CN113624795B - 用于表面缺陷检测和分析的产生脉冲中子的瞬时伽马发射测量系统 - Google Patents
用于表面缺陷检测和分析的产生脉冲中子的瞬时伽马发射测量系统 Download PDFInfo
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Abstract
本发明公开一种确定部件中的结构缺陷的方法，该方法利用具有通过毛细吸收渗透到材料表面上的小裂缝的能力的溶液的中子激活，当暴露于中子脉冲时，所述溶液产生限定能量的可分辨的瞬时伽马释放。在表面上的用户受控位置以期望能量产生的伽马射线的强度被用于确定裂缝位置、长度和深度。
Description
本申请是申请号为201780030260.5，申请日为2017年4月13日，发明名称为“用于表面缺陷检测和分析的产生脉冲中子的瞬时伽马发射测量系统”的发明专利申请的分案申请。
技术领域
本发明总的涉及被辐射表面中的裂缝的检测，更具体地说，涉及被辐射部件的无损检查以确定结构瑕疵。
背景技术
在需要操纵高放射性部件或放射性材料的容器时，重要的是确保评估部件或材料容器的结构完整性，以减小放射性材料失控或失去容纳的可能。由于放射场对设备评估和可操作性的影响，使用标准的视觉和超声无损检测(NDE)技术难以评估放射性部件或位于高放射场中的放射性材料的容器的结构完整性。存在提供设备使用适于高辐射环境的方法和装置评价放射性部件和放射性材料的容器的结构完整性的需求。
发明内容
本发明公开了一种无损地检测被照射的材料的表面中的结构缺陷的方法，包括向材料的表面施加发射限定能量的瞬时伽马释放的液体裂缝渗透剂的步骤，该液体裂缝渗透剂优选具有高含氮量，或者与具有大量同位素的化学物质混合，该同位素具有较大快速中子瞬时捕获伽马发射截面，例如钪、钒、锰或钛。然后使用中子脉冲发生器照射该表面，并且被调谐到该限定的能量的多个贝塔辐射检测器按照规则的模式定位在施加了该混合物的材料的表面；所述多个贝塔辐射检测器各自提供输出，该输出指示在由所述多个贝塔辐射检测器中对应的贝塔辐射检测器观察的表面区域中所述限定能量的瞬时伽马释放的接收。采用该接收来测定缺陷的特征。在一个实施例中，该特征是表面上的缺陷的位置和长度。在另一个实施例中，该特征是表面上的缺陷的深度。优选地，根据接收的强度确定缺陷的深度。
在一个这样的实施例中，混合物通过毛细吸收被吸收到表面内。期望地，中子脉冲发生器是纽催斯特(neutristor)型中子脉冲发生器。优选地，通过在表面和贝塔辐射检测器的有源部分之间布置高原子数牺牲性材料作为电子辐射器。期望地，贝塔辐射检测器是碳化硅(SiC)检测器，选择贝塔辐射检测器的牺牲性层中使用的材料的类型、与有源检测器区域的距离、以及厚度，从而确保由期望发射的瞬时伽马辐射能量的光电吸收产生的大部分电子完全停止在SiC检测器的有源区域中。在一个这样的实施例中，牺牲性材料为铂或钨。
附图说明
当与附图结合阅读，能够从下述优选实施例得到对本发明的进一步理解。其中
图1是本发明的设备布局的示意性表示；以及
图2是图1的SiC检测器阵列中使用的SiC检测器和前置放大器的示意性布局。
具体实施方式
本发明的操作基础是建立在染料渗透剂裂缝检测、瞬时中子伽马(γ)辐射检测、以及平面计算机化断层显像(CT)技术的新颖结合上的。该系统还使用新颖的SiC调谐的伽马强度检测方法和基于固态真空管技术的用于非常小SiC信号输出的前置放大器。优选的实施例如下：非腐蚀性裂缝渗透剂，优选具有高含氮量的非腐蚀性裂缝渗透剂，或者诸如可以从位于佐治亚州Cartersville的Dynaflux Quality Products Company获得的裂缝渗透剂，其与含有大比例的具有较大快速中子瞬时捕获伽马发射截面(例如钪、钒、锰、钛)的一类化学物质混合，酌情在受控的温度和压强下被施加，以确保渗透剂到达被检查的表面时处于液态。本公开描述的系统有将混合物高压喷洒到待检查表面的能力，以允许在该系统硬件不实际触碰表面的情况下施加该物质。包含在测量组件中的由Sandia NationalLaboratory(“Innovation Marketplace”,2014年9月，第1卷第3期)开发的“纽催斯特(neutristor)”型中子脉冲发生器(NPG)组件被操作者放置到表面一英寸内的径向位置处，该径向位置已知在表面上的固定表面参考点0.1mm内。NPG组件被特殊配置的SiC辐射检测器阵列(例如，1mm2检测器的100×100正方形，例如2013年2月18日递交的、名称为“SolidState Radiation Detector With Enhanced Gamma Radiation Sensitivity”、专利申请号13/769,401中所述)包围，这些SiC辐射检测器的位置已知位于NPG组件上的参考点的0.05mm内，这些SiC辐射检测器被调谐以主要测量在从裂缝渗透剂混合物中的瞬时伽马发射同位素发射的伽马辐射与SiC检测器的有源区域之间的材料中生成的光电子吸收产生的电子的强度，如图1所示。
