CN113462473A - Preparation method of perfume type essence with lasting fragrance - Google Patents
Preparation method of perfume type essence with lasting fragrance Download PDFInfo
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- CN113462473A CN113462473A CN202110787446.3A CN202110787446A CN113462473A CN 113462473 A CN113462473 A CN 113462473A CN 202110787446 A CN202110787446 A CN 202110787446A CN 113462473 A CN113462473 A CN 113462473A
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- 239000002304 perfume Substances 0.000 title claims abstract description 32
- 239000003205 fragrance Substances 0.000 title claims abstract description 30
- 230000002045 lasting effect Effects 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 239000003094 microcapsule Substances 0.000 claims abstract description 49
- 239000000463 material Substances 0.000 claims abstract description 37
- 238000001035 drying Methods 0.000 claims abstract description 32
- 239000002994 raw material Substances 0.000 claims abstract description 27
- 238000000227 grinding Methods 0.000 claims abstract description 25
- 238000000034 method Methods 0.000 claims abstract description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 19
- 241000233855 Orchidaceae Species 0.000 claims abstract description 17
- 244000288157 Passiflora edulis Species 0.000 claims abstract description 17
- 235000000370 Passiflora edulis Nutrition 0.000 claims abstract description 17
- 241000220317 Rosa Species 0.000 claims abstract description 17
- 241000722921 Tulipa gesneriana Species 0.000 claims abstract description 17
- 239000002904 solvent Substances 0.000 claims abstract description 16
- 239000002131 composite material Substances 0.000 claims abstract description 15
- 239000008367 deionised water Substances 0.000 claims abstract description 11
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 11
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 230000002087 whitening effect Effects 0.000 claims abstract description 11
- PUSKHXMZPOMNTQ-UHFFFAOYSA-N ethyl 2,1,3-benzoselenadiazole-5-carboxylate Chemical group CCOC(=O)C1=CC=C2N=[Se]=NC2=C1 PUSKHXMZPOMNTQ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 34
- 239000000203 mixture Substances 0.000 claims description 32
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 30
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 30
- 238000002156 mixing Methods 0.000 claims description 27
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 25
- 239000000047 product Substances 0.000 claims description 18
- 239000002244 precipitate Substances 0.000 claims description 15
- 238000001132 ultrasonic dispersion Methods 0.000 claims description 15
- 238000012216 screening Methods 0.000 claims description 14
- 239000012535 impurity Substances 0.000 claims description 13
- UJNOLBSYLSYIBM-WISYIIOYSA-N [(1r,2s,5r)-5-methyl-2-propan-2-ylcyclohexyl] (2r)-2-hydroxypropanoate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(=O)[C@@H](C)O UJNOLBSYLSYIBM-WISYIIOYSA-N 0.000 claims description 10
- 238000004806 packaging method and process Methods 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 9
- 230000001954 sterilising effect Effects 0.000 claims description 9
- 238000004659 sterilization and disinfection Methods 0.000 claims description 9
- 235000019441 ethanol Nutrition 0.000 claims description 8
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 7
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 7
- 229940041616 menthol Drugs 0.000 claims description 7
- 239000000341 volatile oil Substances 0.000 claims description 7
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 6
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 6
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 6
- 244000037364 Cinnamomum aromaticum Species 0.000 claims description 5
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 claims description 5
- SVURIXNDRWRAFU-OGMFBOKVSA-N cedrol Chemical compound C1[C@]23[C@H](C)CC[C@H]3C(C)(C)[C@@H]1[C@@](O)(C)CC2 SVURIXNDRWRAFU-OGMFBOKVSA-N 0.000 claims description 5
