CN114853469A - 一种防滑陶瓷岩板的制备方法 - Google Patents

一种防滑陶瓷岩板的制备方法 Download PDF

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CN114853469A
CN114853469A CN202210564281.8A CN202210564281A CN114853469A CN 114853469 A CN114853469 A CN 114853469A CN 202210564281 A CN202210564281 A CN 202210564281A CN 114853469 A CN114853469 A CN 114853469A
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薛健
杨立辉
唱学彬
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Hebei Lingbiao Technology Development Co ltd
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Abstract

本发明提供了一种防滑陶瓷岩板的制备方法，属于陶瓷岩板技术领域。本发明首先将坯体原料磨成浆料后形成坯体干粉，将干粉压制制备得到陶瓷岩板生坯；陶瓷岩板生坯于150‑200℃下干燥10‑15h；对步骤(2)干燥后的陶瓷岩板生坯施面釉浆料，得面釉层，施粗糙釉浆料，得防滑耐磨釉层陶瓷岩板坯，然后经干燥和烧成，制备得到防滑陶瓷岩板。本发明提供的防滑陶瓷岩板通过提升地面陶瓷岩板的防滑性能，可以很好地降低意外滑倒造成伤害事件的发生概率，还具有优良的防污性能。

Description

一种防滑陶瓷岩板的制备方法
技术领域
本发明属于陶瓷岩板技术领域，具体涉及一种防滑陶瓷岩板的制备方法。
背景技术
陶瓷岩板作为一种新型陶瓷产品，其超大的规格能承载比传统陶瓷岩板更为丰富的纹理元素，加上装饰效果简洁大气、留缝少、避免藏污纳垢、施工铺贴效率高等优势，使其在高端家居产品市场中的占有率不断增大。但是，近年来，由于地面装饰材料光滑而导致意外伤害事件，使消费者对地面铺贴材料的防滑性能格外关注。陶瓷岩板作为一种最广泛应用于各种公共场所和家庭装修的地面铺贴材料，对其防滑性能的关注度更高。目前防滑陶瓷岩板主要是通过喷洒或涂抹防滑剂、腐蚀剂或选用特殊干粒材料、凹凸模具、提高釉温等方式，将陶瓷岩板表面制成具有宏观或微观的凹凸结构，利用这种结构，在压力下和鞋底产生的机械咬合作用以及真空吸附作用来达到防滑效果。
申请号为CN 202111223691.8的专利公布了一种具有深刻凹凸纹理的陶瓷岩板及其制备方法，该专利采用特殊模具压制成型，使表面形成颗粒凹凸点，施釉烧成后表面存在细小颗粒效果，达到防滑效果，但是这类产品由于坯面有凹凸模具效果，不同的压制效果，其产品的质感差异较大。且模具多次压制后，模具有损耗，坯面效果会产生明显差异变化，产品难以获得稳定一致的防滑效果，且陶瓷岩板由于产品规格大，坯体薄，采用凹凸模具压制成型易造成陶瓷岩板坯体开裂、强度差、加工性能差等问题。
申请号为CN 202011404686.2的专利公布了一种细砂防滑陶瓷岩板的制备方法及制备的细砂防滑陶瓷岩板，该专利采用以高温粘度大，烧成范围宽，外添加粘结剂的釉料为底釉，结合高压喷釉工艺，使雾化后的釉料与高温坯体接触后，水分迅速蒸发，底部与坯体形成结合层，面部形成较致密的细颗粒层，该细颗粒层高温烧成后形成具有防滑功能的细砂防滑陶瓷岩板。但是该专利存在工艺复杂、釉面光泽波动大、质感低端等问题。
发明内容
有鉴于此，本发明提供了一种防滑陶瓷岩板的制备方法，本发明提供的防滑陶瓷岩板通过提升地面陶瓷岩板的防滑性能，可以很好地降低意外滑倒造成的伤害事件的发生概率，还具有优良的防污性能。
本发明的目的是提供一种防滑陶瓷岩板的制备方法，包括以下步骤：
(1)将坯体原料磨成浆料后形成坯体干粉，将干粉压制，得到陶瓷岩板生坯；
(2)陶瓷岩板生坯进行第一次干燥，所述干燥温度为150-200℃，干燥时间为10-15h；
(3)对步骤(2)干燥后的陶瓷岩板生坯施面釉浆料，进行第二次干燥，得面釉层，施粗糙釉浆料，进行第三次干燥，得防滑耐磨釉层陶瓷岩板坯，然后经保温、烧成，制备得到防滑陶瓷岩板。
优选的，步骤(1)中所述坯体，以重量份数计，由以下原料组成：钾长石15-20份、钠长石10-15份、透辉石5-8份、锆英砂30-35份、铁矿石3-5份、煅烧高岭土20-25份、霞石1-5份、膨润土8-10份以及硫酸镁1-3份。
优选的，步骤(1)中所述压制压力350～450Kg/cm2，所述坯体规格：长1.5～3.0m、宽0.5～1.5m，厚度＜8mm。
优选的，步骤(3)中所述面釉由以下重量份的原料构成：钾长石36份、霞长石12份、煅烧土10份、高岭土7份、氧化铝16份、石英17份、白云石1份、烧滑石1份。
优选的，步骤(3)中所述粗糙釉由以下重量份的原料构成：高温透明熔块粉60-100份，煅烧高岭土25-35份，氧化铝1～2份，将以上原料加水球磨后制成釉浆。
优选的，所述高温透明熔块粉购买自广东源磊粉体有限公司。
优选的，步骤(3)中所述第二次干燥温度为110～120℃，所述第二次干燥的干燥时间为2～4min。
优选的，步骤(3)中所述第三次干燥的干燥温度为80～100℃，所述第三次干燥的干燥时间为2～4min。
优选的，步骤(3)中所述烧成温度1172～1193℃，高火保温时间8～12分钟，烧成时间150～200分钟。
