CN114099397A - Mud-shaped mask and preparation method thereof - Google Patents
Mud-shaped mask and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
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Abstract
The invention discloses a mud-shaped mask and a preparation method thereof, and relates to the field of skin care products. The mud-like mask comprises tuckahoe powder, Indian grape seed oil, stem extract of dendrobium stem, leaf extract of aloe barbadensis, root extract of sophora flavescens ait, fruit extract of fructus lycii ningxia and chrysanthemum indicum extract. According to the invention, the natural plant powder poria cocos powder is used for replacing mineral powder such as kaolin, volcanic mud/rock and the like in the traditional mud mask, a skin care system with multiple effects and remarkable effects is formed through the synergistic effect of the functional components, and the problems of skin dryness, itching, tightness, redness and the like caused by dry cuticle due to strong adsorption capacity, skin moisture and oil content on the surface of the skin, and tight feeling of the skin after cleaning in the prior art are solved. The mud mask disclosed by the invention has good use feeling and skin feeling, and after the mud mask is used, the skin is moist and has no tightness, the moisture content of the skin is increased, the oil secretion of the skin is improved, and the mud mask has the effects of moisturizing, improving the elasticity of the skin and the like.
Description
Technical Field
The invention belongs to the field of skin care products, and particularly relates to a mud-shaped mask and a preparation method thereof.
Background
The mud-shaped mask is a direct-coating mask, is one of indispensable categories in masks, and the existing mud-shaped mask mainly adds a large amount of mineral powder such as kaolin, volcanic mud/rock and the like to enable a final product to have a mud-shaped appearance. The mineral powder has excellent adsorption function, and can absorb redundant oil of skin, so that the mineral powder achieves good deep cleaning effect. However, when the mineral powder paste mask is used, the mineral powder excessively adsorbs moisture and oil on the surface of the skin along with the volatilization of moisture, so that the cleaning force is strong, the excessive cleaning is easy to occur, and the problems of dry skin, tight feeling and the like after the use are caused. The skin is in a dry and water-deficient state, and the horny layer is dry, so that skin problems such as pruritus, tightness, redness and the like are easily caused, the skin is more easily stimulated, the probability of allergy is increased, and the skin aging is accelerated. Therefore, the problems of skin shortage, dryness, tightness and the like after the mineral powder mask is washed off are urgently needed to be solved.
In view of the above problems, it is very useful to develop a poultice mask which is excellent in feeling of use and skin feel, and which moisturizes the skin after use, increases the moisture content of the skin, improves the secretion of oil from the skin, and improves the elasticity of the skin.
Disclosure of Invention
Based on the defects of the prior art, the invention aims to provide the mud-shaped mask and the preparation method thereof, and the mud-shaped mask has good use feeling and skin feeling, is moist and free from tightness after being used, improves the moisture content of the skin, improves the secretion of skin oil, and has the effects of moisturizing, improving the skin elasticity and the like.
The technical problem to be solved by the invention is realized by the following technical scheme:
the invention firstly provides a mud-shaped facial mask.
According to the invention, the facial mask comprises poria cocos powder, Indian fruit oil, dendrobium stem extract, aloe barbadensis leaf extract, sophora flavescens root extract, fructus lycii extract, echinacea purpurea extract and conventional auxiliary materials in the field of cosmetics.
According to some specific embodiments of the present invention, the tuckahoe powder is used in an amount of 0.5wt% to 20.0wt%, for example, 0.5wt%, 1.0wt%, 1.5wt%, 2.0wt%, 2.5wt%, 3.0wt%, 3.5wt%, 4.0wt%, 4.5wt%, 5.0wt%, 5.5wt%, 6.0wt%, 6.5wt%, 7.0wt%, 7.5wt%, 8.0wt%, 8.5wt%, 9.0wt%, 9.5wt%, 10.0wt%, 10.5wt%, 11.0wt%, 11.5wt%, 12.0wt%, 12.5wt%, 13.0wt%, 13.5wt%, 14.0wt%, 14.5wt%, 15.0wt%, 15.5wt%, 16.0wt%, 16.5wt%, 17.0wt%, 17.5wt%, 18.0wt%, 18.5wt%, 19.0wt%, and 20% based on the total weight of the mask.
According to still other specific embodiments of the present invention, the tuckahoe powder is used in an amount of 0.5wt% to 15.0wt% based on the total weight of the mask.
According to the invention, the addition amount of the crabapple oil is 0.01-8.0 wt% based on the total weight of the mask.
According to the invention, the addition amount of the dendrobium stem extract is 0.01-5.0 wt% based on the total weight of the mask.
According to the invention, the aloe barbadensis leaf extract is added in an amount of 0.01-5.0 wt% based on the total weight of the mask.
According to the invention, the adding amount of the sophora flavescens root extract is 0.01-5.0 wt% based on the total weight of the mask.
According to the invention, the lycium barbarum fruit extract is added in an amount of 0.01-5.0 wt% based on the total weight of the mask.
According to the invention, the addition amount of the echinacea purpurea extract is 0.01-5.0 wt% based on the total weight of the mask.
According to some specific embodiments of the present invention, the crabapple oil is added in an amount of 0.05wt% to 5.0wt% based on the total weight of the mask.
According to some specific embodiments of the present invention, the dendrobium stem extract is added in an amount of 0.01wt% to 3.0wt% based on the total weight of the mask.
