CN115089499A - Mud film with space cage type structure and preparation method - Google Patents
Mud film with space cage type structure and preparation method Download PDFInfo
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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Abstract
The invention discloses a mud membrane with a space cage type structure and a preparation method thereof, wherein the mud membrane comprises a phase A composition, a phase B composition and a phase C composition; the A phase composition comprises: hydrosolvent, kaolin, glycerol, butanediol, sodium hyaluronate, menthol lactate, xanthan gum and p-hydroxyacetophenone; the B phase composition comprises: caprylic or capric triglyceride, squalane, cyclopentadimethylsiloxane, polysorbate-60, sorbitan laurate, polydimethylsiloxane, sodium polyacryloyldimethyltaurate, isohexadecane, and PEG-7 glyceryl cocoate; the C phase composition comprises: tripeptide-1 copper, ceramide NP, hydroxypropyl tetrahydropyrane triol, methyl propylene glycol, and 1, 2-hexanediol. The mud membrane with the space cage type structure provided by the invention is easy to form a cage structure with space holding capacity, is good in air permeability, improves the thick and closed property of a common mud membrane, and reduces the skin load.
Description
Technical Field
The invention relates to the technical field of mud membranes, in particular to a mud membrane with a space cage type structure and a preparation method thereof.
Background
With the development of skin care industry, mud films can be used as common skin care products, people face various pollutions such as over-fatigue, irregular living habits and dust in the external environment, and people gradually begin to consider the practicability and the use feeling of the mud films.
The general application method of the mud mask is to coat a thick layer on the face to isolate the skin from the outside, keep standing for 15-20 minutes, and clean the face after nutrients contained in the mud mask are slowly absorbed by the skin. When the mud film is smeared on the face, the weight of the skin on the face can be increased and decreased, the mud film covers the face to seal the air permeability of the skin, and meanwhile, the traditional mud film is easy to cause skin barrier damage and poor in using effect.
Disclosure of Invention
In order to overcome the defects in the prior art, the invention aims to provide the mud membrane with the space cage structure, which is easy to form a cage structure with space holding capacity, has good air permeability, improves the thick and solid sealing property of a common mud membrane, reduces the skin burden feeling, and can better adsorb facial grease and repair skin barriers in a multidimensional way by using mineral mud attached to the face.
The technical scheme adopted by the invention for solving the technical problems is as follows:
a mud film with a space cage type structure, which comprises a phase A composition, a phase B composition and a phase C composition;
the A phase composition comprises: hydrosolvent, kaolin, glycerin, butanediol, sodium hyaluronate, menthol lactate, xanthan gum and p-hydroxyacetophenone;
the B phase composition comprises: caprylic or capric triglyceride, squalane, cyclopentadimethylsiloxane, polysorbate-60, sorbitan laurate, polydimethylsiloxane, sodium polyacryloyldimethyltaurate, isohexadecane, and PEG-7 glyceryl cocoate;
the C phase composition comprises: tripeptides 1 copper, ceramide NP, hydroxypropyl tetrahydropyranyl triol, methyl propylene glycol, and 1, 2-hexanediol.
As a further improvement of the invention: the composition comprises the following components in percentage by weight:
50-80% of water solvent, 3.0-6.0% of kaolin, 2.0-4.0% of glycerol, 2.0-4.0% of butanediol, 0.01-0.1% of sodium hyaluronate, 0.1-0.5% of menthol lactate, 0.1-0.5% of xanthan gum and 0.1-1% of p-hydroxyacetophenone;
caprylic or capric triglyceride 2.0-10.0%, squalane 2.0-7.0%, cyclopentadimethylsiloxane 2.0-4.0%, polysorbate-602.0-3.0%, sorbitan laurate 2.0-3.0%, polydimethylsiloxane 0.2-1.0%, sodium polyacryloyldimethyltaurate 0.1-1.0%, isohexadecane 0.01-0.3%, and PEG-7 glyceryl cocoate 0.01-0.1%;
tripeptide-1 copper 0.05-0.2%, ceramide NP 0.005-0.02%, hydroxypropyl tetrahydropyrane triol 0.02-0.2%, methyl propylene glycol 0.01-0.15% and 1, 2-hexanediol 0.2-1.5%.
