CN114702346A - Chrysanthemum nutrient fertilizer and preparation method thereof - Google Patents
Chrysanthemum nutrient fertilizer and preparation method thereof Download PDFInfo
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 130
- 235000007516 Chrysanthemum Nutrition 0.000 title claims abstract description 55
- 235000015097 nutrients Nutrition 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 35
- 241000723353 Chrysanthemum Species 0.000 title abstract description 9
- 239000000843 powder Substances 0.000 claims abstract description 45
- 238000000034 method Methods 0.000 claims abstract description 30
- 230000000813 microbial effect Effects 0.000 claims abstract description 24
- 230000008569 process Effects 0.000 claims abstract description 15
- 235000013619 trace mineral Nutrition 0.000 claims abstract description 13
- 239000011573 trace mineral Substances 0.000 claims abstract description 13
- 244000005700 microbiome Species 0.000 claims abstract description 7
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims description 63
- 239000000203 mixture Substances 0.000 claims description 58
- 238000000855 fermentation Methods 0.000 claims description 57
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 43
- 239000002994 raw material Substances 0.000 claims description 33
- 239000002245 particle Substances 0.000 claims description 25
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 22
- 239000011591 potassium Substances 0.000 claims description 22
- 229910052700 potassium Inorganic materials 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 20
- 235000009604 Chrysanthemum X morifolium Nutrition 0.000 claims description 17
- 239000007788 liquid Substances 0.000 claims description 15
- 238000007873 sieving Methods 0.000 claims description 15
- 239000002689 soil Substances 0.000 claims description 15
- 235000016709 nutrition Nutrition 0.000 claims description 13
- 238000005273 aeration Methods 0.000 claims description 12
- 238000012258 culturing Methods 0.000 claims description 12
- MOMKYJPSVWEWPM-UHFFFAOYSA-N 4-(chloromethyl)-2-(4-methylphenyl)-1,3-thiazole Chemical compound C1=CC(C)=CC=C1C1=NC(CCl)=CS1 MOMKYJPSVWEWPM-UHFFFAOYSA-N 0.000 claims description 11
- 235000001674 Agaricus brunnescens Nutrition 0.000 claims description 11
- 240000003183 Manihot esculenta Species 0.000 claims description 11
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 11
- 235000007164 Oryza sativa Nutrition 0.000 claims description 11
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 11
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 11
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 11
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 claims description 11
- 229910000389 calcium phosphate Inorganic materials 0.000 claims description 11
- 235000019691 monocalcium phosphate Nutrition 0.000 claims description 11
- 235000009566 rice Nutrition 0.000 claims description 11
- 235000019983 sodium metaphosphate Nutrition 0.000 claims description 11
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 11
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 claims description 11
- 244000307697 Agrimonia eupatoria Species 0.000 claims description 10
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 10
- 238000007605 air drying Methods 0.000 claims description 10
- 229910021538 borax Inorganic materials 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 10
- 239000000835 fiber Substances 0.000 claims description 10
- 238000011081 inoculation Methods 0.000 claims description 10
- 239000003895 organic fertilizer Substances 0.000 claims description 10
- 239000002686 phosphate fertilizer Substances 0.000 claims description 10
- 239000004328 sodium tetraborate Substances 0.000 claims description 10
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 10
- 238000005507 spraying Methods 0.000 claims description 10
- 239000004575 stone Substances 0.000 claims description 10
- 235000000125 common agrimony Nutrition 0.000 claims description 9
- 244000173853 Sanguisorba officinalis Species 0.000 claims description 6
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- 235000010855 food raising agent Nutrition 0.000 claims description 6
- 108010010803 Gelatin Proteins 0.000 claims description 5
- 239000000292 calcium oxide Substances 0.000 claims description 5
- 235000012255 calcium oxide Nutrition 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 229920000159 gelatin Polymers 0.000 claims description 5
- 239000008273 gelatin Substances 0.000 claims description 5
- 235000019322 gelatine Nutrition 0.000 claims description 5
- 235000011852 gelatine desserts Nutrition 0.000 claims description 5
- 239000008187 granular material Substances 0.000 claims description 5
- 239000001963 growth medium Substances 0.000 claims description 5
- 238000009630 liquid culture Methods 0.000 claims description 5
- 238000000643 oven drying Methods 0.000 claims description 5
- 230000002572 peristaltic effect Effects 0.000 claims description 5
- 239000002244 precipitate Substances 0.000 claims description 5
- 238000003825 pressing Methods 0.000 claims description 5
- 238000010298 pulverizing process Methods 0.000 claims description 5
- 238000005086 pumping Methods 0.000 claims description 5
- 239000007858 starting material Substances 0.000 claims description 5
- 230000001954 sterilising effect Effects 0.000 claims description 5
- 239000010902 straw Substances 0.000 claims description 5
- 244000058281 Ulmus pumila Species 0.000 claims description 2
- 235000001547 Ulmus pumila Nutrition 0.000 claims description 2
- 240000007594 Oryza sativa Species 0.000 claims 2
- 239000004615 ingredient Substances 0.000 claims 2
- 235000010894 Artemisia argyi Nutrition 0.000 claims 1
