CN113925826B - Moisturizing and moisturizing composition, mask and preparation method and application thereof - Google Patents
Moisturizing and moisturizing composition, mask and preparation method and application thereof Download PDFInfo
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- CN113925826B CN113925826B CN202111455965.6A CN202111455965A CN113925826B CN 113925826 B CN113925826 B CN 113925826B CN 202111455965 A CN202111455965 A CN 202111455965A CN 113925826 B CN113925826 B CN 113925826B
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Classifications
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to a moisturizing composition, a mask, a preparation method and application thereof; firstly, mixing and heating water and auxiliary materials, and then performing low-temperature treatment to prepare a mixed solution A; the mixed solution A is added with the fermentation liquor of the plant and fungus composition, and the mixed solution B is prepared by stirring; the mixed solution B is subjected to low-temperature treatment and then added with plant composition extract essential oil for stirring treatment to obtain the moisturizing and moisturizing composition, and the moisturizing and moisturizing composition not only can penetrate into the bottom layer of skin, change the oil-water ratio of the surface of the skin, improve the absorption speed of the skin and strengthen the moisturizing effect of the skin, but also can change the problems that the active ingredients of the surface of the skin are easy to oxidize, the moisturizing effect is poor in persistence, the moisturizing effect can only stay on the stratum corneum, the preservative needs to be additionally added and the like.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a moisturizing composition, a mask, a preparation method and application thereof.
Background
Along with the improvement of the living standard of people, people pay more and more attention to the care and maintenance of the skin of the people. Healthy skin should be smooth, moist and elastic, depending mainly on the moisture content in the skin. In recent years, people work in an air-conditioning room or a dry environment for a long time, and the problem of skin water shortage is increasingly remarkable, so that the skin of people is drier and drier, and the skin aging speed is accelerated. The past grease skin care can not meet the requirements of modern people on moisturizing cosmetics, and more people like natural raw material extracts with good moisturizing performance and high safety performance.
Most of the moisturizing masks in the current market are added with industrially produced polyalcohol substances as moisturizers, and commonly used polyalcohol substances include glycerin, propylene glycol, butanediol, vaseline and the like. The moisturizing agents can control the exchange of moisture with the surrounding air to maintain the skin in an equilibrium state higher than the normal moisture content, play a role in relieving skin dryness, and can not fundamentally solve the problem of water shortage of the skin, and also can bring bad skin feel such as greasiness, and the moisturizing effect is reduced when the relative humidity of the environment is too low, and the moisturizing effect for a long time is also not ideal.
The skin moisturizing agent has the advantages of moisture absorption, capability of adjusting the acid-base value of the skin surface, excellent skin affinity, and meanwhile, the skin moisturizing agent has the effects of relieving the damage of external substances to the skin, delaying aging, conditioning the skin and the like, and can help the skin to restore to the healthy state of moisture elasticity. However, the purely natural moisturizing factors have the defects of difficult preservation, easy microbial infection and quite common self-rancidity, so that an additional preservative is required to be added.
The plant extract prepared by the traditional process has the advantage that the efficacy of the raw materials is difficult to be expected due to the limitations of extraction solvents, processes, preparation methods and the like. The fermentation technology can extract smaller molecular active nutrient substances from natural plant resources, enhance the efficacy, reduce the toxicity, improve the effectiveness and the safety of raw material use, and is easier to absorb, so that the fermentation technology has good application prospect in the application of natural plants and fungus components.
Disclosure of Invention
The invention provides a moisturizing composition, a mask and a preparation method and application thereof, and aims to solve the technical problems that in the prior art, the moisturizing effect of the mask is poor, active ingredients are easy to oxidize, the moisturizing effect is poor in persistence, the moisturizing effect can only stay on a stratum corneum, and the skin dryness cannot be fundamentally solved due to the additional addition of a preservative.
The technical scheme adopted by the invention is as follows:
the invention provides a preparation method of a moisturizing composition, which comprises the following steps:
1) Mixing 45-65 parts by weight of water and 15-25 parts by weight of auxiliary materials, and heating until the auxiliary materials are completely dissolved to obtain a mixed solution A;
2) Cooling the mixed solution A, adding 20-40 parts by weight of plant and fungus composition fermentation liquor, and uniformly stirring to obtain a mixed solution B;
3) And cooling the mixed solution B, adding 2-10 parts by weight of plant composition to extract essential oil, and uniformly stirring to obtain the moisturizing and moisturizing composition.
Wherein the auxiliary materials comprise glycerol, butanediol, xanthan gum, trehalose and hydrogenated lecithin; the dosage ratio of glycerin, butanediol, xanthan gum, trehalose and hydrogenated lecithin is 5-15 g: 2-10 g:0.5 g to 5g:0.5 g to 10g:0.1 g to 1g.