- 229940026455 cedrol Drugs 0.000 claims description 5
- PCROEXHGMUJCDB-UHFFFAOYSA-N cedrol Natural products CC1CCC2C(C)(C)C3CC(C)(O)CC12C3 PCROEXHGMUJCDB-UHFFFAOYSA-N 0.000 claims description 5
- SVURIXNDRWRAFU-UHFFFAOYSA-N juniperanol Natural products C1C23C(C)CCC3C(C)(C)C1C(O)(C)CC2 SVURIXNDRWRAFU-UHFFFAOYSA-N 0.000 claims description 5
- YEFOAORQXAOVJQ-RZFZLAGVSA-N schisandrol a Chemical compound C1[C@H](C)[C@@](C)(O)CC2=CC(OC)=C(OC)C(OC)=C2C2=C1C=C(OC)C(OC)=C2OC YEFOAORQXAOVJQ-RZFZLAGVSA-N 0.000 claims description 5
- 239000012258 stirred mixture Substances 0.000 claims description 5
- 238000009777 vacuum freeze-drying Methods 0.000 claims description 5
- 239000002518 antifoaming agent Substances 0.000 claims description 3
- 150000002191 fatty alcohols Chemical class 0.000 claims description 2
- 239000002671 adjuvant Substances 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 230000005923 long-lasting effect Effects 0.000 claims 1
- 230000008569 process Effects 0.000 abstract description 7
- 210000005036 nerve Anatomy 0.000 description 12
- 210000004556 brain Anatomy 0.000 description 10
- 230000000694 effects Effects 0.000 description 5
- 230000001914 calming effect Effects 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 230000001105 regulatory effect Effects 0.000 description 4
- 238000007873 sieving Methods 0.000 description 4
- 241000934878 Sterculia Species 0.000 description 3
- 235000021282 Sterculia Nutrition 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 230000001276 controlling effect Effects 0.000 description 3
- 229940059107 sterculia Drugs 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 230000000474 nursing effect Effects 0.000 description 2
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000000834 fixative Substances 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention relates to the technical field of perfume type essence preparation, and discloses a preparation method of perfume type essence with lasting fragrance, which comprises the following steps: s1: preparing raw materials, 20-50 parts of deionized water, 12-40 parts of passion fruit, 20-30 parts of dried rose petals, 2-8 parts of dried tulip petals, 3-6 parts of dried orchid, 30-60 parts of a composite solvent, 10-28 parts of auxiliary materials, 2-14 parts of whitening talcum powder, 8-22 parts of absolute ethyl alcohol and 8-16 parts of microcapsule essence; s2: grinding and dissolving, namely putting the dried passion fruit, the dried rose petals, the dried tulip petals and the dried orchid in a ball mill for grinding for 30-50 minutes; s3: and (5) standing and drying. The perfume type essence has the advantages of reasonable raw material proportion, precise control of various conditions in the preparation process, simple process, mellow fragrance, strong durability, strong applicability and good market prospect.
Description
Technical Field
The invention relates to the technical field of perfume type essence preparation, in particular to a preparation method of perfume type essence with lasting fragrance.
Background
The perfume is an alcoholic solution of essence, and is added with a proper amount of perfume fixative and the like, so that the perfume has aromatic and strong fragrance, is mainly sprayed on parts such as lappets, handkerchiefs, hairlines and the like, and emits pleasant fragrance, so that the perfume is one of important cosmetics.
The essence is widely applied in daily life, is often applied in the fields of skin care, nursing, air freshening, oral cavity nursing, perfume and the like, the existing perfume type essence has more complex preparation process, and the prepared essence is not lasting enough and cannot meet the requirements of people.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a preparation method of perfume type essence with lasting fragrance, which solves the problems that the existing perfume type essence is complex in preparation process, the prepared essence is not lasting enough and cannot meet the requirements of people.