- 241001435059 Artemisia argyi Species 0.000 claims 1
- 241001013248 Eulepidotis folium Species 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 6
- 238000010521 absorption reaction Methods 0.000 abstract description 2
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- 230000000052 comparative effect Effects 0.000 description 5
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 3
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- 238000012360 testing method Methods 0.000 description 2
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- 235000016993 Agrimonia Nutrition 0.000 description 1
- 235000003261 Artemisia vulgaris Nutrition 0.000 description 1
- 240000006891 Artemisia vulgaris Species 0.000 description 1
- 235000008291 Poterium sanguisorba Nutrition 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
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- 238000005286 illumination Methods 0.000 description 1
- 239000010871 livestock manure Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The invention relates to the technical field of plant fertilizer preparation methods, and provides a golden chrysanthemum nutrient fertilizer and a preparation method thereof. The disease occurrence of the golden chrysanthemum flowers and the growth of weeds among flower plants can be inhibited by adding the moxa powder, the occurrence of the wilt of the golden chrysanthemum flowers can be inhibited by combining microorganisms and organic fertilizers by adding the microbial granular fertilizer, the microbial fertilizer can promote the absorption of trace elements by the golden chrysanthemum flowers and offset the negative effects generated by a chemically synthesized fertilizer, the golden chrysanthemum nutrient fertilizer prepared by the invention can promote the growth of the golden chrysanthemum flowers and improve the stress resistance of the golden chrysanthemum flowers in the growth process to a certain extent.
Description
Technical Field
The invention relates to the technical field of preparation methods of plant fertilizers, in particular to a golden chrysanthemum nutrient fertilizer and a preparation method thereof.
Background
The golden chrysanthemum is a rare ornamental flower and an edible flower which are cultivated by long-term artificial selection, the golden chrysanthemum is generally golden yellow, has large balls and more petals, has less wild petals and only one circle, has light green or brown stem color, is mostly provided with upright branches except cliff chrysanthemum, has semi-lignification base, good ornamental performance and excellent medicinal value.
In the existing cultivation of the golden chrysanthemum, organic fertilizers and inorganic fertilizers are usually used, the organic fertilizers are mainly human and animal manure, the accumulation, retting, fermentation, processing techniques and application of the organic fertilizers still stay at the original level, the manufacturing cost of the organic fertilizers is high, the utilization efficiency of effective components of the fertilizers is low, and the requirement of the golden chrysanthemum on nutrition is difficult to meet; the inorganic fertilizer is mainly replaced by crop chemical fertilizer or compound fertilizer, which results in the increase of fertilizer cost and poor fertilizing effect, thereby reducing the commodity value of the golden chrysanthemum, so how to prepare the nutrient fertilizer for promoting the growth of the golden chrysanthemum and improving the commodity value becomes a technical problem to be solved by technical personnel in the field.
Disclosure of Invention
Solves the technical problem
Aiming at the defects of the prior art, the invention provides a Chrysanthemum morifolium nutrient fertilizer and a preparation method thereof, aiming at enabling the Chrysanthemum morifolium nutrient fertilizer to grow and improving the commodity value of the Chrysanthemum morifolium.
Technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme:
a preparation method of a golden chrysanthemum nutrient fertilizer comprises the following preparation steps:
s1, mixing and stirring 25-30 parts of rice bran powder, 4-10 parts of mushroom dregs, 8-12 parts of cassava dregs, 10-15 parts of sawdust, 2-4 parts of borax, 4-6 parts of hairyvein agrimony, 5-10 parts of ulmus pumila leaves, 10-15 parts of medical stone powder, 13-15 parts of soil water-retaining agent and 0.1-0.2 part of fertilizer leavening agent to obtain a fermentation raw material composition;
s2, adding water into the fermentation raw material composition in the S1, stirring while adding water, and detecting the pH value of the fermentation raw material composition after stirring uniformly to ensure that the pH value is 6-9;
s3, piling the fermentation raw material composition treated by the S2, turning when the pile temperature reaches 55-60 ℃, spraying water again on the surface of the partially dried composition in the pile turning process to ensure that the water content is 50-55%, and repeating the pile turning for 1-2 times to obtain the fermentation fertilizer;
s4, mixing 45-55 parts of organic phosphate fertilizer, 1-3 parts of potassium humate, 1-2 parts of trace element fertilizer, 0.4-0.6 part of ammonium sulfate, 0.8-1.5 parts of potassium tripolyphosphate, 0.5-0.7 part of sodium metaphosphate and 1-2 parts of calcium superphosphate, and marking as an organic fertilizer mixture after uniform mixing;
s5, mixing the fermented fertilizer and the organic fertilizer mixture, and then adding 35-40 parts of moxa powder and 20-25 parts of microbial granular fertilizer for mixing again to obtain the golden chrysanthemum nutrient fertilizer.