The preparation method of the plant composition extracted essential oil comprises the following steps:
s1: taking 20 g-50 g of holy basil, 15 g-45 g of seville orange flower and 20 g-50 g of magnolia officinalis flower, drying, crushing into 50-100 mesh particles, and placing the particles into a supercritical extraction device for extraction, wherein the extraction conditions are as follows: extracting at the pressure of 25MPa and the extracting temperature of 40-50 ℃ for 2-5 h, and collecting volatile oil after extraction;
s2: adding active carbon into the volatile oil, filtering, extracting the filtered solution, precipitating the filtered solution, centrifuging, and collecting supernatant to obtain plant composition extract essential oil.
The preparation method of the plant and fungus composition fermentation broth comprises the following steps:
s1: taking 10g to 20g of grifola frondosa, 20g to 50g of snakegourd fruit, 20g to 30g of semen Benincasae, 5g to 30g of peach kernel and 5g to 20g of poria cocos, crushing into 50-100 mesh particles to form a plant and fungus composition, putting the plant and fungus composition into a fermentation tank, and adding 6-10 times of water for mixing; then heating the fermentation tank to 105 ℃, preserving heat for 15 minutes, and then cooling to 25-40 ℃; inoculating lactobacillus acidophilus bacterial liquid in a fermentation tank, closing the fermentation tank, introducing sterile nitrogen, and performing anaerobic fermentation at 20-45 ℃ for 3-5 days to obtain fermentation liquid;
s2: filtering the obtained fermentation liquor to obtain a filtered solution, sterilizing the filtered solution at 105-130 ℃ for 30-60 minutes, centrifuging the sterilized solution, discarding the precipitate, and collecting the supernatant to obtain the fermentation liquor of the plant and fungus composition.
Specifically, in step S1, the ratio of the amount of the plant-fungus composition to the amount of the lactobacillus acidophilus liquid to the amount of water is 10g:3g:100mL.
Specifically, in step S2, the filtered solution is sterilized at 121 ℃ for 30 minutes.
Further, in the step 1) of the preparation method of the moisturizing and hydrating composition, the auxiliary materials can be rapidly dissolved when the heating temperature is 75-85 ℃.
In step 2) of the preparation method of the moisturizing and hydrating composition, the mixed solution A is cooled at the temperature of 45-65 ℃, the stirring speed is 5000rpm, the stirring time is 10-30 minutes, the mixing of the fermentation liquor and the auxiliary material solution can be accelerated, and the lower stability is beneficial to the retention of active ingredients of the fermentation liquor.
In the step (3) of the preparation method of the moisturizing and hydrating composition, the mixed solution B is cooled at the temperature of 30-45 ℃ and the stirring speed is 1500rpm, and the stirring time is 5-15 minutes, so that the volatile oil, the fermentation broth and the mixed solution of the auxiliary materials can be uniformly mixed, and the layering or emulsification of the volatile oil is avoided.
In the formula, the holy basil is dried overground whole herb of herba Lysimachiae Foenum-gracilis (Lysimachia foenumgraetum Hance) of Primulaceae (Primalalaeae) genus Phyllostachys. The holy basil is a traditional spice with strong and durable fragrance, is a Chinese medicinal material capable of relieving exterior syndrome, relieving pain, promoting qi circulation, expelling ascarid and the like, and also has the functions of cleaning face and the like, such as Jinhe xiang Jia and facial fat and bath beans recorded in Ben Cao gang mu. Modern researches have found that the volatile oil of herba Lysimachiae Foenumgraeci has antioxidant effect and is related to the effects of relieving exterior syndrome and removing dirt.
In the present formulation, the substituted flower is a dried flower bud of Citrus aurantium L.var. The chemical components of the substituted flowers are various and mainly comprise flavonoid, alkaloids, volatile oil and the like. Has antiinflammatory and antioxidant effects.
In the formula, the magnolia flower is dried flower buds of magnolia Magnolia officinalis Red. Et Wils. Or magnolia affavellana Magnolia officinalis Red. Et Wils. Var. Biloba Red. Et Wils. Of magnoliaceae. The volatile oil of flos Magnoliae comprises terpenes, alcohols, and ketone ethers, and has antibacterial and antiinflammatory effects.
In the formula, grifola frondosa (Grifola frondosa) is a fungus of Polyporaceae, and the rich Grifola frondosa polysaccharide has activities of antioxidation, anti-radiation, antibiosis and the like, and can provide abundant micromolecular nutrients for skin cells. Therefore, the composition has the effects of protecting skin cells in the aspects of resisting oxidization, relieving radiation injury and the like.
