CN114073645A - A skin care composition containing mineral components and its preparation method - Google Patents

A skin care composition containing mineral components and its preparation method Download PDF

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CN114073645A
CN114073645A CN202010827723.4A CN202010827723A CN114073645A CN 114073645 A CN114073645 A CN 114073645A CN 202010827723 A CN202010827723 A CN 202010827723A CN 114073645 A CN114073645 A CN 114073645A
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欧阳聪
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Guangzhou Pugao Management Consulting Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/26Aluminium; Compounds thereof
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
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    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

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Abstract

The invention discloses a skin care composition containing mineral components and a preparation method thereof. The skin care composition comprises the following components: emulsifiers, thickeners, humectants, mineral mixtures, emollients, jojoba seed oil, phytosterol isostearate, hydrolyzed Adansonia simplicifolia extract, and water; the mineral mixture is a mixture of diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder. The skin care composition can effectively lock water and moisturize the skin, keep the skin tender and moist, and effectively improve the skin elasticity. Moreover, on the basis of moisture retention and moistening, the skin care product can promote the metabolism of the skin, promote the microcirculation of the skin, improve the glossiness of the skin, regulate the energy of the organism and enable the skin to become more brilliant and active. The preparation method of the invention can prepare the skin care composition containing mineral components with uniform texture dispersion and good stability by strictly controlling the reaction process and the adding sequence of the raw materials according to the characteristics of the raw material components.

Description

A skin care composition containing mineral components and its preparation method
Technical Field
The invention relates to the technical field of cosmetics, in particular to a skin care composition containing mineral components and a preparation method thereof.
Background
The skin cream is an important skin care product, has wide application in people, and is the skin care product which is most contacted by people and is the earliest. Under normal conditions, healthy skin can generate protective substances of natural moisturizing factors by itself, and the natural moisturizing factors contain components such as hyaluronic acid and amino acid and can moisturize the skin and maintain the skin elasticity. However, when exposed to a dry environment, the production of natural moisturizing factors is disrupted and the skin becomes water-deficient and dry. At the moment, the skin cream can form a protective barrier on the skin, prevent the water loss of the skin and lock water and keep moisture for the skin.
At present, the skin cream on the market has various types. However, these skin creams usually contain too many water-absorbing and moisture-retaining substances such as sodium hyaluronate to achieve strong water-absorbing and moisture-retaining effects, and after these skin creams are used, they can achieve the water-absorbing and moisture-retaining effects, but at the same time, they can also affect the production of natural skin moisture-retaining factors, so that the natural skin moisture-retaining performance is deteriorated, and finally, the dependence on the skin cream is formed.
Moreover, the efficacy of the traditional skin cream is still mainly limited to traditional moisturizing, and although effective moisturizing can be performed, the skin dryness cannot be fundamentally improved, and more positive improvement cannot be effectively brought to the skin. Along with the increasing requirements of people on the quality of life, people pay more and more attention to skin care, the requirements of people on skin care products are also increased, the selection of people on skin cream is not limited to the effects of moisturizing, but the new vitality of the skin can be more effectively revived on the basis of basic water replenishing and moisturizing.
Disclosure of Invention
The present invention is directed to providing a skin care composition containing mineral components that addresses the deficiencies or inadequacies of the prior art. The skin care composition containing mineral components can effectively lock water and moisturize the skin, keep the skin tender and moist, and effectively improve the skin elasticity. Moreover, on the basis of moisture retention and moistening, the skin care product can promote the metabolism of the skin, promote the microcirculation of the skin, improve the glossiness of the skin, regulate the energy of the organism and enable the skin to become more brilliant and active.
It is still another object of the present invention to provide a method for preparing the mineral component-containing skin care composition described above.
The purpose of the invention is realized by the following technical scheme.
A skin care composition containing mineral components comprises the following components in percentage by mass:
2.8-7.0% of emulsifier, 4.0-12.0% of thickener I, 0.01-0.2% of thickener II, 0.51-0.45% of humectant, 0.14-0.7% of mineral mixture, 2.0-9.0% of emollient, 1.0-5.0% of jojoba seed oil, 1.0-4.0% of phytosterol isostearate, 0.5-3.0% of hydrolyzed Adansonia dubia extract and the balance of water;
the mineral mixture is a mixture of diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder.