Further, in the step S2, in the process of adjusting the pH of the fermentation raw material composition, quicklime water is used to pre-adjust the pH.
Further, the water content of the fermentation raw material composition in the S2 is 50-55%.
Further, the pile height in S3 is 1.2-1.5 m, and the pile width is 2 m.
Further, in the above S4, the lump of the above components needs to be pulverized and sieved before mixing until the difference in particle size of all the components is small.
Furthermore, the preparation process of the mugwort powder in the S5 comprises the following steps: cleaning fresh and intact folium Artemisiae Argyi, oven drying at 50-55 deg.C, pulverizing the dried folium Artemisiae Argyi in a pulverizer, and sieving to obtain powder.
Further, the preparation process of the microbial granular fertilizer in S5 comprises the following steps:
a. mixing the crushed sawdust and straw scraps according to the ratio of 1:1, sieving by a 18-mesh sieve after mixing, and then sterilizing for 20min at the high temperature and the high pressure of 121 ℃ to obtain a fiber composition;
b. uniformly mixing the fiber composition with soil according to the proportion of 1:1, adding water, stirring to ensure that the water content is 12-15%, granulating, and air-drying to obtain air-dried granules;
c. uniformly spraying a gelatin solution with the weight ratio of 15% on the surfaces of the air-dried particles, sieving to obtain cylindrical particles with the diameter of 5 mm and the length of 1 mm, and air-drying the cylindrical particles again for later use;
d. inoculating the microbial strain into an R2A liquid culture medium by using an inoculating loop, culturing for 48h at 37 ℃ and 160R/min to prepare an inoculation liquid, then inoculating the inoculation liquid into an aeration fermentation device for aeration culture at room temperature, pumping the fermentation liquid into a high-speed tubular centrifuge by using a peristaltic pump after culturing for 4d, and centrifuging in a 20000R/min mode to obtain a precipitate, namely a strain cell;
e. and (3) mixing and pressing 10mL of strain cells measured by a plate counting method with the air-dried cylindrical particles in 320gc to obtain the microbial granular fertilizer.
Further, the drying temperature in the step b and the step c is 36-40 ℃.
Furthermore, the aeration fermentation device in the step d consists of an air pump connecting filter, a 5-way pipeline and a fermentation bottle.
The golden chrysanthemum nutrient fertilizer is produced by any one of the preparation methods of the golden chrysanthemum nutrient fertilizer, and the golden chrysanthemum nutrient fertilizer mainly comprises the following raw materials: rice bran powder, mushroom residue, cassava residue, sawdust, borax, hairyvein agrimony, sanguisorba officinalis leaves, medical stone powder, a soil water-retaining agent, a fertilizer starter, an organic phosphate fertilizer, potassium humate, a trace element fertilizer, ammonium sulfate, potassium tripolyphosphate, sodium metaphosphate, calcium superphosphate, moxa powder and a microorganism granular fertilizer.