In the formula, the fructus Trichosanthis is dried mature fruit of Trichosanthes kirilowii Trichosanthes kirilowii maxim or Trichosanthes kirilowii Trichosanthes rosthornii Harm belonging to Cucurbitaceae. The chemical components of fructus Trichosanthis mainly triterpenes, flavonoids, phytosterols, fatty acids, amino acids, proteins, alkaloids, polysaccharides, etc. The trichosanthes triterpenoids have the effects of anti-inflammatory, antibacterial, antioxidation and the like, and the trichosanthes flavone has the effects of protecting vascular endothelial injury and the like, is favorable for changing the complexion, is rich in fatty acid, amino acid and the like, and can provide nutrition for skin and increase the water retention capacity.
In the formula, the wax gourd seeds are dry seeds of a wax gourd Benincasa hispida (thunder.) Cogn. The main chemical components include saponin, urea decomposing enzyme, fatty oil, amino acids, mannitol, beta-sitosterol, mineral matter, vitamin, etc. Mainly has the functions of antibiosis, antioxidation, immunity promotion and the like. Meanwhile, the Chinese medicine records that the semen Benincasae has the effects of benefiting water channels and eliminating edema, and can promote the absorption of moisture and the like.
In the formulation, the peach seed is a dried mature seed of Prunus persica (L.) Batsch or Prunus davidiana (Carr.) Franch. Mainly contains flavone and various organic compounds such as glycosides, steroids, terpenes, phenolic acids, carotenoids, gibberellins, saccharides and the like, and various nutritional components such as fatty acid, amino acid and the like. The peach kernel has the effect of promoting blood circulation from ancient times, can promote blood circulation, increase the supply of facial cell nutrition, moisture and the like, and meanwhile, the peach kernel is smooth in nature and rich in nutrient substances, so that the peach kernel is beneficial to moisture retention and water retention.
In the formula, the Poria cocos is dry sclerotium of Wolf, a fungus of Polyporaceae, poria cocos (Schw.). The chemical components mainly comprise polysaccharides, triterpenes, sterols, amino acids, fatty acids, etc., and have the effects of anti-inflammatory, antioxidant, antibacterial, antiallergic, etc. The traditional Chinese medicine considers that the poria cocos is light in smell and oozing, has ascending nature, generates body fluid, opens striae and striae, and can promote skin cells to absorb substances such as moisture, nutrition and the like.
The beneficial effects of the invention are as follows:
the plant composition of the invention extracts essential oil by supercritical carbon dioxide extraction of holy basil, seville orange flower and magnolia officinalis flower, so as to obtain volatile oil, the antibacterial effect of the volatile oil can effectively control the microbial quantity, maintain the balance of the microbial quantity on the skin surface, and the obtained volatile oil is rich in natural antioxidants, can remove free radicals, resist oxidation and aging, can improve the skin texture, and simultaneously can improve the anti-inflammatory and antiallergic effects.
The fermentation liquor of the plant and fungus composition is prepared by fermenting plants such as grifola frondosa, snakegourd fruit, semen Benincasae, peach kernel, poria cocos and the like and fungus by lactobacillus acidophilus, and can lead to the decomposition or bioconversion of a compound in the plants and the fungus, convert a substrate into components with multiple functions, and adjust the characteristics of the products or change the content of certain bioactive substances; meanwhile, the extraction effect of active ingredients in the microbial transformed plants and fungi is mild, natural active ingredients of the plants and fungi can be reserved to the greatest extent, toxicity is reduced, new active ingredients are generated, multiple extracellular enzymes such as cellulase, protease, pectase and the like can be generated in the metabolic process of the microorganisms to decompose cell walls of the plants and fungi cells, the cells are broken, the bioactive ingredients are released, macromolecular substances can be converted into micromolecular active substances such as amino acids which are easier to absorb by skin, the microbial fermentation products are rich in multiple active enzymes, the antioxidant and whitening capabilities are better, the active ingredients can replace the addition of preservatives, and the situation that the existing products with moisturizing and moisturizing functions need additional preservatives in the market can be effectively avoided.
The main components of the fermentation liquor of the plant and fungus composition disclosed by the invention, which are obviously changed before and after fermentation, are sugar, amino acid, short-chain fatty acid, total phenol and the like, and the biological macromolecular polysaccharide in the fermentation liquor is a polyhydroxy polymer, the polar groups of the biological macromolecular polysaccharide can form hydrogen bonds with water molecules to combine with water, and meanwhile, the polysaccharide can form a uniform film on the surface of skin to prevent the percutaneous loss of water. The content of small molecular humectant such as urea, mannose, amino acid, fatty acid and the like is obviously improved, and the small molecules can permeate into deep skin and improve the hydration capability of cells.
The plant extracts, the fungus extracts and the fermentation liquor with the effects of moisturizing, antioxidation, antibiosis, antiallergic and the like are combined, the effects are coordinated with each other, the water locking and water making capacity of skin can be enhanced, the skin is helped to recover the moisture elasticity, the blood circulation and metabolism are promoted, the skin defense capacity is enhanced, the skin allergy phenomenon is resisted, the skin health is maintained, and meanwhile, the skin caring effect is also achieved.
