CN114948870B - 一种增加破壁灵芝孢子粉悬浮时间的方法 - Google Patents
一种增加破壁灵芝孢子粉悬浮时间的方法 Download PDFInfo
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Abstract
本发明提供一种增加破壁灵芝孢子粉悬浮时间的方法,涉及破壁灵芝孢子粉加工技术领域。所述增加破壁灵芝孢子粉悬浮时间的方法主要包括对破壁灵芝孢子粉进行分级筛选、将孢子粉混合分散剂并超声分散、冻干研磨等步骤。本发明克服了现有技术的不足,通过破壁灵芝孢子粉粒径的筛选和分散剂的配合,有效提升壁灵芝孢子粉冲泡过程中的均匀性和分散性,便于形成均匀的悬浮液,方便食用,减少沉底、挂壁的浪费。
Description
技术领域
本发明涉及破壁灵芝孢子粉加工技术领域,具体涉及一种增加破壁灵芝孢子粉悬浮时间的方法。
背景技术
灵芝孢子是灵芝在生长成熟期,从灵芝菌褶中弹射出来的极其微小的卵形生殖细胞即灵芝的种子,灵芝孢子粉具有灵芝的全部遗传物质和保健作用,其具有增强机体免疫力、抑制肿瘤、保护肝损伤、辐射防护作用。由于灵芝孢子是活体生物体,具有双壁结构,且壁质地坚韧,由几丁质、纤维素、木质素等构成,这些高分子成分不溶于水,且耐酸碱、耐压、耐高温,对消化酶也非常稳定,使孢子的有效物质被包覆而不易吸收,所以对灵芝孢子进行破壁就成为充分利用灵芝孢子内有效物质的一个途径。
一般来说灵芝孢子粉大多制作成胶囊使用或者直接使用破壁的孢子粉,而破壁灵芝孢子粉在实际的使用过程中一般是采用冲水直接服用,但是由于灵芝孢子粉在为破壁前大多一般能够均匀的分散在水中,而破壁后的灵芝孢子粉由于内部孢子油与外壳混合造成大量沉淀,获得的冲服物,极易挂壁和沉底,容易造成有效物质的浪费,而现有的解决方式大多是采用温度高的热水冲泡,且在冲泡过程中不断搅拌,但是当水温降低或者停止搅拌时又会持续产生沉淀,影响实际食用的便捷性。
发明内容
针对现有技术不足,本发明提供一种增加破壁灵芝孢子粉悬浮时间的方法,通过破壁灵芝孢子粉粒径的筛选和分散剂的配合,有效提升壁灵芝孢子粉冲泡过程中的均匀性和分散性,便于形成均匀的悬浮液,方便食用,减少沉底、挂壁的浪费。
为实现以上目的,本发明的技术方案通过以下技术方案予以实现:
一种增加破壁灵芝孢子粉悬浮时间的方法,所述方法包括以下步骤:
(1)对破壁灵芝孢子粉进行分级筛选:选取破壁后的灵芝孢子粉,筛选出粒径分布在D50(0.2μm-1.0μm)、D50(1.2μm-2.0μm)、D50(2.4μm-4.0μm)三种等级的破壁灵芝孢子粉,进行混合,得多粒径破壁灵芝孢子粉备用;
(2)原料混合:将二羟基丙基十八烷酸酯、海藻酸钠、黄原胶置于去离子水中溶解,后加入上述多粒径破壁灵芝孢子粉和氯化钙搅拌均匀得混合料备用;
(3)分散:将上述混合料加入果酸后置于超声分散机中进行超声分散,后取出得分散料备用;
(4)脱水:将上述分散料加热搅拌浓缩,后进行低温冻干,冻干后取出研磨过筛,再于热锅中翻炒后取出,风冷,得处理灵芝孢子粉。
优选的,所述步骤(1)中破壁后的灵芝孢子粉的破壁率≥97%。
优选的,所述步骤(1)中粒径分布在D50(0.2μm-1.0μm)、D50(1.2μm-2.0μm)、D50(2.4μm-4.0μm)的破壁灵芝孢子粉质量比为4∶13∶7。