Advantageous effects
The invention provides a golden chrysanthemum nutrient fertilizer and a preparation method thereof, compared with the prior art, the golden chrysanthemum nutrient fertilizer has the following beneficial effects:
according to the invention, the rice bran powder, the mushroom residues, the cassava powder, the sawdust and other plant fertilizers can be used for fermenting the plant fertilizers through the effect of the fertilizer leavening agent, and the plant scraps can be fermented into organic fertilizers with higher organic matter content through a fermentation mode, so that the cost can be saved, and the effective effect of the plant scraps as the fertilizers can be fully exerted. Secondly, organic fertilizers such as potassium humate, trace element fertilizer, ammonium sulfate, potassium tripolyphosphate, sodium metaphosphate and calcium superphosphate are added into the fertilizer, necessary elements required in the growth process of the golden chrysanthemum flowers can be guaranteed, the disease occurrence of the golden chrysanthemum flowers and the growth of weeds among flower plants can be inhibited by adding the moxa powder, finally, the occurrence of the wilt of the golden chrysanthemum flowers can be inhibited by combining microorganisms and the organic fertilizers by adding the microbial granular fertilizer, the microbial fertilizer can promote the absorption of the trace elements by the golden chrysanthemum flowers and offset the negative effects generated by a chemical synthesis fertilizer, the golden chrysanthemum nutrient fertilizer prepared by the invention can promote the growth of the golden chrysanthemum flowers and improve the stress resistance of the golden chrysanthemum flowers in the growth process to a certain degree.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are a part of the embodiments of the present invention, but not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
the preparation method of the Chrysanthemum morifolium nutritional fertilizer comprises the following preparation steps:
s1, mixing and stirring 28 parts of rice bran powder, 10 parts of mushroom residues, 10 parts of cassava residues, 15 parts of sawdust, 2 parts of borax, 5 parts of hairyvein agrimony, 10 parts of elm leaves, 10 parts of medical stone powder, 13 parts of a soil water-retaining agent and 0.1 part of a fertilizer leavening agent to obtain a fermentation raw material composition;
s2, adding water into the fermentation raw material composition in the S1, adding water while stirring in the water adding process, and detecting the pH value of the fermentation raw material composition after stirring uniformly to enable the pH value to be 8;
s3, piling the fermentation raw material composition treated by the S2, turning when the pile temperature reaches 58 ℃, spraying water again on the surface of the partially dried composition in the pile turning process to enable the water content of the composition to be 50%, and repeating pile turning for 2 times to obtain the fermentation fertilizer;
s4, mixing 45 parts of organic phosphate fertilizer, 3 parts of potassium humate, 1 part of trace element fertilizer, 0.5 part of ammonium sulfate, 1.5 parts of potassium tripolyphosphate, 0.5 part of sodium metaphosphate and 1 part of calcium superphosphate, and marking as an organic fertilizer mixture after uniform mixing;
s5, mixing the fermented fertilizer and the organic fertilizer mixture, and then adding 35 parts of moxa powder and 25 parts of microbial granulated fertilizer for mixing again to obtain the golden chrysanthemum nutrient fertilizer.
In the step S2, quicklime water is used to adjust the pH of the fermentation raw material composition.
The water content in the fermentation material composition in S2 was 53%.
The pile height in S3 was 1.5 m, and the pile width was 2 m.
In S4, the lumps of the above components need to be crushed and sieved before mixing until the difference in particle size of all components is small.
The preparation process of the moxa powder in the S5 comprises the following steps: cleaning fresh and intact folium Artemisiae Argyi, oven drying at 55 deg.C, pulverizing the dried folium Artemisiae Argyi in a pulverizer, and sieving to obtain powder.
The preparation process of the microbial granulated fertilizer in the S5 comprises the following steps:
a. mixing the crushed sawdust and straw scraps according to the ratio of 1:1, sieving by a 18-mesh sieve after mixing, and then sterilizing for 20min at the high temperature and the high pressure of 121 ℃ to obtain a fiber composition;
b. uniformly mixing the fiber composition with soil according to the ratio of 1:1, adding water, stirring to ensure that the water content is 15%, granulating, and air-drying to obtain air-dried granules;
c. uniformly spraying a gelatin solution with the weight ratio of 15% on the surfaces of the air-dried particles, sieving to obtain cylindrical particles with the diameter of 5 mm and the length of 1 mm, and air-drying the cylindrical particles again for later use;
d. inoculating the microbial strain into an R2A liquid culture medium by using an inoculating loop, culturing for 48h at 37 ℃ and 160R/min to prepare an inoculation liquid, then inoculating the inoculation liquid into an aeration fermentation device for aeration culture at room temperature, pumping the fermentation liquid into a high-speed tubular centrifuge by using a peristaltic pump after culturing for 4d, and centrifuging in a 20000R/min mode to obtain a precipitate, namely a strain cell;
e. and (3) mixing and pressing 10mL of strain cells measured by a plate counting method with the air-dried cylindrical particles in 320gc to obtain the microbial granular fertilizer.
The drying temperature in step b and step c is 36 ℃.
And d, the ventilation fermentation device in the step d consists of an air pump connecting filter, a 5-way pipeline and a fermentation bottle.
The golden chrysanthemum nutrient fertilizer is produced by any one of the preparation methods of the golden chrysanthemum nutrient fertilizer, and the golden chrysanthemum nutrient fertilizer mainly comprises the following raw materials: rice bran powder, mushroom residue, cassava residue, sawdust, borax, hairyvein agrimony, sanguisorba officinalis leaves, medical stone powder, a soil water-retaining agent, a fertilizer starter, an organic phosphate fertilizer, potassium humate, a trace element fertilizer, ammonium sulfate, potassium tripolyphosphate, sodium metaphosphate, calcium superphosphate, moxa powder and a microorganism granular fertilizer.