Therefore, the moisturizing and moisturizing composition obtained by adding the plant composition to extract essential oil and the plant and fungus composition fermentation liquor can not only go deep into the bottom layer of skin, change the oil-water ratio of the surface of the skin, improve the absorption speed of the skin and strengthen the moisturizing effect of the skin, but also change the problems that the active ingredients of the skin are easy to oxidize, the moisturizing effect is poor in persistence, the moisturizing effect can only stay in the stratum corneum, an additional preservative is needed and the like, and can fundamentally solve the technical problem of skin dryness.
The invention also provides a moisturizing and hydrating composition prepared by the preparation method of the moisturizing and hydrating composition.
The invention also provides a facial mask prepared from the moisturizing composition.
The invention further provides application of the moisturizing composition in preparing a mask.
Detailed Description
The principles and features of the present invention are described below with examples given for the purpose of illustration only and are not intended to limit the scope of the invention.
1. Examples
Example 1: the plant composition extracting essential oil (I) and its preparation process includes the following steps:
s1: taking 50g of holy basil, 30g of seville orange flower and 20g of magnolia officinalis, drying to obtain dried raw materials, crushing the dried raw materials, and filtering by a 50-100-mesh filter screen;
s2: placing the raw materials prepared in the step S1 into supercritical CO 2 Extracting in an extraction device;
the extraction conditions are as follows: extracting at 50deg.C under 25MPa for 2 hr, and collecting volatile oil;
s3: adding 5% of active carbon into the obtained volatile oil, stirring for 4-8 hours at 100rpm, filtering, and extracting the filtered solution;
and (3) standing the filtered solution at the temperature of between-4 and 10 ℃ for 12 to 24 hours, centrifuging the solution, and collecting supernatant after centrifuging to obtain the plant composition extracted essential oil.
Example 2: the plant composition extracting essential oil (II) and its preparation process includes the following steps:
the difference from example 1 is that in step S1, the raw materials are in parts by weight: 35g of holy basil, 15g of substituted flowers and 50g of magnolia officinalis flowers;
in step S2, the extraction conditions thereof are set as follows: the extraction pressure is 25MPa, the extraction temperature is 40 ℃, and the extraction time is 3 hours.
Example 3: the plant composition extracting essential oil (III) and its preparation process includes the following steps:
the difference from example 1 is that in step S1, the raw materials are in parts by weight: 20g of holy basil, 45g of substituted flowers and 35g of magnolia officinalis;
in step S2, the extraction conditions thereof are set as follows: the extraction pressure is 25MPa, the extraction temperature is 40 ℃, and the extraction time is 5 hours.
Example 4: a fermentation broth (I) of a plant and fungus composition and a preparation method thereof comprise the following steps:
s1: taking 10g of grifola frondosa, 40g of snakegourd fruit, 30g of semen Benincasae, 10g of peach kernel and 10g of poria cocos, crushing the raw materials, and filtering by a 50-100-mesh filter screen to form a plant and fungus composition;
the dosage ratio of the plant and fungus composition to lactobacillus acidophilus to water is 10g:3g:100mL;
the lactobacillus acidophilus is activated by adopting sterile water to obtain lactobacillus acidophilus bacterial liquid;
s2: putting the filtered plant and fungus composition in the step S1 into a fermentation tank, and adding 6-8 times of water for mixing;
then the fermentation conditions are set as follows: heating the fermentation tank to 105 ℃, preserving heat for 15 minutes, and cooling to 37 ℃;
inoculating lactobacillus acidophilus bacterial liquid in a fermentation tank, closing the fermentation tank, introducing sterile nitrogen, performing anaerobic fermentation for 3 days, and controlling the fermentation temperature at 35-39 ℃ to obtain fermentation liquid;
s3: filtering the obtained fermentation liquor to obtain a filtered solution, sterilizing the filtered solution at 121 ℃ for 30 minutes, centrifuging the sterilized solution at 4000r/min for 15 minutes, discarding the precipitate, and collecting the supernatant to obtain the fermentation liquor of the plant and fungus composition.
Example 5: a fermentation broth (II) of a plant and fungus composition and a preparation method thereof comprise the following steps:
the difference from example 4 is that in step S1, the weight parts of the plant and fungus composition are: 20g of grifola frondosa, 50g of snakegourd fruit, 20g of semen Benincasae, 5g of peach seed and 5g of poria cocos;
in step S2, the fermentation conditions thereof are set as follows: heating the fermentation tank to 105 ℃, preserving heat for 15 minutes, and cooling to 31 ℃; anaerobic fermentation is carried out for 3 days, and the fermentation temperature is controlled between 28 ℃ and 34 ℃.