As a further improvement of the invention: the composition comprises the following components in percentage by weight:
60-75% of hydrosolvent, 4.0-6.0% of kaolin, 2.2-3.5% of glycerol, 2.2-3.5% of butanediol, 0.01-0.05% of sodium hyaluronate, 0.15-0.3% of menthol lactate, 0.11-0.2% of xanthan gum and 0.4-0.6% of p-hydroxyacetophenone;
caprylic or capric triglyceride 4.5-7%, squalane 4.0-6.5%, cyclopentadimethylsiloxane 2.3-3.0%, polysorbate-602.0-2.7%, sorbitan laurate 2.0-2.7%, polydimethylsiloxane 0.4-0.8%, sodium polyacryloyldimethyltaurate 0.1-0.5%, isohexadecane 0.05-0.2% and PEG-7 glyceryl cocoate 0.01-0.07%;
tripeptide-1 copper 0.05-0.15%, ceramide NP 0.007-0.02%, hydroxypropyl tetrahydropyrane triol 0.03-0.15%, methyl propylene glycol 0.02-0.1% and 1, 2-hexanediol 0.4-1.0%.
A preparation method of a mud membrane with a space cage type structure comprises the following steps:
s1: cleaning and sterilizing the production equipment and the using tools, and then checking whether all valves of the emulsifying pot are closed.
S2: adding the phase A into an emulsifying pot, starting homogenizing for 5-10 minutes, stirring and heating to 80-90 ℃, and preserving heat for 5-15 minutes until complete dissolution is ensured; adding the phase B material into an oil phase pan, stirring and heating to 75-85 deg.C until the solution is complete.
S3: and (3) keeping the emulsifying pot in a vacuum state, adding the dissolved substance of the composition of the phase B in the step S2 into the emulsifying pot, emulsifying and homogenizing for 3-6 minutes, preserving heat and defoaming for 15-25 minutes to ensure that no bubbles emerge, and starting to cool.
S4: cooling to 40-50 deg.C, adding the C phase material into emulsifying pot, and stirring for cooling.
S5: cooling to 35-40 deg.C, stopping stirring, detecting the quality of mud film, and discharging when it is qualified.
As a further improvement of the invention: the step S2 includes: adding the phase A into an emulsifying pot, starting homogenizing for 5-8 minutes, stirring and heating to 85 ℃, and keeping the temperature for 10 minutes until complete dissolution is ensured; adding the B phase material into an oil phase pot, stirring and heating to 80 ℃ until the B phase material is completely dissolved.
As a further improvement of the invention: the step S3 includes: and (4) keeping the vacuum state of an emulsifying pot, adding the dissolved substance of the composition of the phase B in the step S2 into the emulsifying pot, emulsifying and homogenizing for 4-5 minutes, preserving heat and defoaming for 20 minutes to ensure that no bubbles emerge, and starting to cool.
As a further improvement of the invention: the vacuum state is-0.08 mpa-0.02 mpa.
As a further improvement of the invention: the vacuum state is-0.05 mpa.
Compared with the prior art, the invention has the beneficial effects that:
the mud film provided by the invention has a space cage-shaped structure, has a unique spherical structure, is easy to form a cage-shaped structure with space holding capacity when being mutually and fully crosslinked, has good air permeability, improves the thick and closed property of a common mud film, reduces the skin load, can better adsorb facial grease when being pasted on mineral mud of the face, can resist oxidation, brighten the skin color, compact the skin, lighten fine lines and repair skin barriers in a multidimensional way.
Drawings
Fig. 1 is a first structural schematic diagram of the present invention.
Fig. 2 is a second structural schematic diagram of the present invention.