Example 2:
the preparation method of the Chrysanthemum morifolium nutritional fertilizer comprises the following preparation steps:
s1, mixing and stirring 30 parts of rice bran powder, 4 parts of mushroom residues, 8 parts of cassava residues, 10 parts of sawdust, 4 parts of borax, 4 parts of hairyvein agrimonia herb and bud, 8 parts of elm leaves, 13 parts of medical stone powder, 14 parts of soil water-retaining agent and 0.1 part of fertilizer leavening agent to obtain a fermentation raw material composition;
s2, adding water into the fermentation raw material composition in the S1, adding water while stirring in the water adding process, and detecting the pH value of the fermentation raw material composition after stirring uniformly to ensure that the pH value is 6;
s3, piling the fermentation raw material composition treated by the S2, turning when the pile temperature reaches 55 ℃, spraying water again on the surface of the partially dried composition in the pile turning process to enable the water content of the composition to be 52%, and repeating the pile turning for 1 time to obtain the fermentation fertilizer;
s4, mixing 50 parts of organic phosphate fertilizer, 1 part of potassium humate, 2 parts of trace element fertilizer, 0.6 part of ammonium sulfate, 1 part of potassium tripolyphosphate, 0.6 part of sodium metaphosphate and 2 parts of calcium superphosphate, and marking as an organic fertilizer mixture after uniform mixing;
s5, mixing the fermented fertilizer and the organic fertilizer mixture, and then adding 38 parts of moxa powder and 23 parts of microbial granulated fertilizer for mixing again to obtain the golden chrysanthemum nutrient fertilizer.
In the step S2, quicklime water is used to adjust the pH of the fermentation raw material composition.
The water content of the fermentation raw material composition in S2 was 55%.
The pile height in S3 is 1.2 m, and the pile width is 2 m.
In S4, the lumps of the above components need to be crushed and sieved before mixing until the difference in particle size of all components is small.
The preparation process of the moxa powder in the S5 comprises the following steps: cleaning fresh and intact folium Artemisiae Argyi, oven drying at 52 deg.C, pulverizing the dried folium Artemisiae Argyi in a pulverizer, and sieving to obtain powder.
The preparation process of the microbial granulated fertilizer in the S5 comprises the following steps:
a. mixing the crushed sawdust and straw scraps according to the ratio of 1:1, sieving by a 18-mesh sieve after mixing, and then sterilizing for 20min at the high temperature and the high pressure of 121 ℃ to obtain a fiber composition;
b. uniformly mixing the fiber composition with soil according to the proportion of 1:1, adding water, stirring to ensure that the water content is 12%, granulating, and air-drying to obtain air-dried granules;
c. uniformly spraying a gelatin solution with the weight ratio of 15% on the surfaces of the air-dried particles, sieving to obtain cylindrical particles with the diameter of 5 mm and the length of 1 mm, and air-drying the cylindrical particles again for later use;
d. inoculating the microbial strain into an R2A liquid culture medium by using an inoculating loop, culturing for 48h at 37 ℃ and 160R/min to prepare an inoculation liquid, then inoculating the inoculation liquid into an aeration fermentation device for aeration culture at room temperature, pumping the fermentation liquid into a high-speed tubular centrifuge by using a peristaltic pump after culturing for 4d, and centrifuging in a 20000R/min mode to obtain a precipitate, namely a strain cell;
e. and (3) mixing and pressing 10mL of strain cells measured by a plate counting method with the air-dried cylindrical particles in 320gc to obtain the microbial granular fertilizer.
The drying temperature in step b and step c was 38 ℃.
And d, the ventilation fermentation device in the step d consists of an air pump connecting filter, a 5-way pipeline and a fermentation bottle.
The golden chrysanthemum nutrient fertilizer is produced by any one of the preparation methods of the golden chrysanthemum nutrient fertilizer, and the golden chrysanthemum nutrient fertilizer mainly comprises the following raw materials: rice bran powder, mushroom residue, cassava residue, sawdust, borax, hairyvein agrimony, sanguisorba officinalis leaves, medical stone powder, a soil water-retaining agent, a fertilizer starter, an organic phosphate fertilizer, potassium humate, a trace element fertilizer, ammonium sulfate, potassium tripolyphosphate, sodium metaphosphate, calcium superphosphate, moxa powder and a microorganism granular fertilizer.