In a preferred embodiment, the diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder all have a particle size of less than 15 μm, more preferably less than 10 μm.
In a preferred embodiment, the pearl powder is black pearl powder.
In a preferred embodiment, the mineral mixture is diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder according to a mass ratio (0.5-1): (0.2-1): (0.1-1): (0.1-1): (0.2-1): (0.3-1).
In a more preferred embodiment, the mineral mixture is diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder, wherein the mass ratio of diamond powder to pearl powder to tourmaline powder is 8: 5: 4: 4: 5: 5 in a mixture.
In a preferred embodiment, the emulsifier comprises 0.8-2.0% of C12-20 alkyl glucoside and 2.0-5.0% of cetearyl alcohol by mass percentage of the composition.
In a preferred embodiment, the thickener I comprises myristyl myristate 2.0-8.0% and pentaerythritol distearate 2.0-4.0% by weight of the composition.
In a preferred embodiment, the thickener ii is selected from more than one of xanthan gum and carrageenan.
In a preferred embodiment, the humectant comprises 0.01-0.05% of sclerotium rolfsii gum and 0.5-4.0% of betaine by mass percentage of the composition.
In a preferred embodiment, the emollient comprises 1.0-5.0% shea butter and 1.0-4.0% hydrogenated polyisobutene by weight of the composition.
In a preferred embodiment, the composition further comprises, by mass percent of the composition: 0.2-1.0% of antioxidant, 0.02-0.12% of anti-allergic agent, 0.45-1.0% of preservative and 0.02-0.1% of essence;
the antioxidant is tocopherol acetate;
and/or, the anti-sensitivity agent is allantoin;
and/or, the preservative is selected from more than one of caprylyl glycol and ethylhexyl glycerin.
In a preferred embodiment, the mineral-containing skin care composition is a skin cream.
The method for preparing the mineral-containing skin care composition comprises the following steps:
s1, mixing the emulsifier, the thickener I, the emollient, the antioxidant, the jojoba seed oil and the phytosterol isostearate, stirring, heating to 80 ℃, and keeping the temperature for 10 minutes for later use;
s2, adding the humectant, the thickener II and the anti-allergy agent into water, stirring and mixing uniformly, heating to 80 ℃, and homogenizing at 2000r/min for 8 minutes; adding the components subjected to heat preservation in the step S1, homogenizing at 3000r/min for 10 minutes, and then cooling;
s3, cooling to 60 ℃, adding the mineral mixture, homogenizing at 2000r/min for 5 minutes, stirring uniformly, and continuously cooling;
s4, cooling to below 45 ℃, adding the hydrolyzed Palmaria championii extract, homogenizing and stirring uniformly, and continuing cooling;
s5, cooling to 42 ℃, adding the preservative and the essence, homogenizing at 2000r/min for 3 minutes, and uniformly stirring;
s6, discharging to obtain the skin care composition containing mineral ingredients.
Compared with the prior art, the invention has the following advantages and beneficial effects:
in the skin care composition, the moisturizing components including sclerotium rolfsii and betaine are combined, and the phytosterol isostearate, the jojoba seed oil and the hydrolyzed macaque tree extract are combined, so that the skin can be effectively moisturized, the skin is kept tender and moist, the skin metabolism is promoted, and the natural skin moisturizing barrier is repaired, so that the skin moisturizing problem is fundamentally solved, the natural skin moisturizing effect is not influenced, the skin elasticity is effectively improved, and the skin cell activity is recovered. Moreover, the micron-sized mineral components including diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder are added into the skin care composition, so that delicate balance of skin can be restored, microcirculation of the skin is promoted, and water-locking and moisture-keeping performances of the skin are further enhanced; meanwhile, the added micron-sized mineral components can effectively improve the skin glossiness, regulate the body energy, bring positive emotional cure, enable the skin to become more brilliant and active and enable users to have better spiritual appearance.
In addition, the skin care composition is provided in the form of emulsified cream for use, and has light, non-sticky, soft and smooth skin feeling, strong moistening feeling, safety and no stimulation.
The preparation method of the invention strictly controls the reaction process and the adding sequence of the raw materials according to the characteristics of the raw material components in the skin care composition containing the mineral components, and can prepare the skin care composition containing the mineral components with uniform texture dispersion and good stability.