本发明的无损检查系统10具有可以在待检测材料的表面20上移动的喷洒系统18，以在表面上裂缝渗透剂溶液30。中子脉冲发生器12发射与裂缝渗透剂溶液30内的同位素反应的脉冲流，以发射被SiC辐射检测器24检测的瞬时伽马辐射。SiC辐射检测器的输出被馈送给前置放大器26，前置放大器的输出被发送给处理电子器件，处理电子器件，处理电子器件解释接收信号的强度和变化，以确定裂缝的存在以及位置、长度和深度。通过在SiC检测器的有源部分和表面之间布置稿原子数的牺牲性材料(例如铂或钨)作为电子辐射器，实现SiC贝塔(β)辐射能力灵敏度的调谐。选择检测器的牺牲性层中使用的材料类型、与有源检测器区域的距离、以及厚度，以确保由期望的所发射的瞬时伽马辐射能量在牺牲性层中的光电子吸收产生的绝大多数电子完全停止在SiC检测器的有源区域内。这可以由本领域技术人员通过以下方式实现：适当地调节电子辐射器的表面与SiC的覆盖肖特基界面区域的铝的前表面之间的距离，使得能量小于全部伽马能量的电子几乎不可能到达并且停止在SiC检测器的有源体积中。这将确保所测量的检测器输出与每个检测器看到的裂缝中的渗透剂材料的量成比例，从而与裂缝的尺寸属性成比例。图2提供了SiC检测器和相关联的阵列几何形状的示意图。
SiC检测器24通过牺牲性材料36接收瞬时伽马辐射38，牺牲性材料36转换瞬时伽马辐射以通过光电子吸收产生电子，其中牺牲性材料36与肖特基接触面的距离是可变的，以确保捕获到全部电子。在该实施例中，电子行进穿过大约10μm厚的N掺杂的SiC 40，到达基底42，电子在基底42处被背面为金的欧姆接触44收集，并且输出电流28通过前置放大器26被传送给处理电子器件46。在中子脉冲发生器触发一次或多次后由检测器阵列中每个非常小且精确定位的SiC检测器获得的相对测量强度数据将被用于确定缺陷的尺寸特征。检测器信号输出将被输入到单独的前置放大器中，这些单独的前置放大器集成到利用小型化设计(例如2016年1月15日递交的名称为“In-Containment Ex-Core Detector System”的美国专利申请No.14/996,667所述)的中子脉冲发生器结构中。然后，放大后的测量检测器电流信号被发送给位于高辐射区域外的方便位置处的测量和分析系统。使用平面CT算法，根据SiC检测器阵列几何形状和阵列中每个检测器的相对测量结果确定期望的测量的裂缝尺寸属性(例如深度、宽度、长度)之间的与具体应用相关的关联性。
虽然已经详细描述了本发明的具体实施例，但是本领域技术人员应当理解，基于本公开的整体教导，可以开发出这些具体内容的各种修改和替换。因此，所公开的具体实施例仅为了示意性的说明，而不是为了限制本发明的范围，本发明的范围的全部广度由所附的权利要求及其任何及全部等价部分给出。
Claims (15)
1.一种无损检测被照射的材料的表面中的结构缺陷的方法，包括以下步骤：
向待检查的材料的表面施加包括非腐蚀性裂缝渗透剂的混合物，所述混合物还包括对于限定能量的、快速中子诱发的瞬时伽马发射反应具有较大截面的化学物质，所述化学物质包含钪、钛、锰或钒；
使用中子脉冲发生器照射所述材料的表面；
在施加了所述混合物的材料的表面上按照规则的模式定位多个贝塔辐射检测器，所述贝塔辐射检测器被调谐到在位于检测器的有源区域和被检查的表面之间的电子生成窗中生成的光电产生电子的所述限定能量，所述多个贝塔辐射检测器各自提供输出，该输出指示在由所述多个贝塔辐射检测器中的对应一个贝塔辐射检测器观察的表面区域中所述限定能量的瞬时伽马释放的接收；以及
采用所述接收来测定所述缺陷的特征。
2.根据权利要求1所述的方法，其中所述特征为所述表面上的所述缺陷的位置、长度和深度中的至少一种。
3.根据权利要求2所述的方法，其中根据所述接收的强度来确定所述缺陷的深度。
4.根据权利要求1所述的方法，其中所述混合物通过毛细吸收被吸收到所述表面内。
5.根据权利要求1所述的方法，其中所述中子脉冲发生器是纽催斯特型中子脉冲发生器。