Example 3:
the preparation method of the Chrysanthemum morifolium nutritional fertilizer comprises the following preparation steps:
s1, mixing and stirring 25 parts of rice bran powder, 7 parts of mushroom residues, 12 parts of cassava residues, 13 parts of sawdust, 3 parts of borax, 6 parts of hairyvein agrimony, 5 parts of garden burnet leaves, 15 parts of medical stone powder, 15 parts of soil water-retaining agent and 0.2 part of fertilizer leavening agent to obtain a fermentation raw material composition;
s2, adding water into the fermentation raw material composition in the S1, adding water while stirring in the water adding process, and detecting the pH value of the fermentation raw material composition after stirring uniformly to enable the pH value to be 9;
s3, stacking the fermentation raw material composition treated by the S2, turning when the temperature of the stack reaches 60 ℃, spraying water to the surface of the partially dried composition again in the process of turning to ensure that the water content of the composition is 55%, and repeating the turning for 1 time to obtain the fermentation fertilizer;
s4, mixing 55 parts of organic phosphate fertilizer, 2 parts of potassium humate, 1 part of trace element fertilizer, 0.4 part of ammonium sulfate, 0.8 part of potassium tripolyphosphate, 0.7 part of sodium metaphosphate and 1 part of calcium superphosphate, and marking as an organic fertilizer mixture after uniformly mixing;
s5, mixing the fermented fertilizer and the organic fertilizer mixture, and then adding 40 parts of moxa powder and 20 parts of microbial granulated fertilizer for mixing again to obtain the golden chrysanthemum nutrient fertilizer.
In the step S2, quicklime water is used to adjust the pH of the fermentation raw material composition.
The water content of the fermentation material composition in S2 was 50%.
The pile height in S3 is 1.4 m, and the pile width is 2 m.
In S4, the lumps of the above components need to be crushed and sieved before mixing until the difference in particle size of all components is small.
The preparation process of the moxa powder in the S5 comprises the following steps: cleaning fresh and intact folium Artemisiae Argyi, oven drying at 50 deg.C, pulverizing the dried folium Artemisiae Argyi in a pulverizer, and sieving to obtain powder.
The preparation process of the microbial granulated fertilizer in the S5 comprises the following steps:
a. mixing the crushed sawdust and straw scraps according to the ratio of 1:1, sieving with a 18-mesh sieve after mixing is finished, and then sterilizing at the high temperature and the high pressure of 121 ℃ for 20min to obtain a fiber composition;
b. uniformly mixing the fiber composition with soil according to the ratio of 1:1, adding water, stirring to ensure that the water content is 13%, granulating, and air-drying to obtain air-dried granules;
c. uniformly spraying a gelatin solution with the weight ratio of 15% on the surfaces of the air-dried particles, sieving to obtain cylindrical particles with the diameter of 5 mm and the length of 1 mm, and air-drying the cylindrical particles again for later use;
d. inoculating the microbial strain into an R2A liquid culture medium by using an inoculating loop, culturing for 48h at 37 ℃ and 160R/min to prepare an inoculation liquid, then inoculating the inoculation liquid into an aeration fermentation device for aeration culture at room temperature, pumping the fermentation liquid into a high-speed tubular centrifuge by using a peristaltic pump after culturing for 4d, and centrifuging in a 20000R/min mode to obtain a precipitate, namely a strain cell;
e. and (3) mixing and pressing 10mL of strain cells measured by a plate counting method with the air-dried cylindrical particles in 320gc to obtain the microbial granular fertilizer.
The drying temperature in the step b and the step c is 40 ℃.
And d, the ventilation fermentation device in the step d consists of an air pump connecting filter, a 5-way pipeline and a fermentation bottle.
The golden chrysanthemum nutrient fertilizer is produced by any one of the preparation methods of the golden chrysanthemum nutrient fertilizer, and the main raw materials of the golden chrysanthemum nutrient fertilizer are as follows: rice bran powder, mushroom residue, cassava residue, sawdust, borax, hairyvein agrimony, sanguisorba officinalis leaves, medical stone powder, a soil water-retaining agent, a fertilizer starter, an organic phosphate fertilizer, potassium humate, a trace element fertilizer, ammonium sulfate, potassium tripolyphosphate, sodium metaphosphate, calcium superphosphate, moxa powder and a microorganism granular fertilizer.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in the process, method, article, or apparatus that comprises the element.