According to some specific embodiments of the present invention, the aloe vera leaf extract is added in an amount of 0.01wt% to 3.0wt% based on the total weight of the mask.
According to some specific embodiments of the present invention, the extract of sophora flavescens ait is added in an amount of 0.01wt% to 3.0wt% based on the total weight of the mask.
According to some specific embodiments of the present invention, the lycium barbarum fruit extract is added in an amount of 0.01wt% to 2.0wt% based on the total weight of the mask.
According to some specific embodiments of the present invention, the echinacea purpurea extract is added in an amount of 0.01wt% to 2.0wt% based on the total weight of the mask.
According to the invention, the conventional auxiliary materials in the facial mask comprise the conventional auxiliary materials in the field of cosmetics, such as polyhydric alcohol, chelating agent, thickening agent, emulsifier, fatty alcohol, emollient, skin conditioner, pH regulator, antioxidant, preservative and essence.
According to some specific embodiments of the present invention, the polyhydric alcohol in the mask pack includes one or more of glycerin, butylene glycol, propylene glycol, dipropylene glycol, and pentylene glycol.
According to some specific embodiments of the present invention, the chelating agent in the mask is a chelating agent commonly used in cosmetics, such as disodium EDTA, trisodium EDTA, tetrasodium EDTA, and sodium glucoheptonate.
According to some specific embodiments of the present invention, the thickener in the mask pack comprises one or more of xanthan gum, carrageenan, hydroxyethyl cellulose, sodium polyacrylate grafted starch, polyvinyl alcohol, carbomer, acrylic acid/C10-30 alkanol acrylate crosspolymer, and ammonium acryloyldimethyl taurate/VP copolymer.
According to some embodiments of the invention, the emulsifier in the mask comprises one or more of sucrose stearate, cetearyl glucoside, arachidyl glucoside, cocoyl glucoside, glyceryl stearate, PEG-100 stearate, ceteareth-20, methyl glucose sesquistearate.
According to some embodiments of the invention, the fatty alcohol in the mask comprises one or more of cetyl alcohol, arachidyl alcohol, behenyl alcohol, and cetearyl alcohol.
According to some specific embodiments of the present invention, the emollient comprises one or more of shea butter, jojoba esters, caprylic/capric triglyceride, isostearyl isostearate, isopropyl isostearate, and dimethicone.
According to some embodiments of the invention, the skin conditioning agent in the mask comprises one or more of tocopherol acetate, panthenol, and betaine.
According to some specific embodiments of the present invention, the pH adjusting agent in the mask pack includes one or more of citric acid and lactic acid.
According to some specific embodiments of the present invention, the antioxidant in the mask is pentaerythritol tetrakis (bis-tert-butyl hydroxyhydrocinnamate).
According to some specific embodiments of the present invention, the preservative in the mask is a preservative commonly used in cosmetics.
According to some specific embodiments of the present invention, the essence in the mask is a common essence in cosmetics.
According to the invention, the mask comprises the following raw materials in parts by weight:
phase A: 100 percent of water To, 3.0 To 15.0 percent of polyol, 0.01 To 0.5 percent of chelating agent, 0 To 3.0 percent of thickening agent and 0.5 To 20.0 percent of tuckahoe powder;
phase B: 0.5-5.0 wt% of emulsifier, 0.5-10.0 wt% of fatty alcohol, 0.5-15.0 wt% of emollient, 0.01-0.1 wt% of antioxidant and 0.01-8.0 wt% of crabapple oil;
and C phase: 0.5-6.0 wt% of skin conditioner, 0.01-5.0 wt% of stem extract of dendrobium nobile, 0.01-5.0 wt% of aloe barbadensis leaf extract, 0.01-5.0 wt% of root extract of sophora flavescens ait, 0.01-5.0 wt% of lycium barbarum fruit extract, 0.01-5.0 wt% of echinacea purpurea extract, 0-1.0wt% of preservative, 0-1.0wt% of essence and 0.01-0.5 wt% of pH regulator.
According to some specific embodiments of the invention, the facial mask comprises the following components in percentage by weight:
phase A: 100 percent of water To, 3.0 To 15.0 percent of butanediol, 0.01 To 0.5 percent of EDTA disodium, 0 To 3.0 percent of xanthan gum and 0.5 To 20.0 percent of tuckahoe powder;
phase B: 0.5wt% -5.0wt% of cetyl alcohol/coco glucoside/cetearyl alcohol, 0.5wt% -10.0wt% of cetearyl alcohol, 0.5wt% -5.0wt% of shea butter, 0.01wt% -10.0wt% of caprylic/capric triglyceride, 0.01wt% -0.1wt% of pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamic acid) ester, and 0.01wt% -8.0wt% of crabapple oil;
and C phase: 0.5 to 4.0 weight percent of panthenol, 0.01 to 5.0 weight percent of dendrobium stem extract, 0.01 to 5.0 weight percent of aloe barbadensis leaf extract, 0.01 to 5.0 weight percent of sophora flavescens root extract, 0.01 to 5.0 weight percent of lycium barbarum fruit extract, 0.01 to 5.0 weight percent of echinacea purpurea extract, 0 to 1.0 weight percent of phenoxyethanol/ethylhexylglycerin and 0.01 to 0.5 weight percent of citric acid.