优选的,所述步骤(2)中二羟基丙基十八烷酸酯、海藻酸钠、黄原胶、去离子水、多粒径破壁灵芝孢子粉、氯化钙混合的质量比为2∶7∶3∶200∶100∶0.3。
优选的,所述步骤(2)中二羟基丙基十八烷酸酯、海藻酸钠、黄原胶置于去离子水中溶解的方式为水浴加热至70-80℃,以600-800r/min的转速搅拌15-20min,且后续加入多粒径破壁灵芝孢子粉和氯化钙搅拌的转速为400-600r/min,搅拌混合的时间为20-30min。
优选的,所述步骤(3)中果酸的添加量为混合料质量的0.3-0.7%。
优选的,所述步骤(4)中分散料加热搅拌浓缩的温度为80℃,且浓缩为原有体积的2/3停止加热。
优选的,所述步骤(4)中冻干的温度为零下50℃,且研磨过500目筛。
优选的,所述步骤(4)中热锅翻炒的温度为100-120℃,翻炒时间为1-3min。
本发明提供一种增加破壁灵芝孢子粉悬浮时间的方法,与现有技术相比优点在于:
(1)本发明将破壁灵芝孢子粉按照一定的粒径等级筛选配比,后混合分散剂进行混合后混合其余物质制成网状悬浮结构物质,便于后续对破壁灵芝孢子粉进行冲泡时保持其悬浮性能,防止沉淀和挂壁,提升食用的便捷性;
(2)本发明通过二羟基丙基十八烷酸酯、海藻酸钠、黄原胶混合多粒径破壁灵芝孢子粉和氯化钙能够有效形成均匀的网状交联悬浮物质,防止破壁灵芝孢子粉的沉淀,且在后续脱水粉碎后再冲水能够使得物质快速交联形成网状结构,保证各物质混合的均匀性的同时便于后续冲泡时均匀悬浮液的形成,且粉碎处理也能够使得物质在较广的水温冲泡时均能够快速交联悬浮,便于冲泡食用。
具体实施方式
为使本发明实施例的目的、技术方案和优点更加清楚,下面结合本发明实施例对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
实施例:
处理破壁灵芝孢子粉的制备:
(1)选取破壁率≥97%的破壁芝孢子粉,筛选出粒径分布在D50(0.2μm-1.0μm)、D50(1.2μm-2.0μm)、D50(2.4μm-4.0μm)的三种等级,并按照4∶13∶7的质量比对上述三种等级的破壁灵芝孢子粉进行混合,得多粒径破壁灵芝孢子粉;
(2)将200g的去离子水,水浴加热至70-80℃保温,后添加2g二羟基丙基十八烷酸酯、7g海藻酸钠、3g黄原胶,以700r/min的转速搅拌18min,后加入100g的多粒径破壁灵芝孢子粉和0.3g的氯化钙调整转速至500r/min,混合搅拌25min,得混合料;
(3)将1.5g果酸加入至上述混合料中后置于超声分散机中进行超声分散5min,得分散料;
(4)将上述分散料于80℃温度下加热搅拌浓缩至原有体积的2/3后停止加热,后置于零下50℃环境中低温冻干,将冻干后物质取出研磨过500目筛,后置于100℃的热锅中炒制2min,取出,得处理破壁灵芝孢子粉。
对比例1:
处理破壁灵芝孢子粉的制备:
选取破壁率≥97%的破壁芝孢子粉,筛选出粒径分布在D50(0.2μm-1.0μm)、D50(1.2μm-2.0μm)、D50(2.4μm-4.0μm)的三种等级,并按照4∶13∶7的质量比对上述三种等级的破壁灵芝孢子粉进行混合,得多粒径破壁灵芝孢子粉,为处理破壁灵芝孢子粉;
对比例2:
处理破壁灵芝孢子粉的制备:
(1)选取破壁率≥97%的破壁芝孢子粉,将200g的去离子水,水浴加热至70-80℃保温,后添加2g二羟基丙基十八烷酸酯、7g海藻酸钠、3g黄原胶,以700r/min的转速搅拌18min,后加入100g的多破壁芝孢子粉和0.3g的氯化钙调整转速至500r/min,混合搅拌25min,得混合料;
