils in examples 1 to 9 and comparative examples 1 to 9
As can be seen from table 1, the total normal emissivity of the essential oil in example 1 is the highest, which reaches 0.80, and the results reported in fig. 1 can be referred to, while in other examples or comparative examples, the total normal emissivity of the essential oil is slightly reduced or significantly reduced, especially for the essential oils which do not contain thermal oils and do not undergo radiation from the far infrared radiation source, the total far infrared emissivity is significantly reduced, and when the formula of the far infrared ceramic powder in the far infrared radiation source is changed, such as some components are reduced or removed, the total normal emissivity of the formed far infrared radiation source is reduced, and further the total normal emissivity of the essential oil is also reduced. The data show that the essential oil in the scheme has excellent far infrared radiation characteristic under the radiation of a far infrared radiation source, and can enhance the thermal effect of each component in the essential oil, especially the thermal effect of the thermal effect component in the essential oil, so that the absorption of the essential oil by skin is promoted, the synergistic effect among the components of the essential oil is fully exerted, and the effect of quickly and effectively relieving pain is realized.
(2) Characterization of skin irritation
(1) Taking two groups of experimental-grade white mice, one group is 14 mice, the back of one group is cut off hairs, the essential oil in the examples 1-9 and the comparative examples 1-9 is respectively coated on the parts of the backs of the white mice, which are cut off hairs, the other group is not cut off hairs, and the essential oil in the examples 1-9 and the comparative examples 1-9 is respectively coated on the parts of the backs of the white mice, which are not cut off hairs; after 2h, no irritation or allergic reaction such as redness, rash, blister occurred in both groups of mice.
(2) The essential oils of examples 1-9 and comparative examples 1-9 were applied to 18-60 year old volunteers, and after 2h, no irritation or allergic reaction such as redness, rash, blister occurred in all staff.
(3) Characterization of antibacterial Properties
The results of the antibacterial property test on the essential oils of examples 1 to 9 and comparative examples 1 to 9 are shown in table 2.
Table 2 antibacterial property test results of essential oils in examples 1 to 9 and comparative examples 1 to 9
As can be seen from Table 2, the essential oil in the scheme has certain far infrared radiation characteristic after being radiated by a far infrared radiation source, and the far infrared radiation characteristic enhances the antibacterial performance of the essential oil. In the above examples and comparative examples, the antibacterial property of the essential oil containing no thermal effect oil was significantly reduced, and the antibacterial property of the essential oil was greatly reduced without irradiating the essential oil with a far infrared radiation source in comparative example 5.
(4) Skin feel Performance characterization
(1) Characterization of skin absorption Effect
The essential oils in examples 1 to 9 and comparative examples 1 to 5 are respectively smeared on certain parts of human arm skin, after 5 minutes, the oil absorption paper is used for wiping the parts of the arm skin smeared with the essential oils, in the essential oil absorption paper wiping the essential oils in examples 1 to 9 and comparative examples 1 to 9, the oil absorption paper wiping the essential oils in examples 1 to 9 and comparative examples 1 to 9 has no obvious oil stains, while the oil absorption paper wiping the essential oils in comparative examples 2 and 5 has a little oil stains, probably because no hot oil component exists in the essential oil components in comparative examples 2 and 5, the hot effect of the essential oils is obviously reduced, and the absorption effect of the essential oils by the skin is poor.
(2) Characterization of skin burning sensation
The essential oils of examples 1 to 9 and comparative examples 1 to 9 were applied to a certain area of the skin of an arm of a human body, respectively, and thermal effect measurement was performed on the skin of the arm to which the essential oil was applied by a thermal infrared imager, and the ratio of thermal effect area/area of applied essential oil was measured for the total thermal effect area of the skin of the arm and the peripheral area where the temperature difference between the diffusion of the thermal effect area and the diffusion temperature is not far, with the result shown in table 3 below.
Table 3 results of thermal effects of essential oils of examples 1 to 9 and comparative examples 1 to 9
As can be seen from Table 3, the values of the ratio of the thermal effect area/the area of applied essential oil of the essential oils in examples 1-9 are all relatively similar, and from the results, the thermal effect of the essential oil in example 1 is the best, which means that the formula of the essential oil in example 1 has the best thermal effect after being radiated by the far infrared radiation source. In comparative examples 2 to 4, the thermal effect of the essential oil was significantly reduced without containing the thermal effect oil or without the thermal effect oil component within a reasonable range. In addition, the essential oil in the comparative example 5 is not radiated by a far infrared radiation source, and the thermal effect is obviously weakened. In comparative examples 6 to 9, in the formulations of the far infrared ceramic powders in the far infrared radiation source, some components were contained in a small amount or were not contained, resulting in a corresponding decrease in the radiation effect of the far infrared radiation source on the essential oil, and thus the thermal effect of the essential oil was also slightly decreased.