Detailed Description
The technical solution of the present invention is further described in detail with reference to the following specific examples, but the scope and implementation of the present invention are not limited thereto. The present invention may be embodied in many different forms and is not limited to the embodiments described herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
Also, unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
The skin care composition containing mineral components comprises the following components in percentage by mass:
2.8-7.0% of emulsifier, 4.0-12.0% of thickener I, 0.01-0.2% of thickener II, 0.51-0.45% of humectant, 0.14-0.7% of mineral mixture, 2.0-9.0% of emollient, 1.0-5.0% of jojoba seed oil, 1.0-4.0% of phytosterol isostearate, 0.5-3.0% of hydrolyzed Adansonia dubia extract and the balance of water;
wherein the mineral mixture is a mixture of diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder.
In the skin care composition, the basic moisturizing component humectant is compounded, so that the basic requirements on moisture retention and moisture retention of skin can be effectively met, and the skin can be kept tender and moist. In addition, the compatible phytosterol isostearic acid ester is an ester of phytosterol and isostearic acid, has high permeability to skin, can keep moisture on the surface of the skin, reduce the percutaneous water loss rate of the skin, promote the metabolism of the skin and inhibit skin inflammation, and simultaneously has good spreadability, smooth and non-sticky skin feeling. The compatible jojoba seed oil can promote the generation of skin collagen and elastin, improve the skin elasticity, enable the skin to be smooth and compact, and fundamentally recover the moisturizing performance of the skin. The hydrolyzed Palmaria houtt extract is extracted from Palmaria houtt fruits, contains a large amount of trace elements, vitamins and nutrient elements, can increase skin elasticity, promote reproduction of skin cell tissues, soften skin, effectively improve skin color, revive skin activity and simultaneously has good antioxidant property.
In a preferred embodiment, the diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder all have a particle size of less than 15 μm, more preferably less than 10 μm.
More preferably, the particle size of the diamond powder, the pearl powder, the tourmaline powder, the nephrite powder, the ruby powder and the sapphire powder is 0.5-3.5 mu m.
In a preferred embodiment, the pearl powder is black pearl powder.
The micronized mineral stones are used as active ingredients to help restore the delicate balance of the skin. Wherein, the diamond powder can promote the regeneration of the skin by softening and exfoliating the skin and stay on the surface of the skin to generate reflected light and improve the transparency and luster of the skin; the pearl powder comprises aragonite, mineral substances, pearl protein, proteoglycan and amino acid derivatives, so that the pearl powder can supplement the mineral substances for skin, fill wrinkles and play the effects of resisting wrinkles and brightening the skin; tourmaline is a borosilicate crystal, can contain elements such as aluminum, iron, magnesium, sodium, lithium, potassium and the like, is called as a mixed gem, can prevent the invasion of the outside to the skin, can eliminate the toxin of the organism and can make the skin bright; the main component of the nephrite powder is calcium, magnesium and iron, and is rich in iron and/or magnesium, and the nephrite powder can be used for caring heart and liver, moistening hair, resisting inflammation, and eliminating skin scar; the ruby powder mainly contains alumina and trace element chromium, can regulate sebum through metabolizing lipid, remodel skin, and is beneficial to recovering the luster and brightness of the skin; the cyanobacteria powder mainly contains alumina and microelements titanium and/or iron, can directly act on the generation of collagen by catalyzing intercellular reaction, improves the smoothness of the skin and restores the skin compactness from the inside.
In a preferred embodiment, the mineral mixture is diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder according to a mass ratio (0.5-1): (0.2-1): (0.1-1): (0.1-1): (0.2-1): (0.3-1).
In a more preferred embodiment, the mineral mixture is diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder, wherein the mass ratio of diamond powder to pearl powder to tourmaline powder is 8: 5: 4: 4: 5: 5 in a mixture.
In a preferred embodiment, the emulsifier comprises 0.8-2.0% of C12-20 alkyl glucoside and 2.0-5.0% of cetearyl alcohol by mass percentage of the composition.