Example 6: a fermentation broth (III) of a plant and fungus composition and a preparation method thereof comprise the following steps:
the difference from example 4 is that in step S1, the weight parts of the plant and fungus composition are:
10g of grifola frondosa, 20g of snakegourd fruit, 20g of semen Benincasae, 30g of peach seed and 20g of poria cocos;
in step S2, the fermentation conditions thereof are set as follows: heating the fermentation tank to 105 ℃, preserving heat for 15 minutes, and cooling to 31 ℃; anaerobic fermentation is carried out for 5 days, and the fermentation temperature is controlled between 28 ℃ and 34 ℃.
EXAMPLE 7,
The moisturizing composition of the embodiment comprises the following raw materials in table 1.
TABLE 1
A method for preparing a moisturizing and hydrating composition, comprising the steps of:
1) According to the weight parts of table 1, respectively weighing water, auxiliary materials and plant composition extracted essential oil, plant and fungus composition fermentation liquor for standby;
wherein the auxiliary materials comprise glycerin, butanediol, xanthan gum, trehalose and hydrogenated lecithin, and the dosage ratio of the glycerin, the butanediol, the xanthan gum, the trehalose and the hydrogenated lecithin is 10g:5g:1g:2g:0.3g;
mixing water and auxiliary materials, heating to 65-75 ℃ to enable the water and the auxiliary materials to be completely dissolved, and thus obtaining a mixed solution A;
2) Cooling the mixed solution A, reducing the temperature of the mixed solution A to 60 ℃, and then adding the fermentation liquor of the plant and fungus composition into the mixed solution A for stirring at a stirring speed of 5000rpm for 10 minutes to obtain a mixed solution B;
3) And (3) when the temperature of the mixed solution B is reduced to 40 ℃, adding the plant composition extract essential oil into the mixed solution B, and stirring at 1500rpm for 5 minutes to obtain the moisturizing and hydrating composition.
Injecting the moisturizing composition into films of non-woven fabrics, silk screens, cotton or fibrilia, biotin fibers, alginate fibers, bamboo charcoal fibers, hydrogel and the like through a filling machine to obtain the moisturizing mask; meanwhile, the moisturizing and hydrating composition can also be manufactured into a facial mask directly smeared on the face.
EXAMPLE 8,
The moisturizing composition of the embodiment comprises the raw materials shown in table 2.
TABLE 2
A process for the preparation of a moisturizing composition differs from example 7 in that in step 2) the temperature of the mixed solution A is reduced to 50 ℃.
EXAMPLE 9,
The moisturizing composition of the present embodiment comprises the raw materials shown in Table 3.
TABLE 3 Table 3
| Component (A) | Parts by weight |
| Extraction of essential oil from plant composition (I) | 2.00 |
| Fermentation liquor of plant and fungus composition (I) | 30.00 |
| Glycerol | 10.00 |
| Butanediol (butanediol) | 5.00 |
| Xanthan gum | 1.00 |
| Trehalose | 2.00 |
| Hydrogenated lecithin | 0.30 |
| Deionized water | To 100 |
A method for preparing a moisturizing composition, which is different from example 7 in that in step 2), the temperature of the mixed solution a is reduced to 40 ℃, the stirring speed is 5000rpm, and the time is 30 minutes;
in step 3), the temperature of the mixed solution B is reduced to 30 ℃; the stirring speed was 1500rpm for 15 minutes.
EXAMPLE 10,
The moisturizing and hydrating composition of this embodiment is different from embodiment 7 in that the plant and fungus composition fermentation broth (I) of embodiment 7 is changed to the plant and fungus composition fermentation broth (II).
EXAMPLE 11,
The moisturizing and hydrating composition of this embodiment is different from embodiment 7 in that the plant and fungus composition fermentation broth (I) of embodiment 7 is changed to the plant and fungus composition fermentation broth (III).
EXAMPLE 12,
The moisturizing composition of this example is different from example 7 in that the essential oil (I) extracted from the plant composition of example 7 is changed to the essential oil (II) extracted from the plant composition.
EXAMPLE 13,
The moisturizing composition of this example is different from example 7 in that the essential oil (I) extracted from the plant composition of example 7 is changed to the essential oil (III) extracted from the plant composition.
EXAMPLE 14,
The moisturizing and hydrating composition of this embodiment is different from embodiment 7 in that the fermentation broth (I) of the plant and fungus composition in embodiment 7 is changed to the fermentation broth (II) of the plant and fungus composition, and the extraction of essential oil (I) of the plant composition is changed to the extraction of essential oil (II) of the plant composition.
EXAMPLE 15,
The moisturizing and hydrating composition of this embodiment is different from embodiment 7 in that the fermentation broth (I) of the plant and fungus composition in embodiment 7 is changed to the fermentation broth (II) of the plant and fungus composition, and the extraction of essential oil (I) of the plant composition is changed to the extraction of essential oil (III) of the plant composition.
EXAMPLE 16,
The moisturizing and hydrating composition of this embodiment is different from embodiment 7 in that the plant and fungus composition fermentation broth (i) in embodiment 7 is changed to the plant and fungus composition fermentation broth (iii), and the plant composition extract essential oil (i) is changed to the plant composition extract essential oil (ii).