Detailed Description
The invention will now be further described with reference to the accompanying description and examples:
detailed description of the invention:
a mud film with a space cage type structure, which comprises a phase A composition, a phase B composition and a phase C composition;
the A phase composition comprises: hydrosolvent, kaolin, glycerin, butanediol, sodium hyaluronate, menthol lactate, xanthan gum and p-hydroxyacetophenone;
the B phase composition comprises: caprylic or capric triglyceride, squalane, cyclopentadimethylsiloxane, polysorbate-60, sorbitan laurate, polydimethylsiloxane, sodium polyacryloyldimethyltaurate, isohexadecane, and PEG-7 glyceryl cocoate;
the C phase composition comprises: tripeptide-1 copper, ceramide NP, hydroxypropyl tetrahydropyrane triol, methyl propylene glycol, and 1, 2-hexanediol.
Further, the percentage content of each component in the phase A composition, the phase B composition and the phase C composition is as follows:
50-80% of water solvent, 3.0-6.0% of kaolin, 2.0-4.0% of glycerol, 2.0-4.0% of butanediol, 0.01-0.1% of sodium hyaluronate, 0.1-0.5% of menthol lactate, 0.1-0.5% of xanthan gum and 0.1-1% of p-hydroxyacetophenone;
caprylic or capric triglyceride 2.0-10.0%, squalane 2.0-7.0%, cyclopentadimethylsiloxane 2.0-4.0%, polysorbate-602.0-3.0%, sorbitan laurate 2.0-3.0%, polydimethylsiloxane 0.2-1.0%, sodium polyacryloyldimethyltaurate 0.1-1.0%, isohexadecane 0.01-0.3% and PEG-7 glyceryl cocoate 0.01-0.1%;
the C phase composition comprises: tripeptide-1 copper 0.05-0.2%, ceramide NP 0.005-0.02%, hydroxypropyl tetrahydropyrane triol 0.02-0.2%, methyl propylene glycol 0.01-0.15% and 1, 2-hexanediol 0.2-1.5%.
Further, the percentage content of each component in the phase A composition, the phase B composition and the phase C composition is as follows:
60-75% of water solvent, 4.0-6.0% of kaolin, 2.2-3.5% of glycerol, 2.2-3.5% of butanediol, 0.01-0.05% of sodium hyaluronate, 0.15-0.3% of menthol lactate, 0.11-0.2% of xanthan gum and 0.4-0.6% of p-hydroxyacetophenone;
caprylic or capric triglyceride 4.5-7%, squalane 4.0-6.5%, cyclopentadimethylsiloxane 2.3-3.0%, polysorbate-602.0-2.7%, sorbitan laurate 2.0-2.7%, polydimethylsiloxane 0.4-0.8%, sodium polyacrylyldimethyltaurate 0.1-0.5%, isohexadecane 0.05-0.2%, and PEG-7 glyceryl cocoate 0.01-0.07%;
the C phase composition comprises: tripeptide-1 copper 0.05-0.15%, ceramide NP 0.007-0.02%, hydroxypropyl tetrahydropyrane triol 0.03-0.15%, methyl propylene glycol 0.02-0.1% and 1, 2-hexanediol 0.4-1.0%.
A preparation method of a mud membrane with a space cage type structure comprises the following steps:
s1: cleaning and sterilizing the production equipment and the using tools, and then checking whether all valves of the emulsifying pot are closed.
S2: adding the phase A into an emulsifying pot, starting homogenizing for 5-10 minutes, stirring and heating to 80-90 ℃, and preserving heat for 5-15 minutes until complete dissolution is ensured; adding the B phase material into the oil phase pan, stirring and heating to 75-85 deg.C until completely dissolved.
S3: and (3) keeping the emulsifying pot in a vacuum state (-0.08 mpa-0.02 mpa), adding the dissolved substance of the composition of the phase B in the step S2 into the emulsifying pot, emulsifying and homogenizing for 3-6 minutes, preserving heat and defoaming for 15-25 minutes to ensure that no bubbles are emitted, and starting cooling.
S4: cooling to 40-50 deg.C, adding the C phase material into emulsifying pot, and stirring for cooling.
S5: cooling to 35-40 deg.C, stopping stirring, detecting the quality of mud film, and discharging when it is qualified.