The C12-20 alkyl glucoside is matched with the cetearyl alcohol to use an emulsifying system, so that the skin care composition has excellent emulsifying and dispersing effects, and the texture of the skin care composition is more exquisite and uniform. Moreover, the emulsifying system formed by the C12-20 alkyl glucoside can be stored for a longer time in a larger temperature range, so that the skin care composition has a longer shelf life and meets the long-term use rule of skin care products; in addition, the C12-20 alkyl glucoside also has the moisturizing function, has good moisturizing and caring effects on the skin, and has soft, fine and non-irritant effects on the skin, so that the basic moisturizing effect of the whole skin care composition is more excellent.
In a preferred embodiment, the thickener I comprises myristyl myristate 2.0-8.0% and pentaerythritol distearate 2.0-4.0% by weight of the composition.
Myristyl myristate is a light waxy ester, and can give rich and soft skin feel to skin; the pentaerythritol distearate is a wax which is thickened strongly, can give smooth and soft skin feel to the skin and can bring about strong moistening effect. The thickening system formed by matching myristyl myristate and pentaerythritol distearate can effectively improve the viscosity of the skin care composition, achieves the texture effect of cream, is convenient to apply, and brings smooth, rich and moist skin feeling to the composition.
In a preferred embodiment, the thickener ii is selected from more than one of xanthan gum and carrageenan.
In a preferred embodiment, the humectant comprises 0.01-0.05% of sclerotium rolfsii gum and 0.5-4.0% of betaine by mass percentage of the composition.
The sclerotium rolfsii gum is a film-shaped scleroglucan produced by sclerotium rolfsii and used for preventing the dehydration process of hyphae of the sclerotium rolfsii, and the onion oil is helpful for the hyphae to enter host cells. The sclerotium rolfsii gum has excellent moisturizing property, can bring a moisturizing feeling to the skin, can activate the activity of cells in the body, improves the self-repairing capability of the skin, delays the skin aging and improves the roughness of the skin. And, a corresponding thickening effect can be contributed to the overall skin care composition system, which contributes to the formation of the gel texture of the overall skin care composition. Betaine can maintain intracellular and extracellular osmotic pressure to protect cell cutin, thereby enhancing skin moisture retention from the aspect of deep care of keratinocyte reinforced connection, providing good moisture retention, reducing skin wrinkle generation and increasing skin elasticity, and providing silky smooth skin feeling.
In a preferred embodiment, the emollient comprises 1.0-5.0% shea butter and 1.0-4.0% hydrogenated polyisobutene by weight of the composition.
The shea butter contains high-proportion fat accompaniments, particularly triterpene alcohol, vitamin E, vitamin A, allantoin and the like which are essential nutrients for growth, is rich in nutrition, and can prevent skin moisture loss, help to heal wounds and increase skin defense capacity and softness; meanwhile, the rich unsaturated fatty acid is easy to absorb, can enhance the moisture retention capacity of the skin, and can moisten dry and cutin-damaged skin. The hydrogenated polyisobutene has good spreadability, and ensures light skin feeling and non-greasy after-use skin feeling in the smearing process.
In a preferred embodiment, the composition further comprises, by mass percent of the composition: 0.2-1.0% of antioxidant, 0.02-0.12% of anti-allergic agent, 0.45-1.0% of preservative and 0.02-0.1% of essence.
The antioxidant is tocopherol acetate. The antioxidant can improve the antioxidant activity of skin cells, enhance the anti-aging effect of the skin cells and keep the skin tender.
And/or, the anti-sensitivity agent is allantoin. Allantoin can be combined with various substances to form a compound salt, has the effects of light shielding, sterilization, corrosion prevention, pain relief and oxidation resistance, and ensures that the composition is safe and has no stimulation. Moreover, the allantoin also has excellent effects of moistening skin, moisturizing and softening cutin, can promote the water absorption capacity of the skin, soften and soften the cutin, improve the hydrophilicity of cutin molecules, reduce the water evaporation of the skin and recover the natural water absorption capacity of the skin, so that the intercellular spaces are filled with water, and the skin achieves the state of moist and glossy; meanwhile, a lubricating film can be formed on the surface of the skin to seal water, so that the effect of moisturizing the skin is achieved. The anti-allergy relieving effect is realized, and the basic moisturizing effect of the skin care composition can be effectively enhanced.