EXAMPLE 17,
The moisturizing and hydrating composition of this embodiment is different from embodiment 7 in that the plant and fungus composition fermentation broth (i) in embodiment 7 is changed to the plant and fungus composition fermentation broth (iii), and the plant composition extract essential oil (i) is changed to the plant composition extract essential oil (iii).
2. Comparative example
Comparative example 1: an essential oil (I) extracted from a single plant composition and a method for preparing the same, comprising the steps of:
s1: taking 50g of holy basil, drying to obtain dried raw materials, crushing the dried raw materials, and filtering by adopting a 50-100-mesh filter screen;
s2: placing the raw materials prepared in the step S1 into supercritical CO 2 Extracting in an extraction device;
the extraction conditions are as follows: extracting at 50deg.C under 25MPa for 2 hr, and collecting volatile oil;
s3: adding 5% of active carbon into the obtained volatile oil, stirring for 4-8 hours at 100rpm, filtering, and extracting the filtered solution;
and (3) standing the filtered solution at the temperature of between-4 and 10 ℃ for 12 to 24 hours, centrifuging the solution, and collecting supernatant after centrifuging to obtain the single plant composition extracted essential oil.
Comparative example 2: the essential oil (II) extracted from a single plant composition and the preparation method thereof are different from comparative example 1 in that 50g of the raw material holy basil is replaced by 30g of the raw material substituted flower.
Comparative example 3: the essential oil (III) extracted from a single plant composition and the preparation method thereof are different from comparative example 1 in that 50g of the raw material holy basil is changed into 20g of the raw material magnolia officinalis.
Comparative example 4: a single plant and fungus composition fermentation broth (I) and a preparation method thereof comprise the following steps:
s1: taking 10g of grifola frondosa, crushing the raw materials, and filtering by adopting a 50-100-mesh filter screen;
the dosage ratio of the grifola frondosa to the lactobacillus acidophilus to the water is 10g:3g:100mL;
the lactobacillus acidophilus is activated by adopting sterile water to obtain lactobacillus acidophilus bacterial liquid;
s2: putting the grifola frondosa filtered in the step S1 into a fermentation tank, and adding 8-10 times of water for mixing;
then the fermentation conditions are set as follows: heating the fermentation tank to 105 ℃, preserving heat for 15 minutes, and cooling to 37 ℃;
inoculating lactobacillus acidophilus bacterial liquid in a fermentation tank, closing the fermentation tank, introducing sterile nitrogen, performing anaerobic fermentation for 3 days, and controlling the fermentation temperature at 35-39 ℃ to obtain fermentation liquid;
s3: filtering the obtained fermentation liquor to obtain a filtered solution, sterilizing the filtered solution at 121 ℃ for 30 minutes, centrifuging the sterilized solution at 4000r/min for 15 minutes, discarding the precipitate, and collecting the supernatant to obtain the fermentation liquor of the plant and fungus composition.
Comparative example 5: a single plant and fungus composition fermentation broth (II) and a preparation method thereof are different from comparative example 4 in that 10g of raw material grifola frondosa is replaced by 40g of snakegourd fruit.
Comparative example 6: a single plant and fungus composition fermentation broth (III) and a preparation method thereof are different from comparative example 4 in that 10g of raw material grifola frondosa is replaced by 30g of semen Benincasae.
Comparative example 7: a single plant and fungus composition fermentation broth (IV) and a preparation method thereof are different from comparative example 4 in that 10g of raw material grifola frondosa is replaced by 10g of peach kernel.
Comparative example 8: a single plant and fungus composition broth (V) and a method for preparing the same are different from comparative example 4 in that 10g of raw material Grifola frondosa is replaced by 10g of Poria cocos.
Comparative example 9: a moisturizing and hydrating composition is different from example 7 in that the essential oil (I) extracted from a plant composition is changed to a single plant composition.
Comparative example 10: a moisturizing and hydrating composition is different from example 7 in that the essential oil (I) extracted from a plant composition is changed to the essential oil (II) extracted from a single plant composition.
Comparative example 11: a moisturizing composition is different from example 7 in that the essential oil (I) extracted from a plant composition is changed to the essential oil (III) extracted from a single plant composition.
Comparative example 12: a moisturizing and hydrating composition is different from example 7 in that the fermentation broth (I) of the plant and fungus composition is changed to the fermentation broth (I) of the single plant and fungus composition.
Comparative example 13: a moisturizing and hydrating composition is different from example 7 in that the fermentation broth (I) of the plant and fungus composition is changed to the fermentation broth (II) of the single plant and fungus composition.
Comparative example 14: a moisturizing and hydrating composition is different from example 7 in that the fermentation broth (I) of the plant and fungus composition is changed to the fermentation broth (III) of the single plant and fungus composition.