According to still other specific embodiments of the present invention, the mask comprises the following raw materials in parts by weight:
phase A: 100 percent of water To, 3.0 To 10.0 percent of butanediol, 0.01 To 0.5 percent of EDTA disodium, 0 To 1.0 percent of xanthan gum and 0.5 To 15.0 percent of tuckahoe powder;
phase B: 0.5 to 5.0 weight percent of cetyl alcohol/coco glucoside/cetearyl alcohol, 0.5 to 6.0 weight percent of cetearyl alcohol, 0.5 to 5.0 weight percent of shea butter, 0.01 to 10.0 weight percent of caprylic/capric triglyceride, 0.01 to 0.05 weight percent of pentaerythritol tetra (bis-tert-butyl hydroxyhydrocinnamate), and 0.05 to 5.0 weight percent of crabapple oil;
and C phase: 0.5 to 2.0 weight percent of panthenol, 0.01 to 3.0 weight percent of dendrobium stem extract, 0.01 to 3.0 weight percent of aloe barbadensis leaf extract, 0.01 to 3.0 weight percent of sophora flavescens root extract, 0.01 to 2.0 weight percent of lycium barbarum fruit extract, 0.01 to 2.0 weight percent of echinacea purpurea extract, 0 to 0.8 weight percent of phenoxyethanol/ethylhexylglycerin and 0.01 to 0.38 weight percent of citric acid.
According to the present invention, the mask may be prepared using a method conventional in the art.
According to some embodiments of the present invention, the mask is prepared by including the steps of:
1) stirring the phase A until the phase A is completely dissolved, heating to 80-85 ℃, and preserving heat;
2) stirring phase B until completely dissolved, heating to 80-85 deg.C, and maintaining the temperature;
3) adding the phase B into the phase A raw material, homogenizing for 3-5 min, and preserving heat;
4) cooling to 45 deg.C under stirring, adding phase C, and stirring;
5) stirring and cooling, cooling to below 38 ℃, filtering and discharging.
According to the invention, the tuckahoe powder used by the mask is preferably tuckahoe broken wall powder.
According to the invention, the granularity of the poria cocos wall-broken powder is 10-60 microns, and preferably 20-50 microns.
The invention also provides a preparation method of the mud-shaped mask.
According to the invention, the mask comprises the following raw materials in parts by weight:
phase A: 100 percent of water To, 3.0 To 15.0 percent of polyol, 0.01 To 0.5 percent of chelating agent, 0 To 3.0 percent of thickening agent and 0.5 To 20.0 percent of tuckahoe powder;
phase B: 0.5-5.0 wt% of emulsifier, 0.5-10.0 wt% of fatty alcohol, 0.5wt% of emollient
15.0wt%, antioxidant 0.01wt% -0.1wt%, and crabapple oil 0.01wt% -8.0 wt%;
and C phase: 0.5-6.0 wt% of skin conditioner, 0.01-5.0 wt% of stem extract of dendrobium nobile, 0.01-5.0 wt% of aloe barbadensis leaf extract, 0.01-5.0 wt% of root extract of sophora flavescens ait, 0.01-5.0 wt% of lycium barbarum fruit extract, 0.01-5.0 wt% of echinacea purpurea extract, 0-1.0wt% of preservative, 0-1.0wt% of essence and 0.01-0.5 wt% of pH regulator.
According to some specific embodiments of the invention, the facial mask comprises the following components in percentage by weight:
phase A: 100 percent of water To, 3.0 To 15.0 percent of butanediol, 0.01 To 0.5 percent of EDTA disodium, 0 To 3.0 percent of xanthan gum and 0.5 To 20.0 percent of tuckahoe powder;
phase B: 0.5wt% -5.0wt% of cetyl alcohol/coco glucoside/cetearyl alcohol, 0.5wt% -10.0wt% of cetearyl alcohol, 0.5wt% -5.0wt% of shea butter, 0.01wt% -10.0wt% of caprylic/capric triglyceride, 0.01wt% -0.1wt% of pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamic acid) ester, and 0.01wt% -8.0wt% of crabapple oil;
and C phase: 0.5 to 4.0 weight percent of panthenol, 0.01 to 5.0 weight percent of dendrobium stem extract, 0.01 to 5.0 weight percent of aloe barbadensis leaf extract, 0.01 to 5.0 weight percent of sophora flavescens root extract, 0.01 to 5.0 weight percent of lycium barbarum fruit extract, 0.01 to 5.0 weight percent of echinacea purpurea extract, 0 to 1.0 weight percent of phenoxyethanol/ethylhexylglycerin and 0.01 to 0.5 weight percent of citric acid.
According to still other specific embodiments of the present invention, the mask comprises the following raw materials in parts by weight:
phase A: 100 percent of water To, 3.0 To 10.0 percent of butanediol, 0.01 To 0.5 percent of EDTA disodium, 0 To 1.0 percent of xanthan gum and 0.5 To 15.0 percent of tuckahoe powder;
phase B: 0.5 to 5.0 weight percent of cetyl alcohol/coco glucoside/cetearyl alcohol, 0.5 to 6.0 weight percent of cetearyl alcohol, 0.5 to 5.0 weight percent of shea butter, 0.01 to 10.0 weight percent of caprylic/capric triglyceride, 0.01 to 0.05 weight percent of pentaerythritol tetra (bis-tert-butyl hydroxyhydrocinnamate), and 0.05 to 5.0 weight percent of crabapple oil;
and C phase: 0.5 to 2.0 weight percent of panthenol, 0.01 to 3.0 weight percent of dendrobium stem extract, 0.01 to 3.0 weight percent of aloe barbadensis leaf extract, 0.01 to 3.0 weight percent of sophora flavescens root extract, 0.01 to 2.0 weight percent of lycium barbarum fruit extract, 0.01 to 2.0 weight percent of echinacea purpurea extract, 0 to 0.8 weight percent of phenoxyethanol/ethylhexylglycerin and 0.01 to 0.38 weight percent of citric acid.