Although the present invention has been described in detail with reference to the above embodiments, it should be understood by those skilled in the art that various changes, modifications and equivalents may be made therein without departing from the spirit and scope of the invention.
Claims (10)
1. A far infrared radiation essential oil is characterized in that:
the far infrared radiation essential oil comprises functional components, and the mass percentage of the functional components in the far infrared radiation essential oil is not more than 45%;
the far infrared radiation essential oil has a characteristic absorption peak in a far infrared region of 4-14 mu m after being radiated by a far infrared radiation source, and the normal total emissivity is not lower than 0.70.
2. The far infrared radiation essential oil as set forth in claim 1, wherein: the functional component comprises thermal efficiency oil, and the mass percentage of the thermal efficiency oil in the far infrared radiation essential oil is not higher than 15%;
the thermal effect oil contains at least one of ginger oil, chili oil, black pepper oil and peppermint oil.
3. The far infrared radiation essential oil as set forth in claim 2, wherein: the heat effect oil comprises ginger oil, chili oil, black pepper oil and mint oil, and in the heat effect oil, the ginger oil: chili oil: black pepper oil: 5-15 parts of peppermint oil: 5 to 15:5 to 15:5 to 15.
4. The far infrared radiation essential oil as set forth in claim 2, wherein: the functional component also comprises formula oil, and the mass percentage of the formula oil in the far infrared radiation essential oil is not higher than 30%;
the formula oil contains at least one of juniper berry extract, holly root extract, horse-lily extract, pubescent angelica root extract, cinnamon extract, asarum extract, red perilla extract, clove basil extract, benzoin extract, centella asiatica extract, garden balsam stem extract, gastrodia elata extract, angelica sinensis extract, ligusticum wallichii extract, caulis spatholobi extract, ginseng extract and bighead atractylodes rhizome extract.
5. The far infrared radiation essential oil of claim 4, wherein: the formula oil contains at least three of juniper berry extract, holly root extract, horse-lily extract, pubescent angelica root extract, cinnamon extract, asarum extract, red perilla extract, clove basil extract, benzoin extract, centella asiatica extract, garden balsam stem extract, gastrodia elata extract, angelica sinensis extract, ligusticum wallichii extract, caulis spatholobi extract, ginseng extract and bighead atractylodes rhizome extract.
6. The far infrared radiation essential oil of claim 5, wherein the formula oil comprises, in parts by mass: 2-10 parts of juniper berry extract, 2-10 parts of holly extract, 2-10 parts of horse-lily extract, 2-10 parts of pubescent angelica root extract, 2-10 parts of cinnamon extract, 2-10 parts of asarum extract, 2-10 parts of red perilla extract, 2-10 parts of clove basil extract, 2-10 parts of benzoin extract, 2-10 parts of centella extract, 3-10 parts of garden balsam stem extract, 3-10 parts of gastrodia tuber extract, 3-10 parts of angelica extract, 3-10 parts of ligusticum wallichii extract, 3-10 parts of suberect spatholobus stem extract, 3-10 parts of ginseng extract and 3-10 parts of bighead atractylodes rhizome extract.
7. The far-infrared radiation essential oil according to claim 1, further comprising a base oil component, wherein the base oil component accounts for not less than 55% by mass of the far-infrared radiation essential oil.
8. A method for preparing far infrared radiation essential oil according to any one of claims 1 to 8, comprising the following operations: all the raw materials for preparing the far infrared radiation essential oil are mixed, the material formed by the raw materials is used as a precursor mixture, and the far infrared radiation source is used for providing 4-14 mu m of far infrared radiation to the precursor mixture at the temperature of 50-70 ℃.
9. The method for preparing far-infrared radiation essential oil according to claim 1, characterized in that: the far infrared radiation source comprises far infrared ceramic powder and epoxy resin, and the mass ratio of the far infrared ceramic powder to the epoxy resin is 40-50.
10. The method for preparing far-infrared radiation essential oil of claim 11, wherein: calculated according to the mass percentage, the far infrared ceramic powder comprises 10-20 percent of praseodymium-neodymium oxide, 5-15 percent of zirconia, 10-15 percent of ferric oxide, 5-15 percent of lanthanum oxide, 3-5 percent of palladium oxide and the balance of tourmaline.
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