Performance testing
Taking a common fertilizer as a comparative example to carry out a comparative test, respectively carrying out golden chrysanthemum culture on the golden chrysanthemum nutrient fertilizer (noted as example 1-3) prepared in the comparative example and the golden chrysanthemum nutrient fertilizer prepared in the example 1-3, respectively pouring the fertilizers in the comparative example and the fertilizer in the example 1-3 into culture pots, respectively culturing the golden chrysanthemum under the same conditions and plant heights according to the same temperature, humidity and illumination degree, and finally extracting and detecting components contained in the cultured golden chrysanthemum, wherein the obtained detection results are recorded in the following table:
compared with the golden chrysanthemum cultured by the comparative fertilizer, the golden chrysanthemum nutrient fertilizer prepared by the invention can promote the production of the golden chrysanthemum and improve the content of total flavone components in the golden chrysanthemum, and the golden chrysanthemum nutrient fertilizer prepared by the invention is more suitable for culturing the golden chrysanthemum and has wider market prospect.
The above examples are only intended to illustrate the technical solution of the present invention, but not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.
Claims (10)
1. The preparation method of the Chrysanthemum morifolium nutritional fertilizer is characterized by comprising the following preparation steps:
s1, mixing and stirring 25-30 parts of rice bran powder, 4-10 parts of mushroom dregs, 8-12 parts of cassava dregs, 10-15 parts of sawdust, 2-4 parts of borax, 4-6 parts of hairyvein agrimony, 5-10 parts of ulmus pumila leaves, 10-15 parts of medical stone powder, 13-15 parts of soil water-retaining agent and 0.1-0.2 part of fertilizer leavening agent to obtain a fermentation raw material composition;
s2, adding water into the fermentation raw material composition in the S1, stirring while adding water, and detecting the pH value of the fermentation raw material composition after stirring uniformly to ensure that the pH value is 6-9;
s3, piling the fermentation raw material composition treated by the S2, turning when the pile temperature reaches 55-60 ℃, spraying water again on the surface of the partially dried composition in the pile turning process to ensure that the water content is 50-55%, and repeating the pile turning for 1-2 times to obtain the fermentation fertilizer;
s4, mixing 45-55 parts of organic phosphate fertilizer, 1-3 parts of potassium humate, 1-2 parts of trace element fertilizer, 0.4-0.6 part of ammonium sulfate, 0.8-1.5 parts of potassium tripolyphosphate, 0.5-0.7 part of sodium metaphosphate and 1-2 parts of calcium superphosphate, and marking as an organic fertilizer mixture after uniform mixing;
s5, mixing the fermented fertilizer and the organic fertilizer mixture, and then adding 35-40 parts of moxa powder and 20-25 parts of microbial granular fertilizer for mixing again to obtain the golden chrysanthemum nutrient fertilizer.
2. The method for preparing a Chrysanthemum morifolium nutritional fertilizer as claimed in claim 1, wherein in the step of adjusting the pH of the fermentation raw material composition in S2, quicklime water is used for pre-adjusting the pH value.
3. The preparation method of the Chrysanthemum morifolium nutritional fertilizer as claimed in claim 1, wherein the water content in the fermentation raw material composition in S2 is 50% -55%.
4. The method for preparing the Chrysanthemum morifolium nutritional fertilizer as claimed in claim 1, wherein the heap height in S3 is 1.2-1.5 m, and the heap width is 2 m.
5. The method for preparing a Jinju nutritional fertilizer according to claim 1, wherein the S4 is characterized in that before mixing, the lumps of the ingredients are crushed and sieved until the particle size difference of all the ingredients is small.
6. The preparation method of the Chrysanthemum morifolium nutritional fertilizer as claimed in claim 1, wherein the preparation process of the Artemisia argyi powder in S5 comprises the following steps: cleaning fresh and intact folium Artemisiae Argyi, oven drying at 50-55 deg.C, pulverizing the dried folium Artemisiae Argyi in a pulverizer, and sieving to obtain powder, i.e. folium Artemisiae Argyi powder.
7. The method for preparing the Chrysanthemum morifolium nutritional fertilizer as claimed in claim 1, wherein the preparation process of the microbial granulated fertilizer in S5 comprises the following steps:
a. mixing the crushed sawdust and straw scraps according to the ratio of 1:1, sieving by a 18-mesh sieve after mixing, and then sterilizing for 20min at the high temperature and the high pressure of 121 ℃ to obtain a fiber composition;
b. uniformly mixing the fiber composition with soil according to the proportion of 1:1, adding water, stirring to ensure that the water content is 12-15%, granulating, and air-drying to obtain air-dried granules;
c. uniformly spraying a gelatin solution with the weight ratio of 15% on the surfaces of the air-dried particles, sieving to obtain cylindrical particles with the diameter of 5 mm and the length of 1 mm, and air-drying the cylindrical particles again for later use;
d. inoculating the microbial strain into an R2A liquid culture medium by using an inoculating loop, culturing for 48h at 37 ℃ and 160R/min to prepare an inoculation liquid, then inoculating the inoculation liquid into an aeration fermentation device for aeration culture at room temperature, pumping the fermentation liquid into a high-speed tubular centrifuge by using a peristaltic pump after culturing for 4d, and centrifuging in a 20000R/min mode to obtain a precipitate, namely a strain cell;
e. and (3) mixing and pressing 10mL of strain cells measured by a plate counting method with the air-dried cylindrical particles in 320gc to obtain the microbial granular fertilizer.