According to the present invention, the preparation method of the mud-like mask comprises the steps of:
1) stirring the phase A until the phase A is completely dissolved, heating to 80-85 ℃, and preserving heat;
2) stirring phase B until completely dissolved, heating to 80-85 deg.C, and maintaining the temperature;
3) adding the phase B into the phase A raw material, homogenizing for 3-5 min, and preserving heat;
4) cooling to 45 deg.C under stirring, adding phase C, and stirring;
5) stirring and cooling, cooling to below 38 ℃, filtering and discharging.
According to the invention, the tuckahoe powder used by the mask is preferably tuckahoe broken wall powder.
According to the invention, the granularity of the poria cocos wall-broken powder is 10-60 microns, and preferably 20-50 microns.
The invention has the beneficial effects that:
(1) according to the invention, the natural plant powder poria cocos powder is adopted to replace mineral powder such as kaolin, volcanic mud/rock and the like in the traditional mud-like mask, and the mineral powder poria cocos powder is combined with the Indian fruit oil, the stem extract of dendrobium nobile, the leaf extract of aloe barbadensis, the root extract of sophora flavescens ait, the wolfberry fruit extract of Ningxia, the echinacea purpurea extract and conventional auxiliary materials in the field of cosmetics to prepare the mud-like mask, so that the problems of skin such as itching, tightness, flushing and the like due to the fact that the mineral powder mud-like mask in the prior art is high in adsorption capacity, adsorbs moisture and oil on the surface of the skin, and is dry and tight after cleaning are solved.
(2) The mud mask has good use feeling and skin feeling on the premise of keeping good spreadability and being easy to wash off, and the skin is moist and has no tight feeling after use.
(3) The facial mask disclosed by the invention has the effects of increasing the moisture content of the skin, improving the secretion of skin oil, moisturizing, improving the elasticity of the skin and the like.
Drawings
FIG. 1 is a graph of skin feel test results;
FIG. 2 is a graph of skin moisture content test results;
FIG. 3 is a graph of skin oil test results;
fig. 4 is a graph of skin elasticity test results.
Detailed Description
The invention is further illustrated below with reference to specific examples, to which, however, the invention is not restricted.
It should be appreciated by those skilled in the art that the present invention is not limited to the embodiments, and any changes and modifications to the present invention are within the scope of the present invention.
The experimental methods described in the following examples are all conventional methods unless otherwise specified; the experimental materials and reagents are commercially available, unless otherwise specified.
For convenience of explanation, the main raw materials described in the present invention are listed below, and are commercially available unless the preparation method thereof is specifically described. Specifically, the method comprises the following steps:
poria powder (commercially available) is neutral, contains triterpenes, polysaccharides and choline, fat, lecithin, potassium, magnesium, etc., and has effects in removing speckle, whitening skin, moistening skin, keeping moisture, delaying aging, promoting epithelial fibrocyte proliferation, and beautifying skin color.
The adducted fruit oil (purchased conventionally) contains a large amount of unsaturated fatty acids (omega-3, omega-6 and omega-9), can enhance the barrier function of epidermis, reduce the loss of water and improve the water retention rate of skin; it contains abundant vitamin E, has good antioxidant effect, and can eliminate free radicals and resist skin aging. In addition, it has the function of stabilizing cell membrane and can reduce the damage of ultraviolet ray to skin.
The dendrobium stem extract (purchased in the conventional market) has the effect of promoting the expression of aquaporin AQP3 in epidermal keratinocyte cells, can deeply supplement water, enhance the skin elasticity, and smoothen and tenderize the skin.
The aloe vera leaf extract (which is purchased from the market conventionally) contains certain amino acids, metal salts and the like which are the same as natural moisturizing factors contained in human skin, so that the moisturizing property of the aloe vera leaf extract is more prominent; the polysaccharide component rich in the chitosan has stronger permeability and is easier to be absorbed by the skin, thereby playing the role of nourishing and moistening the skin.
Matrine contained in the extract of the root of kuh-seng (purchased in the conventional market) has certain inhibition effect on various inflammatory factors and has good anti-inflammatory effect.
The Ningxia wolfberry fruit extract (purchased in the conventional market) is rich in nutrient substances such as carotene, vitamin A, calcium, iron and the like, can activate skin cells, promote cell metabolism, improve the skin water locking function and help the skin to keep full, smooth and fine.
Echinacea purpurea extract (purchased from general markets) is an excellent immune promoter and immune regulator, and polysaccharide components (such as 4-methoxy-glucurone-arabinose-xylan and the like) rich in the Echinacea purpurea extract have obvious humoral immunity enhancing function, are used for treating trauma, eczema and the like in folk, and have promoting effects on improving skin barrier function and enhancing skin autoimmunity.