And/or, the preservative is selected from more than one of caprylyl glycol and ethylhexyl glycerin. The adopted caprylyl glycol and ethylhexyl glycerin not only have the antiseptic effect, but also have the moisturizing effect, and can further enhance the basic moisturizing effect of the skin care composition.
The technical scheme of the invention is described in detail in the following with reference to specific examples, wherein the skin care composition containing mineral ingredients of the invention is prepared into cream form.
Examples 1 to 5
The raw material compositions of the mineral component-containing skin creams of examples 1 to 5 by mass are shown in table 1.
TABLE 1 raw material composition (100% by mass in total) of mineral-component-containing skin cream of examples 1 to 5
Figure BDA0002636832980000041
Figure BDA0002636832980000051
The skin cream containing mineral components of examples 1 to 5 were prepared by the following method, specifically including the steps of:
s1, mixing the emulsifier, the thickener I, the emollient, the tocopherol acetate, the jojoba seed oil and the phytosterol isostearate, stirring, heating to 80 ℃, and keeping the temperature for 10 minutes for later use;
s2, adding the humectant, the thickener II and the allantoin into water, stirring and mixing uniformly, heating to 80 ℃, and homogenizing at 2000r/min for 8 minutes; adding the components subjected to heat preservation in the step S1, homogenizing at 3000r/min for 10 minutes, and then cooling;
s3, cooling to 60 ℃, adding the mineral mixture, homogenizing at 2000r/min for 5 minutes, stirring uniformly, and continuously cooling;
s4, cooling to below 45 ℃, adding the hydrolyzed Palmaria championii extract, homogenizing and stirring uniformly, and continuing cooling;
s5, cooling to 42 ℃, adding the preservative and the essence, homogenizing at 2000r/min for 3 minutes, and uniformly stirring;
s6, discharging to obtain the skin cream containing mineral components.
Comparative example 1
In contrast to example 1, this comparative example contained no phytosterol isostearate.
Comparative example 2
In contrast to example 1, this comparative example contained no jojoba seed oil and no hydrolyzed macadamia extract.
Comparative example 3
In contrast to example 1, this comparative example does not contain jojoba seed oil and phytosterol isostearate.
Comparative example 4
In comparison with example 1, this comparative example did not contain a mineral mixture including diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder, and sapphire powder.
Skin creams of comparative examples 1 to 4 were prepared according to the preparation method of example 1.
The skin creams prepared in the examples 1-5 and the comparative examples 1-4 are subjected to physicochemical property tests of heat resistance (45 +/-2 ℃, 3 months, and room temperature recovery), cold resistance (-17 +/-2 ℃, 3 months, and room temperature recovery) and cold-heat cycle (24 hours and 5 cycles at 45 ℃, normal temperature and-17 ℃), and the results are not abnormal, so that the skin creams in the examples 1-5 and the comparative examples 1-4 have good physicochemical stability and good weather-proof quality guarantee effect.
1. Efficacy of use test
The skin creams of examples 1-5 and comparative examples 1-4 were tested for efficacy and a commercially available facial cream (1: (b))
Figure BDA0002636832980000052
Baiyou high skin penetration vitality cream) as a reference comparison.
(1) Patch test
Test samples: the skin creams of examples 1-5 and the skin creams of comparative examples 1-4.
The test population: 270 people, 20-35 years old, 180 women and 90 men, and has healthy skin and no allergic history of skin diseases. Randomly divided into 9 groups of 30 people each, and the proportion of male and female in each group is 1: 2, the skin creams of the test examples 1 to 5 and the comparative examples 1 to 4 were respectively applied in units of groups.
The test method comprises the following steps: according to the cosmetic safety technical specification (2015 edition) human skin patch test method, the skin cream of the examples 1-5 and the skin cream of the comparative examples 1-4 are subjected to patch tests, and the results are recorded according to the skin reaction grading standard.
Wherein, the skin reaction grading standard is as follows: negative reaction, grade 0. +/-., suspicious reaction, only weak erythema, grade 1. Positive reaction (erythema reaction), erythema, infiltration, edema, and pimple, grade 2. + + strong positive reaction (herpetic response), erythema, infiltration, edema, papules, herpes, response beyond the test area, grade 3. + + + +, very strong positive reaction (confluent herpes reaction), obvious erythema, severe infiltration, edema, confluent herpes, reaction beyond the test area, grade 4.