Further, the step S2 includes: adding the phase A into an emulsifying pot, starting homogenizing for 5-8 minutes, stirring and heating to 85 ℃, and keeping the temperature for 10 minutes until complete dissolution is ensured; adding the B phase material into an oil phase pot, stirring and heating to 80 ℃ until the B phase material is completely dissolved.
Further, the step S3 includes: and (3) keeping the emulsifying pot in a vacuum state (-0.05mpa), adding the dissolved substance of the composition of the phase B in the step S2 into the emulsifying pot, emulsifying and homogenizing for 4-5 minutes, preserving heat and defoaming for 20 minutes to ensure that no bubbles are emitted, and starting to cool.
FIG. 1 is a diagram of the structure of a mud film with a spatial cage structure observed under the microscope Regulus 3.0kV 8.9mm x1.5k SE (UL), when the ruler is marked 30 microns.
FIG. 2 is a diagram of the structure of a mud film with a space cage structure as observed under the microscope Regulus 8.0kV 8.9 mm. times.6.00k SE (UL), when the ruler is 5 microns.
The implementation case is as follows:
a mud film with a space cage type structure, which comprises a phase A composition, a phase B composition and a phase C composition;
the A phase composition comprises: hydrosolvent, kaolin, glycerin, butanediol, sodium hyaluronate, menthol lactate, xanthan gum and p-hydroxyacetophenone;
the B phase composition comprises: caprylic or capric triglyceride, squalane, cyclopentadimethylsiloxane, polysorbate-60, sorbitan laurate, polydimethylsiloxane, sodium polyacryloyldimethyltaurate, isohexadecane, and PEG-7 glyceryl cocoate;
the C phase composition comprises: tripeptide-1 copper, ceramide NP, hydroxypropyl tetrahydropyranyl triol, methyl propylene glycol, and 1, 2-hexanediol;
the composition comprises the following components in percentage by weight:
60-75% of water solvent, 4.0-6.0% of kaolin, 2.2-3.5% of glycerol, 2.2-3.5% of butanediol, 0.01-0.05% of sodium hyaluronate, 0.15-0.3% of menthol lactate, 0.11-0.2% of xanthan gum and 0.4-0.6% of p-hydroxyacetophenone;
caprylic or capric triglyceride 4.5-7%, squalane 4.0-6.5%, cyclopentadimethylsiloxane 2.3-3.0%, polysorbate-602.0-2.7%, sorbitan laurate 2.0-2.7%, polydimethylsiloxane 0.4-0.8%, sodium polyacryloyldimethyltaurate 0.1-0.5%, isohexadecane 0.05-0.2% and PEG-7 glyceryl cocoate 0.01-0.07%;
the C phase composition comprises: tripeptide-1 copper 0.05-0.15%, ceramide NP 0.007-0.02%, hydroxypropyl tetrahydropyrane triol 0.03-0.15%, methyl propylene glycol 0.02-0.1% and 1, 2-hexanediol 0.4-1.0%.
A preparation method of a mud membrane with a space cage type structure comprises the following steps:
s1: cleaning and sterilizing the production equipment and the using tools, and then checking whether all valves of the emulsifying pot are closed.
S2: adding the phase A into an emulsifying pot, starting homogenizing for 5-8 minutes, stirring and heating to 85 ℃, and keeping the temperature for 10 minutes until complete dissolution is ensured; adding the B phase material into an oil phase pot, stirring and heating to 80 ℃ until the B phase material is completely dissolved.
S3: and (3) keeping the emulsifying pot in a vacuum state (-0.05mpa), adding the dissolved substance of the composition of the phase B in the step S2 into the emulsifying pot, emulsifying and homogenizing for 4-5 minutes, preserving heat and defoaming for 20 minutes to ensure that no bubbles are emitted, and starting to cool.
S4: cooling to 45 deg.C, adding the C phase material into emulsifying pot, and stirring for cooling.
S5: cooling to 38 ℃, stopping stirring, detecting the quality of the mud film, and discharging when the mud film is qualified.