Comparative example 15: a moisturizing and hydrating composition is different from example 7 in that the fermentation broth (I) of the plant and fungus composition is changed to the fermentation broth (IV) of the single plant and fungus composition.
Comparative example 16: a moisturizing and hydrating composition is different from example 7 in that the fermentation broth (I) of the plant and fungus composition is changed to the fermentation broth (V) of the single plant and fungus composition.
Comparative example 17: a moisturizing and hydrating composition is different from example 7 in that essential oil (I) is extracted without adding a plant composition.
Comparative example 18: a moisturizing and hydrating composition is different from example 7 in that the fermentation broth (I) of the plant and fungus composition is not added.
Comparative example 19: a moisturizing and hydrating composition is different from example 7 in that essential oil (I) extracted from a plant composition and fermentation broth (I) of a plant and fungus composition are not added.
3. In order to better illustrate the inventive and advantageous effects of the present invention over the prior art, the following experiment was continued:
test example 1
Experimental samples: the compositions of examples 7 to 17, comparative examples 9 to 19.
Test preparation: 90 subjects aged 20-40 years were selected and randomized into 21 groups of 10 persons each. Any product with similar efficacy (cosmetic, external medicine or oral health care product) cannot be used 15 days before the tested part.
The testing method comprises the following steps:
the subjects of group 21 were cleaned and allowed to sit still in a constant temperature and humidity environment (temperature 25.+ -. 1 ℃ C., humidity 50.+ -. 5%) for 1 hour, the compositions of examples 7 to 17 and comparative examples 9 to 19 were uniformly applied to a circular nonwoven fabric having a diameter of 5cm, and after 15 minutes of application to the face, the resultant was removed and washed, and the moisture values of the skin before the skin was subjected to facial mask (blank) were measured by a skin moisture tester (Corneometer CM 825) and used for 1 hour, 2 hours and 4 hours. Judging the moisturizing effect of the mask according to the increase of the moisture content of the skin. The results are shown in Table 4.
[ skin moisture increase rate= (test value-blank value)/blank value×100% ]
Table 4 test results
*P<0.05
The following rules can be found from the data in table 4:
examples 7 to 9 show that the moisture-retaining effect of the weight ratio of the essential oil (I) extracted from the plant composition in example 7 to the fermentation broth (I) of the plant and fungus composition is better;
examples 7 to 17 show that the moisturizing effect is more remarkable in example 16, and the moisturizing effect of the combination of the essential oil (II) extracted from the plant composition and the fermentation broth (III) of the plant and fungus composition is more remarkable;
comparative examples 9 to 16 show that the moisture retention effect of the single plant composition extract essential oil or the single plant and fungus composition fermentation broth is not as good as that of the plant composition extract essential oil or the plant and fungus composition fermentation broth;
comparative examples 17 to 19 show that a moisturizing composition prepared from the plant composition extract essential oil and the plant and fungus composition fermentation broth has significantly better moisturizing effect than a moisturizing composition prepared from the plant composition extract essential oil alone or the plant and fungus composition fermentation broth or both.
Test example 2
Samples of example 7 and comparative examples 17 to 19 were taken, and antibacterial effect evaluation test was performed by referring to "evaluation method of antibacterial and antibacterial effects of daily chemical products (QB/T2738-2005)". The test operation is carried out according to a method for testing the antibacterial effect (bacteriostasis ring method) of the 7.5 antibacterial daily chemical product, and staphylococcus aureus (Staphylococcus aureus), candida albicans (Candida albicans) and pseudomonas aeruginosa (Pseudomonas aeruginosa) are used as test bacteria. The evaluation results of the antibacterial effect are shown in Table 5.
From the data in Table 5, it can be seen that a moisturizing and moisturizing composition prepared from the essential oil extracted from the plant composition and the fermentation broth of the plant and fungus composition has remarkable bacteriostatic effects on staphylococcus aureus (Staphylococcus aureus), candida albicans (Candida albicans) and pseudomonas aeruginosa (pseudomonas aeruginosa) (Pseudomonas aeruginosa). Compared with the condition that the plant composition is used singly to extract essential oil or the plant and fungus composition fermentation broth or both are not used, the antibacterial effect is obviously better.
In conclusion, various plant raw materials can be mutually synergistic, and when the plant composition extracts essential oil and the plant and fungus composition fermentation liquor are in a specific proportion, the efficacy is obviously improved, and compared with the effect of singly using the raw materials or the extract or the fermentation liquor on the skin moisture increase rate, the moisturizing and moisturizing composition, the mask and the preparation method and application thereof have better moisturizing and moisturizing effects.
In the description of the present specification, the terms "one embodiment," "some embodiments," "particular embodiments," and the like, mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the present invention. In this specification, schematic representations of the above terms do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The foregoing description of the preferred embodiments of the invention is not intended to limit the invention to the precise form disclosed, and any such modifications, equivalents, and alternatives falling within the spirit and scope of the invention are intended to be included within the scope of the invention.