Cetyl alcohol/coco glucoside/cetostearyl alcohol (commercially available in general) is an O/W type emulsifier of plant origin, has wide application range, and can emulsify various mineral oils, vegetable oils and silicone oils to obtain a stable emulsifying system; the consistency of the product can be adjusted by adjusting the addition amount of the thickener, and the system has better stability by a proper amount of the macromolecular thickener; has excellent spreading performance and good temperature resistance stability.
Butanediol, conventional commercial, CAS No.: 107-88-0.
Glycerol, conventional commercial, CAS No.: 56-81-5.
Disodium EDTA, conventional commercial, CAS No.: 6381-92-6.
Xanthan gum, conventional commercial, CAS No.: 11138-66-2.
Cetostearyl alcohol, conventionally available commercially, CAS No.: 67762-27-0.
Shea butter, conventionally commercially available, CAS No.: 91080-23-8.
Pentaerythritol tetrakis (bis-tert-butylhydroxyhydrocinnamate), conventional commercial available, CAS number: 6683-19-8.
Phenoxyethanol/ethylhexyl glycerin, conventionally commercially available, CAS No.: 901-44-0.
Panthenol, conventional commercial, CAS No.: 81-13-0.
Citric acid, conventional commercial, CAS No.: 77-92-9.
Examples 1 to 6
The components and proportions of the masks of examples 1-6 are shown in Table 1.
Table 1 mask components and proportions
The preparation process comprises the following steps:
1) stirring the phase A until the phase A is completely dissolved, heating to 80-85 ℃, and preserving heat;
2) stirring phase B until completely dissolved, heating to 80-85 deg.C, and maintaining the temperature;
3) adding the phase B into the phase A raw material, homogenizing for 3-5 min, and preserving heat;
4) cooling to 45 deg.C under stirring, adding phase C, and stirring;
5) stirring and cooling, cooling to below 38 ℃, filtering and discharging.
Comparative examples 1 to 4
Comparative examples 1 to 5 the components and proportions of the mask are shown in table 2.
TABLE 2 mask Components and proportions
The preparation process comprises the following steps:
1) stirring the phase A until the phase A is completely dissolved, heating to 80-85 ℃, and preserving heat;
2) stirring phase B until completely dissolved, heating to 80-85 deg.C, and maintaining the temperature;
3) adding the phase B into the phase A raw material, homogenizing for 3-5 min, and preserving heat;
4) cooling to 45 deg.C under stirring, adding phase C, and stirring;
5) stirring and cooling, cooling to below 38 ℃, filtering and discharging.
And (3) marketing competitive products: the main ingredients include water, kaolin, glycerol, caprylic/capric triglyceride, cetostearyl alcohol, glyceryl stearate, PEG-100 stearate, stearic acid, polydimethylsiloxane, phenoxyethanol, ethylhexylglycerol, etc.
(1) Comparison of feeling in use and after-use skin feeling
After the same time of application, using comparative examples 1-7, example 1 and the competitive products, the evaluation of using feeling and skin feeling after using is carried out, and the differences of the formulas of the comparative examples 1-7 and the example 1 are shown in the following table 3.
TABLE 3 Distinguishing of Components in the formulations of comparative examples 1-7 and example 1
Test samples: comparative examples 1-7, example 1 and commercial offerings;
36 volunteers (18-55 years old, male and female unlimited) were selected, comparative examples 1-7, example 1 and commercial offerings were applied to the cheeks of the volunteers, respectively, and then skin feel test was performed. After cleaning the face, a tester uses a mask spoon to pick up 7.5g of the test product, applies the test product on the face uniformly, scrapes off the mask with a mask spoon after 15min, then cleans the face with clear water, and washes the face clean. The tester subjectively scores according to the trial experience. The scoring standard is divided into 10 grades, the scoring indexes and the scoring standards are shown in table 4, and the skin feeling test result is shown in fig. 1.
TABLE 4 test products feel in use and skin feel score criteria after use
As can be seen from FIG. 1, compared with the commercially available competitive products, the product of example 1 is not easily dried when applied thickly, is easily washed off after use, has no tight feeling, and has good moistening and soft feeling; compared with the comparative examples 1 to 7, the product of example 1 is not easy to dry when being used in a thick application state, is easy to wash off, has no tight feeling, and obtains good skin feeling such as moist feeling and soft feeling after being used on the premise of keeping good spreadability. The experimental result shows that the mud-shaped facial mask utilizes the natural plant powder film tuckahoe powder to replace mineral powder, and has the synergistic effect with functional components such as the Indian fruit oil, the stem extract of dendrobium stem, the aloe barbadensis leaf extract, the root extract of sophora flavescens ait, the wolfberry fruit extract of Ningxia and the echinacea purpurea extract, so that the mud-shaped facial mask has good use feeling and skin feel on the premise of keeping good smearing property and being easy to wash.
(2) Skin moisture content, skin oil content, skin elasticity test
Test samples: comparative examples 1-7, example 1 and commercial offerings;
testing parts: two side cheeks;
testing an instrument: RBX-916 intelligent display skin tester;
testing time points: before use (initial value), washing off 0min, washing off 10min, washing off 20min and washing off 30 min.