And (3) testing results: all the reactions are negative, and no adverse reaction cases occur.
(2) Improvement of skin conditions
According to the patch test results, the skin creams of examples 1-5 and comparative examples 1-4 were subjected to a direct use efficacy test.
Test samples: skin creams of examples 1-5, skin creams of comparative examples 1-4, and commercial face creams.
The test population: 50 people, female volunteers 25-35 years old, have healthy skin and no history of skin allergy. The skin cream of examples 1 to 5, the skin cream of comparative examples 1 to 4 and a commercial facial cream were used in groups of 5 persons each at random.
The test method comprises the following steps: after the face of the subject is washed by clean water, the corresponding test sample is smeared on the face for skin care and maintenance, and the skin care and maintenance are respectively carried out 1 time in the morning and at the evening every day and are continuously used for 1 month.
The facial skin conditions of the subjects before and after use, including skin moisture content, skin elasticity, skin wrinkles and skin glossiness, were measured, and the measurement results are shown in tables 2 to 5. Wherein, the facial skin Moisture is measured by a skin Moisture measuring instrument, and the test result is represented by a set humidity Measurement Value (MMV/%); the skin elasticity is measured by a skin elasticity tester (Cutomer dual MPA580), and the ratio Uv/Ue of the skin plastic part to the elastic part is taken as a value, and the smaller the ratio, the better the skin elasticity is; skin wrinkle condition was measured using Skin image analysis system (Skin Visiometer SV 600); the skin gloss was measured using a skin gloss meter and the lift rate was calculated.
(2-1) improvement of moisture content of facial skin
TABLE 2 improvement of moisture content of facial skin with skin creams of examples 1-5 and comparative examples 1-4
Figure BDA0002636832980000061
Figure BDA0002636832980000071
(2-2) improvement of facial skin elasticity
TABLE 3 improvement of facial skin elasticity of skin creams of examples 1 to 5 and comparative examples 1 to 4
Figure BDA0002636832980000072
Figure BDA0002636832980000081
(2-3) improvement of wrinkles on facial skin
TABLE 4 improvement of skin wrinkles by skin creams of examples 1 to 5 and comparative examples 1 to 4
Figure BDA0002636832980000082
Figure BDA0002636832980000091
Figure BDA0002636832980000101
(2-4) improvement of facial skin gloss
TABLE 5 improvement of gloss of facial skin by the skin creams of examples 1-5 and comparative examples 1-4
Figure BDA0002636832980000102
Figure BDA0002636832980000111
The test results in tables 2 to 5 show that the skin cream containing mineral components can effectively lock water and moisturize the skin, keep the skin tender and moist, improve the skin elasticity, reduce skin wrinkles, improve the skin glossiness and enable the skin to become more bright and active.
(3) Improvement in population tests
Test samples: skin creams of examples 1-5, skin creams of comparative examples 1-4, and commercial face creams.
The test population: 200 women, 20-35 years old, have healthy skin and no allergic history of skin diseases. 200 subjects were randomly divided into 10 groups of 20 persons, and the skin cream of examples 1 to 5, the skin cream of comparative examples 1 to 4, and a commercial facial cream were used for each group.
The test method comprises the following steps: after the face of the subject is washed by clean water, the corresponding test sample is smeared on the face for skin care and maintenance, and the skin care and maintenance are respectively carried out 1 time in the morning and at the evening every day and are continuously used for 1 month.
The evaluation grading standard statistics of the experience before and after the use of the subjects are carried out, and the statistical results are shown in table 6. Wherein the grading standard of the scores is as follows: 0 minute, the moisture content, elasticity, wrinkle condition and glossiness of the skin are not obviously improved; 1 minute, the moisture content and the wrinkle condition of the skin are improved, and the change of the elasticity and the glossiness of the skin is not obvious; 2 minutes, the moisture content and the wrinkle condition of the skin are obviously improved, and the elasticity and the glossiness of the skin are slightly improved; 3 minutes, the moisture content and the wrinkle condition of the skin are obviously improved, and the elasticity and the glossiness of the skin are obviously improved; 4 points, the moisture content, elasticity, wrinkle condition and glossiness of the skin are obviously improved.