Experiment of
The obtained mud film with the space cage-shaped structure is subjected to the following tests:
1.1 Experimental materials: a mud film with a space cage-type structure, a comparative example group and a blank group;
1.2 Experimental groups and subgroups
Selecting females with the age range of 20-30 years old and males with the age range of 20-30 years old, wherein the weight difference of the females and the males is not obvious, and dividing the females and the males into 3 main groups according to the principles of similar weight and similar morphological difference, wherein the main groups are respectively an experimental group, a comparative group and a blank group;
1.3 design of test date and treatment
The metabolic cycle of the Skin is generally 28 days (D28), 14 days (D14) and 28 days (D28) can be selected as detection time, a Skin tester is selected as a test instrument to detect the Skin, and the current sensory experience is scored after the test is finished;
the mud film of the comparative example group is prepared from the following raw materials: phase A: 70-80% of aqueous solution, 4.0-6.0% of kaolin, 2.2-3.5% of glycerol, 2.2-3.5% of butanediol, 0.005-0.01% of sodium hyaluronate, 0.11-0.2% of xanthan gum, 0.3-0.5% of magnesium aluminum silicate and 0.4-0.6% of p-hydroxyacetophenone;
phase B: 4.5-7% of caprylic/capric triglyceride, 4.0-6.5% of squalane, 2.3-3.0% of cyclopentadimethylsiloxane, 2.2-2.2% of polysorbate-601.0, 1.5-2.3% of sorbitan laurate and 0.4-0.8% of polydimethylsiloxane;
and C phase: tripeptide-1 copper 0.005-0.01%, hydroxypropyl tetrahydropyrane triol 0.002-0.01%, methyl propylene glycol 0.02-0.1%, 1, 2-hexanediol 0.4-1.0%;
blank set is the average of natural growth without interference.
2.4 results and analysis
TABLE 1 influence of pellicles with space cage structure on the growth performance of face
Note: examples 1-10 were 20-30 year old women, examples 11-14 were 20-30 year old men, and the comparative example group had a male-female ratio of approximately that of the example group, and the blank group was the population mean.
As can be seen from table 1, in the test population, in the test group, the female and male in the test group, in the skin test using the mud film with the space cage-type structure, the test results of the skin moisture, the skin elasticity, the skin sebum and the skin melanin after the mud film with the space cage-type structure is similar and have no obvious difference, and in the sensory evaluation, the female and female give similar structures and have no obvious difference, wherein the sensory scores given by the female and male are both higher than 8.5 points;
compared with the comparative example group in which the mud film with the space cage-type structure is used, the experimental group has higher detection structures of skin moisture, skin elasticity, skin sebum and skin melanin in 14 days and 28 days than the comparative example group, and the crowd in the experimental group is obviously improved compared with the crowd in the comparative example group in terms of sensory evaluation.
In summary, after reading the present disclosure, those skilled in the art can make various other corresponding changes without creative mental work according to the technical solutions and concepts of the present disclosure, and all of them are within the protection scope of the present disclosure.
Claims (8)
1. The mud film with a space cage type structure is characterized by comprising an A phase composition, a B phase composition and a C phase composition;
the A phase composition comprises: hydrosolvent, kaolin, glycerin, butanediol, sodium hyaluronate, menthol lactate, xanthan gum and p-hydroxyacetophenone;
the B phase composition comprises: caprylic or capric triglyceride, squalane, cyclopentadimethylsiloxane, polysorbate-60, sorbitan laurate, polydimethylsiloxane, sodium polyacryloyldimethyltaurate, isohexadecane, and PEG-7 glyceryl cocoate;
the C phase composition comprises: tripeptide-1 copper, ceramide NP, hydroxypropyl tetrahydropyrane triol, methyl propylene glycol, and 1, 2-hexanediol.