与现有技术相比，本发明具有以下有益效果：
本文在普通陶瓷岩板上布施两道釉，第一道面釉为防污釉，建议选择亚光釉，有利于防滑性能的提高，第二道粗糙釉，加入的高温透明熔块细粉，增加砖面的粗糙度，起到防滑作用。通过两种釉料的性能结合，使陶瓷岩板的防滑系数上稳定在一个较高的数值上，达到提高防滑性能、且兼具防污性能的目的。同时，本发明提供的防滑陶瓷岩板的制备工艺具有实施简单，可以在不影响原有产品的工艺配方的前提下，通过增加一道粗糙釉提升防滑性能，具有较好的推广价值。
具体实施方式
为使本发明的目的、技术方案和优点更加清楚，下面将对本发明的技术方案进行清楚、完整的描述。显然，所描述的实施例仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动的前提下所得到的所有其它实施例，都属于本发明所保护的范围。
下述实施例中所述试验方法或测试方法，如无特殊说明，均为常规方法；所述原料和助剂，如无特殊说明，均从常规商业途径获得，或以常规方法制备。
采用GB/T 4100测试湿水静摩擦系数；采用GB/T 4100测试干法静摩擦系数；采用GB/T 3810.7测试釉面耐磨度；采用GB/T 3810.14测试釉面耐污染性。
实施例1
一种防滑陶瓷岩板的制备方法，具体由以下步骤制备而成：
(1)将坯体原料，钾长石15份、钠长石10份、透辉石5份、锆英砂30份、铁矿石3份、煅烧高岭土20份、霞石1份、膨润土8份以及硫酸镁1份混合后，磨成浆料，形成坯体干粉，将干粉在压力350Kg/cm2的条件下压制制备得到长1.5m、宽0.5m，厚度4mm的陶瓷岩板生坯；
(2)陶瓷岩板生坯于150℃下干燥15h；
(3)对步骤(2)干燥后的陶瓷岩板生坯施面釉浆料，所述面釉浆料的制备方法为，将钾长石36份、霞长石12份、煅烧土10份、高岭土7份、氧化铝16份、石英17份、白云石1份、烧滑石1份混合后加水球磨成粒度为200目制成含水率为6.3-8.5％的釉浆，在温度为110℃的条件下干燥4min，得面釉层；施粗糙釉浆料，所述粗糙釉浆料的制备方法为，将高温透明熔块粉60份，煅烧高岭土25份，氧化铝1份，混合后加水球磨成粒度为200目制成含水率为5％的釉浆，在温度为80℃的条件下干燥2min，得防滑耐磨釉层陶瓷岩板坯，最后在1172℃的温度条件下，高火保温8分钟，烧成150分钟，制备得到防滑陶瓷岩板。
实施例2所得的防滑陶瓷岩板的湿水静摩擦系数为1.15，干法静摩擦系数为1.05，釉面耐磨度为12000转，4级，耐污染性5级。
实施例2
一种防滑陶瓷岩板的制备方法，具体由以下步骤制备而成：
(1)将坯体原料，钾长石18份、钠长石13份、透辉石7份、锆英砂32份、铁矿石4份、煅烧高岭土23份、霞石3份、膨润土9份以及硫酸镁2份混合后，磨成浆料，形成坯体干粉，将干粉在压力400Kg/cm2的条件下压制制备得到长2.0m、宽1m，厚度6mm的陶瓷岩板生坯；
(2)陶瓷岩板生坯于180℃下干燥12h；
(3)对步骤(2)干燥后的陶瓷岩板生坯施面釉浆料，所述面釉浆料的制备方法为，将钾长石36份、霞长石12份、煅烧土10份、高岭土7份、氧化铝16份、石英17份、白云石1份、烧滑石1份混合后加水球磨成粒度为200目制成含水率为6.3-8.5％的釉浆，在温度为115℃的条件下干燥3min，得面釉层；施粗糙釉浆料，所述粗糙釉浆料的制备方法为，将高温透明熔块粉80份，煅烧高岭土30份，氧化铝1份，混合后加水球磨成粒度为200目制成含水率为6.5％的釉浆，在温度为90℃的条件下干燥3min，得防滑耐磨釉层陶瓷岩板坯，最后在1183℃的温度条件下，高火保温10分钟，烧成180分钟，制备得到防滑陶瓷岩板。
实施例2所得的陶瓷砖的湿水静摩擦系数为1.05，干法静摩擦系数为1.15，釉面耐磨度为12000转，4级，耐污染性5级。
实施例3
一种防滑陶瓷岩板的制备方法，具体由以下步骤制备而成：
(1)将坯体原料，钾长石20份、钠长石15份、透辉石8份、锆英砂35份、铁矿石5份、煅烧高岭土25份、霞石5份、膨润土10份以及硫酸镁3份混合后，磨成浆料，形成坯体干粉，将干粉在压力450Kg/cm2的条件下压制制备得到长3.0m、宽1.5m，厚度8mm的陶瓷岩板生坯；
(2)陶瓷岩板生坯于150-200℃下干燥10-15h；
(3)对步骤(2)干燥后的陶瓷岩板生坯施面釉浆料，所述面釉浆料的制备方法为，将钾长石36份、霞长石12份、煅烧土10份、高岭土7份、氧化铝16份、石英17份、白云石1份、烧滑石1份混合后加水球磨成粒度为200目制成含水率为8.5％的釉浆，在温度为120℃的条件下干燥4min，得面釉层；施粗糙釉浆料，所述粗糙釉浆料的制备方法为，将高温透明熔块粉100份，煅烧高岭土35份，氧化铝2份，混合后加水球磨成粒度为200目制成含水率为7.5％的釉浆，在温度为100℃的条件下干燥2min，得防滑耐磨釉层陶瓷岩板坯，最后在1193℃的温度条件下，高火保温8分钟，烧成150分钟，制备得到防滑陶瓷岩板。
实施例3所得的防滑陶瓷岩板的湿水静摩擦系数为0.98，干法静摩擦系数为0.99，釉面耐磨度为13000转，4级，耐污染性5级。
对比例1
本对比例提供了一种防滑陶瓷岩板，对比例1与实施例1的不同之处在于，未涂覆粗糙釉。
对比例1所得的陶瓷砖的湿水静摩擦系数为0.25，干法静摩擦系数为0.35，釉面耐磨度为12000转，3级，耐污染性4级。
以上所述仅是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明原理的前提下，还可以做出若干改进和润饰，这些改进和润饰也应视为本发明的保护范围。