(2)将1.5g果酸加入至上述混合料中后置于超声分散机中进行超声分散5min,得分散料;
(3)将上述分散料于80℃温度下加热搅拌浓缩至原有体积的2/3后停止加热,后置于零下50℃环境中低温冻干,将冻干后物质取出研磨过500目筛,后置于100℃的热锅中炒制2min,取出,得处理破壁灵芝孢子粉。
对比例3:
处理破壁灵芝孢子粉的制备:
(1)选取破壁率≥97%的破壁芝孢子粉,筛选出粒径分布在D50(0.2μm-1.0μm)、D50(1.2μm-2.0μm)、D50(2.4μm-4.0μm)的三种等级,并按照4∶13∶7的质量比对上述三种等级的破壁灵芝孢子粉进行混合,得多粒径破壁灵芝孢子粉;
(2)将200g的去离子水,水浴加热至70-80℃保温,后添加2g二羟基丙基十八烷酸酯、7g海藻酸钠、3g黄原胶,以700r/min的转速搅拌18min,后加入100g的多粒径破壁灵芝孢子粉和0.3g的氯化钙调整转速至500r/min,混合搅拌25min,得混合料;
(3)将上述混合料置于超声分散机中进行超声分散5min,得分散料;
(4)将上述分散料于80℃温度下加热搅拌浓缩至原有体积的2/3后停止加热,后置于零下50℃环境中低温冻干,将冻干后物质取出研磨过500目筛,后置于100℃的热锅中炒制2min,取出,得处理破壁灵芝孢子粉。
对比例4:
处理破壁灵芝孢子粉的制备:
(1)选取破壁率≥97%的破壁芝孢子粉,筛选出粒径分布在D50(0.2μm-1.0μm)、D50(1.2μm-2.0μm)、D50(2.4μm-4.0μm)的三种等级,并按照4∶13∶7的质量比对上述三种等级的破壁灵芝孢子粉进行混合,得多粒径破壁灵芝孢子粉;
(2)将200g的去离子水,水浴加热至70-80℃保温,后添加2g丙基十八烷酸酯、7g海藻酸钠、3g黄原胶,以700r/min的转速搅拌18min,后加入100g的多粒径破壁灵芝孢子粉和0.3g的氯化钙调整转速至500r/min,混合搅拌25min,得混合料;
(3)将1.5g果酸加入至上述混合料中后置于超声分散机中进行超声分散5min,得分散料;
(4)将上述分散料置于零下50℃环境中低温冻干,取出,得处理破壁灵芝孢子粉。
检测:
对上述实施例和对比例1-4所得到的处理破壁灵芝孢子粉进行个悬浮实验检测,每组取处理破壁灵芝孢子粉10g,选取100ml的不同温度的清水在同一规格的玻璃杯中进行冲泡,冲泡时采用玻璃棒搅拌均匀,检测不同时间下沉淀情况计算沉淀率(沉淀计算方法为在规定时间将比例被中的液体以5-8ml/s的速度缓慢倾倒至只剩杯底,后将玻璃杯中的沉淀和挂壁物质干燥后称重记为W1,则沉淀率%=W1/10),具体结果如下表所示:
由上表可知,本发明处理的破壁灵芝孢子粉在不同温度下的水冲泡搅拌后均具有良好的悬浮性,且悬浮时间较长,悬浮性能稳定,而未添加分散剂处理的普通分级粒径的破壁灵芝孢子粉悬浮性能较差,易沉淀,且普通未分级的破壁灵芝孢子粉在仅经过分散剂处理后能有效提升悬浮性,但是其受温度影响较大且,且对后续处理后的物质冻干粉碎处理等一系列处理也能够有效降低温度对悬浮性的影响,提升破壁灵芝孢子粉悬浮的稳定性。