2. The mud film with the space cage-type structure as claimed in claim 1, wherein the percentage of each component in the phase A composition, the phase B composition and the phase C composition is as follows:
50-80% of water solvent, 3.0-6.0% of kaolin, 2.0-4.0% of glycerol, 2.0-4.0% of butanediol, 0.01-0.1% of sodium hyaluronate, 0.1-0.5% of menthol lactate, 0.1-0.5% of xanthan gum and 0.1-1% of p-hydroxyacetophenone;
caprylic or capric triglyceride 2.0-10.0%, squalane 2.0-7.0%, cyclopentadimethylsiloxane 2.0-4.0%, polysorbate-602.0-3.0%, sorbitan laurate 2.0-3.0%, polydimethylsiloxane 0.2-1.0%, sodium polyacryloyldimethyltaurate 0.1-1.0%, isohexadecane 0.01-0.3% and PEG-7 glyceryl cocoate 0.01-0.1%;
tripeptide-1 copper 0.05-0.2%, ceramide NP 0.005-0.02%, hydroxypropyl tetrahydropyrane triol 0.02-0.2%, methyl propylene glycol 0.01-0.15% and 1, 2-hexanediol 0.2-1.5%.
3. The mud film with the space cage type structure as claimed in claim 2, wherein the percentage content of each component in the phase A composition, the phase B composition and the phase C composition is as follows:
60-75% of water solvent, 4.0-6.0% of kaolin, 2.2-3.5% of glycerol, 2.2-3.5% of butanediol, 0.01-0.05% of sodium hyaluronate, 0.15-0.3% of menthol lactate, 0.11-0.2% of xanthan gum and 0.4-0.6% of p-hydroxyacetophenone;
caprylic or capric triglyceride 4.5-7%, squalane 4.0-6.5%, cyclopentadimethylsiloxane 2.3-3.0%, polysorbate-602.0-2.7%, sorbitan laurate 2.0-2.7%, polydimethylsiloxane 0.4-0.8%, sodium polyacryloyldimethyltaurate 0.1-0.5%, isohexadecane 0.05-0.2% and PEG-7 glyceryl cocoate 0.01-0.07%;
tripeptide-1 copper 0.05-0.15%, ceramide NP 0.007-0.02%, hydroxypropyl tetrahydropyrane triol 0.03-0.15%, methyl propylene glycol 0.02-0.1% and 1, 2-hexanediol 0.4-1.0%.
4. A preparation method of a mud membrane with a space cage type structure is characterized by comprising the following steps:
s1: cleaning and sterilizing the production equipment and the using tools, and then checking whether all valves of the emulsifying pot are closed.
S2: adding the phase A into an emulsifying pot, starting homogenizing for 5-10 minutes, stirring and heating to 80-90 ℃, and preserving heat for 5-15 minutes until complete dissolution is ensured; adding the B phase material into the oil phase pan, stirring and heating to 75-85 deg.C until completely dissolved.
S3: and (3) keeping the emulsifying pot in a vacuum state, adding the dissolved substance of the composition of the phase B in the step S2 into the emulsifying pot, emulsifying and homogenizing for 3-6 minutes, preserving heat and defoaming for 15-25 minutes to ensure that no bubbles emerge, and starting to cool.
S4: cooling to 40-50 deg.C, adding the C phase material into emulsifying pot, and stirring for cooling.
S5: cooling to 35-40 deg.C, stopping stirring, detecting the quality of mud film, and discharging when it is qualified.
5. The method for preparing a mud film with a space cage type structure as claimed in claim 4, wherein said step S2 comprises: adding the phase A into an emulsifying pot, starting homogenizing for 5-8 minutes, stirring and heating to 85 ℃, and keeping the temperature for 10 minutes until complete dissolution is ensured; adding the B phase material into an oil phase pot, stirring and heating to 80 ℃ until the B phase material is completely dissolved.
6. The method for preparing a mud film with a space cage type structure as claimed in claim 4, wherein said step S3 comprises: and (4) keeping the vacuum state of an emulsifying pot, adding the dissolved substance of the composition of the phase B in the step S2 into the emulsifying pot, emulsifying and homogenizing for 4-5 minutes, preserving heat and defoaming for 20 minutes to ensure that no bubbles emerge, and starting to cool.
7. The method for preparing the mud film with the space cage type structure as claimed in claim 6, wherein the vacuum state is-0.08 mpa-0.02 mpa.
8. The method for preparing the mud film with the space cage type structure as claimed in claim 7, wherein the vacuum state is-0.05 mpa.
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