The test method comprises the following steps: 36 volunteers (18-55 years old, male and female unlimited) were selected, comparative examples 1-7, example 1 and commercial contestants were applied to cheek test on both sides of the volunteers, respectively, and skin condition before and after use was tested. After cleaning the face, a tester uses a mask spoon to pick up 7.5g of the test product, applies the test product on the face uniformly, scrapes off the mask with a mask spoon after 15min, then cleans the face with clear water, and washes the face clean. An RBX-916 intelligent skin display tester is used for respectively testing the moisture content, the oil content and the skin elasticity index of the skin. The larger the test value, the higher the skin moisture content, the higher the oil content, and the better the skin elasticity, and the test average results are shown in tables 5-7 and fig. 2-4 below.
TABLE 5 results of skin moisture content test before and after use of comparative examples 1-7, example 1 and commercial racing
| Initial value | Washing for 0min | Washing for 10min | Washing for 20min | Washing for 30min | |
| Comparative example 1 | 24.25 | 30.75 | 29.25 | 26.00 | 26.25 |
| Comparative example 2 | 25.25 | 32.50 | 31.25 | 28.75 | 27.50 |
| Comparative example 3 | 24.50 | 31.25 | 29.75 | 27.75 | 26.50 |
| Comparative example 4 | 24.75 | 31.00 | 29.75 | 26.75 | 26.50 |
| Comparative example 5 | 25.00 | 29.75 | 28.25 | 26.50 | 25.75 |
| Comparative example 6 | 25.25 | 31.00 | 29.25 | 27.50 | 26.50 |
| Comparative example 7 | 24.75 | 30.25 | 28.75 | 26.75 | 26.00 |
| Example 1 | 25.00 | 32.75 | 31.75 | 29.50 | 28.25 |
| Market contest | 25.25 | 30.50 | 28.00 | 26.75 | 26.50 |
As can be seen from table 5 and fig. 2, the skin moisture content increased after the use of comparative examples 1 to 7, example 1 and the commercial offerings compared to the initial value (before use); the skin moisture content was higher using example 1 compared to comparative examples 1-7 and the commercial offerings at the same test time point. The mud mask has the effects of moisturizing.
TABLE 6 results of testing skin oil content before and after use of comparative examples 1-7, example 1 and commercial competitors
| Initial value | Washing for 0min | Washing for 10min | Washing for 20min | Washing for 30min | |
| Comparative example 1 | 48.00 | 29.75 | 32.25 | 39.00 | 44.25 |
| Comparative example 2 | 51.00 | 26.50 | 31.00 | 35.00 | 42.25 |
| Comparative example 3 | 49.50 | 29.25 | 30.75 | 36.75 | 41.50 |
| Comparative example 4 | 50.75 | 31.00 | 36.75 | 41.00 | 44.50 |
| Comparative example 5 | 51.00 | 32.75 | 37.50 | 44.50 | 49.00 |
| Comparative example 6 | 51.25 | 31.00 | 37.25 | 42.50 | 46.50 |
| Comparative example 7 | 49.75 | 30.25 | 38.75 | 42.75 | 47.00 |
| Example 1 | 51.00 | 23.75 | 29.75 | 33.50 | 39.00 |
| Market contest | 50.25 | 33.50 | 38.25 | 44.00 | 45.25 |
As can be seen from table 6 and fig. 3, the skin oil content was reduced after using comparative examples 1 to 7, example 1 and the commercial auction product, compared to the initial value (before use); at the same test time point, the skin oil content was significantly reduced using example 1 compared to comparative examples 1-7 and the commercial offerings.
As can be seen from the results of the experiments shown in tables 5-6 and fig. 2-3, the inventive mud-like mask uses the natural plant powder tuckahoe powder instead of mineral powder to interact with the crabapple oil, the stem extract of dendrobium nobile lindl, the leaf extract of aloe barbadensis, the root extract of sophora flavescens ait, the fruit extract of lycium barbarum and the chrysanthemum indicum extract, so as to form a skin care system with multiple and significant effects. The paste facial mask has effects of increasing skin moisture content, reducing skin oil content, moisturizing, and improving skin oil secretion.
TABLE 7 results of skin elasticity test before and after use of comparative examples 1-7, example 1 and commercial races
| Sample (I) | Initial value | Washing for 0min | Washing for 10min | Washing for 20min | Washing for 30min |
| Comparative example 1 | 42.25 | 50.25 | 46.75 | 45.75 | 44.00 |
| Comparative example 2 | 41.75 | 50.25 | 47.75 | 46.00 | 43.75 |
| Comparative example 3 | 43.75 | 53.25 | 50.75 | 48.75 | 46.50 |
| Comparative example 4 | 40.75 | 48.75 | 46.00 | 44.75 | 42.25 |
| Comparative example 5 | 42.50 | 49.25 | 46.75 | 45.75 | 43.75 |
| Comparative example 6 | 43.75 | 51.75 | 48.75 | 47.75 | 45.75 |
| Comparative example 7 | 42.50 | 50.75 | 47.00 | 46.50 | 44.25 |
| Example 1 | 44.75 | 56.25 | 53.75 | 51.75 | 47.75 |
| Market contest | 44.50 | 50.75 | 49.25 | 46.75 | 46.00 |
As can be seen from table 7 and fig. 4, the skin elasticity index increased after the use of comparative examples 1 to 7, example 1 and the commercial auction product, compared to the initial value (before use); the mask was seen to significantly improve skin elasticity using example 1, compared to comparative examples 1-7 and the commercial offers, when the skin elasticity index was higher at the same test time point.