Claims (3)
1. A method for preparing a moisturizing and hydrating composition, comprising the steps of:
1) Respectively weighing water, auxiliary materials, 5 parts by weight of plant composition extract essential oil and 40 parts by weight of plant and fungus composition fermentation liquor for standby; wherein the auxiliary materials comprise glycerin, butanediol, xanthan gum, trehalose and hydrogenated lecithin, and the dosage ratio of the glycerin, the butanediol, the xanthan gum, the trehalose and the hydrogenated lecithin is 10g:5g:1g:2g:0.3g; mixing water and auxiliary materials, heating to 65-75 ℃ to enable the water and the auxiliary materials to be completely dissolved, and obtaining a mixed solution A;
2) Cooling the mixed solution A, reducing the temperature of the mixed solution A to 60 ℃, adding the plant and fungus composition fermentation liquor, and uniformly stirring at a stirring speed of 5000rpm for 10 minutes to obtain a mixed solution B;
3) Reducing the temperature of the mixed solution B to 40 ℃, adding the plant composition to extract essential oil, and uniformly stirring at a stirring speed of 1500rpm for 5 minutes to obtain the moisturizing and moisturizing composition;
the preparation method for extracting essential oil from the plant composition comprises the following steps:
s1: taking 50g of holy basil, 30g of seville orange flower and 20g of magnolia officinalis flower, drying to obtain dried raw materials, crushing the dried raw materials, and filtering by adopting a 50-100-mesh filter screen;
s2: extracting in supercritical extraction device under the following conditions: extracting at 50deg.C under 25MPa for 2 hr, and collecting volatile oil;
s3: adding 5% active carbon into the volatile oil, stirring at 100rpm for 4-8 h, filtering, extracting filtered solution, standing the filtered solution at-4-10 ℃ for 12-24 h, centrifuging, and collecting supernatant to obtain the plant composition extracted essential oil;
the preparation method of the plant and fungus composition fermentation broth comprises the following steps:
s1: taking 10g of grifola frondosa, 40g of snakegourd fruit, 30g of semen Benincasae, 10g of peach kernel and 10g of poria cocos, crushing the raw materials, and filtering by a 50-100 mesh filter screen to form a plant and fungus composition, wherein the dosage ratio of the plant to fungus composition to lactobacillus acidophilus to water is 10g:3g:100mL; the lactobacillus acidophilus is activated by adopting sterile water to obtain lactobacillus acidophilus bacterial liquid;
s2: the plant and fungus composition is put into a fermentation tank, and 6-8 times of water is added for mixing; then heating the fermentation tank to 105 ℃, preserving heat for 15 minutes, and then cooling to 37 ℃; inoculating lactobacillus acidophilus bacterial liquid in a fermentation tank, closing the fermentation tank, and introducing sterile nitrogen for anaerobic fermentation at 35-39 ℃ for 3 days to obtain the fermentation liquid;
s3: filtering the obtained fermentation liquor to obtain a filtered solution, sterilizing the filtered solution at 121 ℃ for 30 minutes, centrifuging the sterilized solution at 4000r/min for 15 minutes, discarding the precipitate, and collecting the supernatant to obtain the plant and fungus composition fermentation liquor.
2. A facial mask prepared by the method of preparing the moisturizing composition of claim 1.
3. Use of the method for preparing a moisturizing composition according to claim 1 for preparing a mask.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101219096A (en) * | 2007-01-08 | 2008-07-16 | 胡馨元 | Pharmaceutical composition for removing speckle, production method and using method thereof |
| CN101693004A (en) * | 2009-02-27 | 2010-04-14 | 李艳平 | Face wrinkle-smoothing composition |
| CN107137318A (en) * | 2017-05-31 | 2017-09-08 | 华子昂 | A kind of ferment facial mask for improving skin moisture function and preparation method thereof |
| CN111346173A (en) * | 2020-02-20 | 2020-06-30 | 钱亚秋 | Traditional Chinese medicine composition, traditional Chinese medicine essential oil, traditional Chinese medicine skin care product and preparation method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101219096A (en) * | 2007-01-08 | 2008-07-16 | 胡馨元 | Pharmaceutical composition for removing speckle, production method and using method thereof |
| CN101693004A (en) * | 2009-02-27 | 2010-04-14 | 李艳平 | Face wrinkle-smoothing composition |
| CN107137318A (en) * | 2017-05-31 | 2017-09-08 | 华子昂 | A kind of ferment facial mask for improving skin moisture function and preparation method thereof |
| CN111346173A (en) * | 2020-02-20 | 2020-06-30 | 钱亚秋 | Traditional Chinese medicine composition, traditional Chinese medicine essential oil, traditional Chinese medicine skin care product and preparation method |
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