TABLE 6 results of the human use test of the skin creams of examples 1-5 and comparative examples 1-4
Figure BDA0002636832980000112
From the test results in table 6, it can be seen that the skin creams of examples 1 to 5 have significant effects in moisturizing, improving skin elasticity, reducing skin wrinkles, and increasing skin glossiness, compared to the skin creams of comparative examples 1 to 4.
Various technical features of the above embodiments may be combined arbitrarily, and for the sake of brevity, all possible combinations of the technical features of the above embodiments are not described in this specification. However, as long as there is no contradiction between combinations of these technical features, the scope of the present specification should be considered as being described. Furthermore, the above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.

Claims (10)

1. A skin care composition containing mineral components is characterized by comprising the following components in percentage by mass:
2.8-7.0% of emulsifier, 4.0-12.0% of thickener I, 0.01-0.2% of thickener II, 0.51-0.45% of humectant, 0.14-0.7% of mineral mixture, 2.0-9.0% of emollient, 1.0-5.0% of jojoba seed oil, 1.0-4.0% of phytosterol isostearate, 0.5-3.0% of hydrolyzed Adansonia dubia extract and the balance of water;
the mineral mixture is a mixture of diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder.
2. The skin care composition containing mineral components according to claim 1, wherein the mineral mixture is diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder in a mass ratio of (0.5-1): (0.2-1): (0.1-1): (0.1-1): (0.2-1): (0.3-1).
3. The skin care composition containing mineral components according to claim 1, wherein the mineral mixture is diamond powder, pearl powder, tourmaline powder, nephrite powder, ruby powder and sapphire powder in a mass ratio of 8: 5: 4: 4: 5: 5 in a mixture.
4. The mineral-containing skin care composition according to claim 1, wherein the emulsifier comprises 0.8-2.0% of C12-20 alkyl glucoside and 2.0-5.0% of cetearyl alcohol by mass percentage of the composition.
5. The mineral-containing skin care composition as claimed in claim 1, wherein the thickener I comprises myristyl myristate 2.0-8.0% and pentaerythritol distearate 2.0-4.0% by mass.
6. The mineral-containing skin care composition according to claim 1, wherein the thickener ii is one or more selected from xanthan gum and carrageenan.
7. The mineral-containing skin care composition as claimed in claim 1, wherein the moisturizer comprises 0.01-0.05% of sclerotium rolfsii gum and 0.5-4.0% of betaine by mass percentage of the composition.
8. The mineral-containing skin care composition according to claim 1, wherein the emollient comprises 1.0-5.0% shea butter and 1.0-4.0% hydrogenated polyisobutene by weight of the composition.
9. The mineral component-containing skin care composition according to any one of claims 1 to 8, further comprising, in mass percent based on the composition: 0.2-1.0% of antioxidant, 0.02-0.12% of anti-allergic agent, 0.45-1.0% of preservative and 0.02-0.1% of essence;
the antioxidant is tocopherol acetate; and/or, the anti-sensitivity agent is allantoin; and/or, the preservative is selected from more than one of caprylyl glycol and ethylhexyl glycerin.
10. A method of making the mineral-containing skin care composition of claim 9, comprising the steps of:
s1, mixing the emulsifier, the thickener I, the emollient, the antioxidant, the jojoba seed oil and the phytosterol isostearate, stirring, heating to 80 ℃, and keeping the temperature for 10 minutes for later use;
s2, adding the humectant, the thickener II and the anti-allergy agent into water, stirring and mixing uniformly, heating to 80 ℃, and homogenizing at 2000r/min for 8 minutes; adding the components subjected to heat preservation in the step S1, homogenizing at 3000r/min for 10 minutes, and then cooling;
s3, cooling to 60 ℃, adding the mineral mixture, homogenizing at 2000r/min for 5 minutes, stirring uniformly, and continuously cooling;
s4, cooling to below 45 ℃, adding the hydrolyzed Palmaria championii extract, homogenizing and stirring uniformly, and continuing cooling;
s5, cooling to 42 ℃, adding the preservative and the essence, homogenizing at 2000r/min for 3 minutes, and uniformly stirring;
s6, discharging to obtain the skin care composition containing mineral ingredients.
CN202010827723.4A 2020-08-17 2020-08-17 A skin care composition containing mineral components and its preparation method Pending CN114073645A (en)

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