6.根据权利要求1所述的方法，其中通过把高原子数牺牲性材料布置在被检查的表面和贝塔辐射检测器的有源部分之间作为电子辐射器来实现贝塔辐射检测器的调谐。
7.根据权利要求6所述的方法，其中所述贝塔辐射检测器是碳化硅(SiC)检测器，以及选择所述贝塔辐射检测器的牺牲性层中使用的材料的类型、与有源检测器区域的距离以及厚度，以确保由期望的发射的瞬时伽马辐射能量的光电吸收产生的电子的大多数完全停止在SiC检测器的有源区域内部。
8.根据权利要求6所述的方法，其中所述牺牲性材料为铂或钨。
9.一种用于无损地检测和表征被照射的材料的表面中的缺陷的设备，包括：
喷洒系统，被构造成向待检查的材料的表面喷洒包括非腐蚀性裂缝渗透剂的混合物，所述非腐蚀性裂缝渗透剂具有高含氮量，或者与具有大量同位素的化学物质混合，所述同位素具有光电的限定能量的、较大的快速中子瞬时捕获伽马发射截面，所述化学物质包含钪、钒、锰或钛；
中子脉冲发生器，被构造成照射材料的表面；
多个贝塔辐射检测器，被调谐到在位于贝塔辐射检测器的有源区域和被检查的表面之间的电子生成窗中生成的光电产生电子能量的所述限定能量，所述贝塔辐射检测器在施加了所述混合物的材料的表面上按照预定的模式定位，所述多个贝塔辐射检测器各自提供输出，该输出指示在由所述多个贝塔辐射检测器中的对应一个贝塔辐射检测器观察的表面区域中所述限定能量的瞬时伽马释放的接收；以及
贝塔辐射检测器输出，根据所述贝塔辐射检测器输出能够采用所述接收来测定所述缺陷的特征。
10.根据权利要求9所述的设备，其中所述特征为所述表面上的所述缺陷的位置、长度和深度中的至少一种。
11.根据权利要求10所述的设备，其中根据所述接收的强度来确定所述缺陷的深度。
12.根据权利要求9所述的设备，其中所述中子脉冲发生器是纽催斯特型中子脉冲发生器。
13.根据权利要求9所述的设备，其中所述贝塔辐射检测器包括位于被检查的表面和贝塔辐射检测器的有源部分之间作为电子辐射器的高原子数牺牲性材料。
14.根据权利要求13所述的设备，其中所述贝塔辐射检测器是碳化硅(SiC)检测器，以及选择所述贝塔辐射检测器的牺牲性层中使用的材料的类型、与有源检测器区域的距离以及厚度，以确保由期望的发射的瞬时伽马辐射能量的光电吸收产生的电子的大多数完全停止在SiC检测器的有源区域内部。
15.根据权利要求13所述的设备，其中所述牺牲性材料为铂或钨。
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| CN202110894088.6A CN113624795B (zh) | 2016-05-17 | 2017-04-13 | 用于表面缺陷检测和分析的产生脉冲中子的瞬时伽马发射测量系统 |
| PCT/US2017/027326 WO2017200666A1 (en) | 2016-05-17 | 2017-04-13 | Pulsed neutron generated prompt gamma emission measurement system for surface defect detection and analysis |
| CN201780030260.5A CN109154578B (zh) | 2016-05-17 | 2017-04-13 | 用于表面缺陷检测和分析的产生脉冲中子的瞬时伽马发射测量系统 |
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| EP3458847B1 (en) | 2021-06-09 |
| US9528952B1 (en) | 2016-12-27 |
| JP2019521313A (ja) | 2019-07-25 |
| KR102397712B1 (ko) | 2022-05-12 |
| EP3458847A4 (en) | 2020-02-26 |
| EP3458847A1 (en) | 2019-03-27 |
| JP6981998B2 (ja) | 2021-12-17 |
| CN109154578B (zh) | 2021-11-05 |
| CN113624795A (zh) | 2021-11-09 |
| CN109154578A (zh) | 2019-01-04 |
| WO2017200666A1 (en) | 2017-11-23 |
| KR20180137579A (ko) | 2018-12-27 |
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