Claims (8)

1.一种防滑陶瓷岩板的制备方法，其特征在于，包括以下步骤：
(1)将坯体原料磨成浆料后形成坯体干粉，将干粉压制，得到陶瓷岩板生坯；
(2)陶瓷岩板生坯进行第一次干燥，所述干燥温度为150-200℃，干燥时间为10-15h；
(3)对步骤(2)干燥后的陶瓷岩板生坯施面釉浆料，进行第二次干燥，得面釉层，施粗糙釉浆料，进行第三次干燥，得防滑耐磨釉层陶瓷岩板坯，然后经保温烧成，制备得到防滑陶瓷岩板。
2.根据权利要求1所述的防滑陶瓷岩板的制备方法，其特征在于，步骤(1)中所述坯体，以重量份数计，由以下原料组成：钾长石15-20份、钠长石10-15份、透辉石5-8份、锆英砂30-35份、铁矿石3-5份、煅烧高岭土20-25份、霞石1-5份、膨润土8-10份以及硫酸镁1-3份。
3.根据权利要求1所述的防滑陶瓷岩板的制备方法，其特征在于，步骤(1)中所述压制压力350～450Kg/cm2，所述坯体规格：长1.5～3.0m、宽0.5～1.5m，厚度＜8mm。
4.根据权利要求1所述的防滑陶瓷岩板的制备方法，其特征在于，步骤(3)中所述面釉由以下重量份的原料构成：钾长石36份、霞长石12份、煅烧土10份、高岭土7份、氧化铝16份、石英17份、白云石1份、烧滑石1份。
5.根据权利要求1所述的防滑陶瓷岩板的制备方法，其特征在于，步骤(3)中所述粗糙釉由以下重量份的原料构成：高温透明熔块粉60-100份，煅烧高岭土25-35份，氧化铝1～2份，将以上原料加水球磨后制成釉浆。
6.根据权利要求1所述的防滑陶瓷岩板的制备方法，其特征在于，步骤(3)中所述第二次干燥温度为110～120℃，所述第二次干燥的干燥时间为2～4min。
7.根据权利要求1所述的防滑陶瓷岩板的制备方法，其特征在于，步骤(3)中所述第三次干燥的干燥温度为80～100℃，所述第三次干燥的干燥时间为2～4min。
8.根据权利要求1所述的防滑陶瓷岩板的制备方法，其特征在于，步骤(3)中所述烧成温度为1172～1193℃，保温时间为8～12分钟，烧成时间150～200分钟。
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