In conclusion, the experimental result proves that the mud mask has good use feeling and skin feeling on the premise of keeping good spreadability and being easy to wash off, and the skin is moist and has no tight feeling after use; has effects of increasing skin moisture content, improving skin oil secretion, moisturizing, and improving skin elasticity.
Claims (10)
1. A pasty facial mask is characterized by comprising Poria cocos powder, Indian fruit oil, stem extract of dendrobium nobile lindl, leaf extract of aloe barbadensis, root extract of sophora flavescens ait, wolfberry fruit extract of Ningxia, echinacea purpurea extract and conventional auxiliary materials in the field of cosmetics.
2. The mask according to claim 1, wherein the tuckahoe powder is used in an amount of 0.5wt% to 20.0wt% based on the total weight of the mask; preferably, the usage amount of the tuckahoe powder is 0.5wt% -15.0 wt%.
3. The mask according to claim 1 or 2, wherein the crassula argentea oil is added in an amount of 0.01wt% to 8.0wt%, the stem extract of dendrobium nobile is added in an amount of 0.01wt% to 5.0wt%, the leaf extract of aloe barbadensis is added in an amount of 0.01wt% to 5.0wt%, the root extract of sophora flavescens ait is added in an amount of 0.01wt% to 5.0wt%, the fruit extract of lycium barbarum is added in an amount of 0.01wt% to 5.0wt%, and the extract of echinacea purpurea is added in an amount of 0.01wt% to 5.0wt%, based on the total weight of the mask.
4. The mask according to any one of claims 1 to 3, wherein the crabapple oil is added in an amount of 0.05wt% to 5.0wt%, the stem extract of Dendrobium nobile is added in an amount of 0.01wt% to 3.0wt%, the leaf extract of Aloe barbadensis is added in an amount of 0.01wt% to 3.0wt%, the root extract of Sophora flavescens is added in an amount of 0.01wt% to 3.0wt%, the fruit extract of Lycium barbarum is added in an amount of 0.01wt% to 2.0wt%, and the Echinacea purpurea is extract is added in an amount of 0.01wt% to 2.0wt%, based on the total weight of the mask.
5. The mask according to any one of claims 1 to 4, wherein the conventional adjuvants comprise polyols, chelating agents, thickeners, emulsifiers, fatty alcohols, emollients, skin conditioning agents, pH modifiers, antioxidants, preservatives, fragrances.
6. The mask pack according to any one of claims 1 to 5, wherein the polyhydric alcohol comprises one or more of glycerin, butylene glycol, propylene glycol, dipropylene glycol, pentylene glycol, and/or the chelating agent comprises one or more of disodium EDTA, trisodium EDTA, tetrasodium EDTA, and sodium glucoheptonate, and/or the thickener comprises one or more of xanthan gum, carrageenan, hydroxyethyl cellulose, sodium polyacrylate grafted starch, polyvinyl alcohol, carbomer, acrylic acid/C10-30 alkanol acrylate crosspolymer, ammonium acryloyldimethyl taurate/VP copolymer, and/or the emulsifier comprises sucrose stearate, cetearyl glucoside, arachidyl glucoside, cocoyl glucoside, glyceryl stearate, PEG-100 stearate, sodium glyceryl stearate, sodium glutamate, sodium stearate, sodium glutamate, sodium stearate, sodium glutamate, sodium stearate, sodium glutamate, sodium stearate, sodium glutamate, sodium stearate, sodium glutamate, sodium stearate, sodium glutamate, sodium stearate, sodium glutamate, sodium stearate, sodium glutamate, One or more of ceteareth-20 and methylglucamine sesquistearate, and/or the fatty alcohol comprises one or more of cetyl alcohol, arachidyl alcohol, behenyl alcohol and cetearyl alcohol, and/or the emollient comprises one or more of shea butter, jojoba ester, caprylic/capric triglyceride, isostearyl isostearate, isopropyl isostearate and polydimethylsiloxane, and/or the skin conditioning agent comprises one or more of tocopheryl acetate, panthenol and betaine, and/or the pH adjuster comprises one or more of citric acid and lactic acid, and/or the antioxidant is pentaerythritol tetrakis (di-tert-butyl hydroxyhydrocinnamate).
7. The mask according to any one of claims 1 to 6, wherein the mask comprises the following raw materials in parts by weight:
phase A: 100 percent of water To, 3.0 To 15.0 percent of polyol, 0.01 To 0.5 percent of chelating agent, 0 To 3.0 percent of thickening agent and 0.5 To 20.0 percent of tuckahoe powder;
phase B: 0.5-5.0 wt% of emulsifier, 0.5-10.0 wt% of fatty alcohol, 0.5-15.0 wt% of emollient, 0.01-0.1 wt% of antioxidant and 0.01-8.0 wt% of crabapple oil;
and C phase: 0.5-6.0 wt% of skin conditioner, 0.01-5.0 wt% of stem extract of dendrobium nobile, 0.01-5.0 wt% of aloe barbadensis leaf extract, 0.01-5.0 wt% of root extract of sophora flavescens ait, 0.01-5.0 wt% of lycium barbarum fruit extract, 0.01-5.0 wt% of echinacea purpurea extract, 0-1.0wt% of preservative, 0-1.0wt% of essence and 0.01-0.5 wt% of pH regulator.