需要说明的是,在本文中,诸如第一和第二等之类的关系术语仅仅用来将一个实体或者操作与另一个实体或操作区分开来,而不一定要求或者暗示这些实体或操作之间存在任何这种实际的关系或者顺序。而且,术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性的包含,从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素,而且还包括没有明确列出的其他要素,或者是还包括为这种过程、方法、物品或者设备所固有的要素。在没有更多限制的情况下,由语句“包括一个……”限定的要素,并不排除在包括所述要素的过程、方法、物品或者设备中还存在另外的相同要素。
以上实施例仅用以说明本发明的技术方案,而非对其限制;尽管参照前述实施例对本发明进行了详细的说明,本领域的普通技术人员应当理解:其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分技术特征进行等同替换;而这些修改或者替换,并不使相应技术方案的本质脱离本发明各实施例技术方案的精神和范围。
Claims (7)
1.一种增加破壁灵芝孢子粉悬浮时间的方法,其特征在于,所述方法包括以下步骤:
(1)对破壁灵芝孢子粉进行分级筛选:选取破壁后的灵芝孢子粉,筛选出粒径分布在D50分别为0.2μm-1.0μm、1.2μm-2.0μm、2.4μm-4.0μm三种等级的破壁灵芝孢子粉,进行混合,得多粒径破壁灵芝孢子粉备用,且粒径分布在D50分别为0.2μm-1.0μm、1.2μm-2.0μm、2.4μm-4.0μm的破壁灵芝孢子粉质量比为4∶13∶7;
(2)原料混合:将二羟基丙基十八烷酸酯、海藻酸钠、黄原胶置于去离子水中溶解,后加入上述多粒径破壁灵芝孢子粉和氯化钙搅拌均匀得混合料备用,且二羟基丙基十八烷酸酯、海藻酸钠、黄原胶、去离子水、多粒径破壁灵芝孢子粉、氯化钙混合的质量比为2∶7∶3∶200∶100∶0.3;
(3)分散:将上述混合料加入果酸后置于超声分散机中进行超声分散,后取出得分散料备用;
(4)脱水:将上述分散料加热搅拌浓缩,后进行低温冻干,冻干后取出研磨过筛,再于热锅中翻炒后取出,风冷,得处理灵芝孢子粉。
2.根据权利要求1所述的一种增加破壁灵芝孢子粉悬浮时间的方法,其特征在于:所述步骤(1)中破壁后的灵芝孢子粉的破壁率≥97%。
3.根据权利要求1所述的一种增加破壁灵芝孢子粉悬浮时间的方法,其特征在于:所述步骤(2)中二羟基丙基十八烷酸酯、海藻酸钠、黄原胶置于去离子水中溶解的方式为水浴加热至70-80℃,以600-800r/min的转速搅拌15-20min,且后续加入多粒径破壁灵芝孢子粉和氯化钙搅拌的转速为400-600r/min,搅拌混合的时间为20-30min。
4.根据权利要求1所述的一种增加破壁灵芝孢子粉悬浮时间的方法,其特征在于:所述步骤(3)中果酸的添加量为混合料质量的0.3-0.7%。
5.根据权利要求1所述的一种增加破壁灵芝孢子粉悬浮时间的方法,其特征在于:所述步骤(4)中分散料加热搅拌浓缩的温度为80℃,且浓缩为原有体积的2/3停止加热。
6.根据权利要求1所述的一种增加破壁灵芝孢子粉悬浮时间的方法,其特征在于:所述步骤(4)中冻干的温度为零下50℃,且研磨过500目筛。
7.根据权利要求1所述的一种增加破壁灵芝孢子粉悬浮时间的方法,其特征在于:所述步骤(4)中热锅翻炒的温度为100-120℃,翻炒时间为1-3min。
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