8. The method for preparing the Chrysanthemum morifolium nutritional fertilizer as claimed in claim 7, wherein the drying temperature in the steps b and c is 36-40 ℃.
9. The method for preparing the Chrysanthemum morifolium nutritional fertilizer as claimed in claim 7, wherein the aeration and fermentation device in the step d consists of an air pump connected with a filter, a 5-way pipeline and a fermentation bottle.
10. The Chrysanthemum morifolium nutrient fertilizer as claimed in claim 1, which is produced by the preparation method of the Chrysanthemum morifolium nutrient fertilizer as claimed in any one of claims 1 to 9, and is characterized in that the Chrysanthemum morifolium nutrient fertilizer is prepared from the following main raw materials: rice bran powder, mushroom residue, cassava residue, sawdust, borax, hairyvein agrimony, sanguisorba officinalis leaves, medical stone powder, a soil water-retaining agent, a fertilizer starter, an organic phosphate fertilizer, potassium humate, a trace element fertilizer, ammonium sulfate, potassium tripolyphosphate, sodium metaphosphate, calcium superphosphate, moxa powder and a microorganism granular fertilizer.
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102199590A (en) * | 2011-04-02 | 2011-09-28 | 江苏省苏微微生物研究有限公司 | Method for preparing butyric acid bacteria powder by microencapsulated propagation culture and application |
| CN104326836A (en) * | 2014-11-21 | 2015-02-04 | 中国农业科学院农业资源与农业区划研究所 | Stalk granular inorganic microorganism fertilizer |
| CN106045750A (en) * | 2016-05-24 | 2016-10-26 | 安徽省康隆农业科技有限公司 | Planting fertilizer for Dendranthema morifolium and preparation method thereof |
| CN108235905A (en) * | 2018-01-23 | 2018-07-03 | 合肥雪立歆农业科技有限公司 | A kind of pot marigold cultural method of disease-resistant high yield |
| CN108314550A (en) * | 2018-04-25 | 2018-07-24 | 安徽省马道悠然电子商务有限公司 | A kind of chrysanthemum plantation fertilizer and preparation method thereof |
| CN109247205A (en) * | 2018-09-29 | 2019-01-22 | 安徽喜乐田园生态农业发展有限公司 | A kind of spun gold emperor chrysanthemum method for non-polluted cultivation |
| CN109874811A (en) * | 2019-03-08 | 2019-06-14 | 湖北中医药大学 | A kind of natural inhibitor and preparation method thereof effectively preventing chrysanthemum root rot |
-
2022
- 2022-03-15 CN CN202210266181.7A patent/CN114702346A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102199590A (en) * | 2011-04-02 | 2011-09-28 | 江苏省苏微微生物研究有限公司 | Method for preparing butyric acid bacteria powder by microencapsulated propagation culture and application |
| CN104326836A (en) * | 2014-11-21 | 2015-02-04 | 中国农业科学院农业资源与农业区划研究所 | Stalk granular inorganic microorganism fertilizer |
| CN106045750A (en) * | 2016-05-24 | 2016-10-26 | 安徽省康隆农业科技有限公司 | Planting fertilizer for Dendranthema morifolium and preparation method thereof |
| CN108235905A (en) * | 2018-01-23 | 2018-07-03 | 合肥雪立歆农业科技有限公司 | A kind of pot marigold cultural method of disease-resistant high yield |
| CN108314550A (en) * | 2018-04-25 | 2018-07-24 | 安徽省马道悠然电子商务有限公司 | A kind of chrysanthemum plantation fertilizer and preparation method thereof |
| CN109247205A (en) * | 2018-09-29 | 2019-01-22 | 安徽喜乐田园生态农业发展有限公司 | A kind of spun gold emperor chrysanthemum method for non-polluted cultivation |
| CN109874811A (en) * | 2019-03-08 | 2019-06-14 | 湖北中医药大学 | A kind of natural inhibitor and preparation method thereof effectively preventing chrysanthemum root rot |
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