8. The mud mask is characterized by comprising the following raw materials in parts by weight:
phase A: 100 percent of water To, 3.0 To 15.0 percent of butanediol, 0.01 To 0.5 percent of EDTA disodium, 0 To 3.0 percent of xanthan gum and 0.5 To 20.0 percent of tuckahoe powder;
phase B: 0.5wt% -5.0wt% of cetyl alcohol/coco glucoside/cetearyl alcohol, 0.5wt% -10.0wt% of cetearyl alcohol, 0.5wt% -5.0wt% of shea butter, 0.01wt% -10.0wt% of caprylic/capric triglyceride, 0.01wt% -0.1wt% of pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamic acid) ester, and 0.01wt% -8.0wt% of crabapple oil;
and C phase: 0.5 to 4.0 weight percent of panthenol, 0.01 to 5.0 weight percent of dendrobium stem extract, 0.01 to 5.0 weight percent of aloe barbadensis leaf extract, 0.01 to 5.0 weight percent of sophora flavescens root extract, 0.01 to 5.0 weight percent of lycium barbarum fruit extract, 0.01 to 5.0 weight percent of echinacea purpurea extract, 0 to 1.0 weight percent of phenoxyethanol/ethylhexylglycerin and 0.01 to 0.5 weight percent of citric acid.
9. The mud mask is characterized by comprising the following raw materials in parts by weight:
phase A: 100 percent of water To, 3.0 To 10.0 percent of butanediol, 0.01 To 0.5 percent of EDTA disodium, 0 To 1.0 percent of xanthan gum and 0.5 To 15 percent of tuckahoe powder;
phase B: 0.5 to 5.0 weight percent of cetyl alcohol/coco glucoside/cetearyl alcohol, 0.5 to 6.0 weight percent of cetearyl alcohol, 0.5 to 5.0 weight percent of shea butter, 0.01 to 10.0 weight percent of caprylic/capric triglyceride, 0.01 to 0.05 weight percent of pentaerythritol tetra (bis-tert-butyl hydroxyhydrocinnamate), and 0.05 to 5.0 weight percent of crabapple oil;
and C phase: 0.5 to 2.0 weight percent of panthenol, 0.01 to 3.0 weight percent of dendrobium stem extract, 0.01 to 3.0 weight percent of aloe barbadensis leaf extract, 0.01 to 3.0 weight percent of sophora flavescens root extract, 0.01 to 2.0 weight percent of lycium barbarum fruit extract, 0.01 to 2.0 weight percent of echinacea purpurea extract, 0 to 0.8 weight percent of phenoxyethanol/ethylhexylglycerin and 0.01 to 0.38 weight percent of citric acid.
10. A preparation method of a mud-like mask is characterized by comprising the following steps:
1) stirring the phase A until the phase A is completely dissolved, heating to 80-85 ℃, and preserving heat;
2) stirring phase B until completely dissolved, heating to 80-85 deg.C, and maintaining the temperature;
3) adding the phase B into the phase A raw material, homogenizing for 3-5 min, and preserving heat;
4) cooling to 45 deg.C under stirring, adding phase C, and stirring;
5) stirring and cooling, cooling to below 38 ℃, filtering and discharging.
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| CN115025009A (en) * | 2022-06-15 | 2022-09-09 | 羽楠(广州)化妆品有限公司 | Multifunctional Mannich root ice river mud space sand-shaped clean mud film and preparation method thereof |
| CN115192482A (en) * | 2022-07-13 | 2022-10-18 | 山西焦煤运城盐化集团有限责任公司 | Removable mask dry sheet taking black mud as main matrix and preparation method and application thereof |
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| CN107412132A (en) * | 2017-08-15 | 2017-12-01 | 广西民族大学 | A kind of moisturizing cleawhite pack mud formula |
| CN112057395A (en) * | 2020-08-22 | 2020-12-11 | 荣鼎(广东)生物科技有限公司 | Makeup removing mask containing plukenetia volubilis linneo |
| CN112569177A (en) * | 2021-02-05 | 2021-03-30 | 东晟源研究院(广州)有限公司 | Formula and preparation method of one-time emulsion luminescent mask paste |
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| CN107412132A (en) * | 2017-08-15 | 2017-12-01 | 广西民族大学 | A kind of moisturizing cleawhite pack mud formula |
| CN112057395A (en) * | 2020-08-22 | 2020-12-11 | 荣鼎(广东)生物科技有限公司 | Makeup removing mask containing plukenetia volubilis linneo |
| CN112569177A (en) * | 2021-02-05 | 2021-03-30 | 东晟源研究院(广州)有限公司 | Formula and preparation method of one-time emulsion luminescent mask paste |
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| CN115025009A (en) * | 2022-06-15 | 2022-09-09 | 羽楠(广州)化妆品有限公司 | Multifunctional Mannich root ice river mud space sand-shaped clean mud film and preparation method thereof |
| CN115192482A (en) * | 2022-07-13 | 2022-10-18 | 山西焦煤运城盐化集团有限责任公司 | Removable mask dry sheet taking black mud as main matrix and preparation method and application thereof |
| CN115192482B (en) * | 2022-07-13 | 2023-12-08 | 南风化工(运城)集团有限公司 | Removable mask dry sheet taking black mud as main matrix and preparation method and application thereof |
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