(II) technical scheme
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of perfume type essence with lasting fragrance comprises the following steps:
s1: preparing raw materials, 20-50 parts of deionized water, 12-40 parts of passion fruit, 20-30 parts of dried rose petals, 2-8 parts of dried tulip petals, 3-6 parts of dried orchid, 30-60 parts of a composite solvent, 10-28 parts of auxiliary materials, 2-14 parts of whitening talcum powder, 8-22 parts of absolute ethyl alcohol and 8-16 parts of microcapsule essence;
s2: grinding and dissolving, namely putting the passion fruit, the rose petal, the tulip petal and the orchid in a ball mill for grinding for 30-50 minutes, then screening to remove impurities, adding a composite solvent and deionized water, stirring and mixing to obtain a mixture A, screening by using a 200-mesh and 500-mesh screen, heating while stirring and mixing, and keeping the constant temperature at 40-60 ℃;
s3: standing and drying, standing the obtained mixture A for 10-20 minutes, and then drying at high temperature to obtain a mixture B;
s4: mixing, namely putting the whitening talcum powder, the absolute ethyl alcohol, the microcapsule essence and the mixture B into a stirrer for stirring, wherein the stirring speed is controlled to be 1800 r/min;
s5: ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion for 30-50 minutes, standing for 10-30 minutes, and collecting the precipitate C at the lower layer after standing;
s6: adding auxiliary materials, adding the auxiliary materials and the precipitate C into a stirrer, and stirring for 10-25 minutes to obtain a mixture D;
s7: drying again, namely putting the mixture D into a drying chamber for vacuum freeze drying, and then grinding to obtain a finished product;
s8: collecting and packaging, and packaging the finished product under aseptic condition for later use.
As a further scheme of the present invention, the composite solvent in S1 is a mixture of propylene glycol, dichloromethane, menthyl lactate and diethyl ether, and the ratio of the propylene glycol: dichloromethane: menthyl lactate: ethyl ether 1-3:2-6:3-5: 1-4.
Further, the auxiliary materials in S6 are one or more of schizandrol, cassia seed alcohol, cedrol and fatty alcohol, and the auxiliary materials are ground, sieved after grinding, and subjected to ultraviolet sterilization treatment before being added.
On the basis of the scheme, the microcapsule essence in the S4 is one or more of passion fruit microcapsule essence, rose petal microcapsule essence, tulip petal microcapsule essence, orchid microcapsule essence and apple microcapsule essence.
Further, menthol and peppermint essential oil are added in the step of mixing in the step of S2.
On the basis of the scheme, the temperature for high-temperature drying in the S3 is 40-70 ℃, and air circulation is kept during drying.
In a further scheme of the invention, the precipitate C obtained in the step S6 is preserved at a constant temperature of 30-60 ℃ for 2-5 hours, and then auxiliary materials are added.
Further, 2-8 parts of a defoaming agent is added in the S4 during mixing, and the raw materials are added and stirred during mixing, wherein the stirring time is 20-40 minutes.
(III) advantageous effects
Compared with the prior art, the invention provides the preparation method of the perfume type essence with lasting fragrance, and the preparation method has the following beneficial effects:
1. the raw materials are reasonable in proportion, various conditions are precisely controlled in the preparation process, the process is simple, the prepared perfume type essence is mellow in fragrance, strong in durability and applicability and good in market prospect, impurities with large particles can be removed through the screening step, and the raw materials can be mixed more fully through the heating constant-temperature stirring step without damaging the performance of the raw materials.
2. According to the invention, the product has the effects of calming the nerves, benefiting intelligence, regulating nerves, clearing away the heart fire, soothing the nerves and refreshing the brain by adding the auxiliary materials, and the purity and safety of the auxiliary materials can be ensured after grinding, sieving and ultraviolet sterilization, so that the overall quality of the product is improved.
3. According to the invention, the types of the flavors of the essence can be enriched by adding the microcapsule essence, the microcapsule essence can be fused with the raw materials, the flavor is slowly released, the durability of the essence is improved, the menthol and the mint essential oil can refresh the brain and refresh the brain when in use, and the functions of the essence are enriched.
4. According to the invention, excessive volatilization of components in the essence can be prevented by controlling the drying temperature, waste of raw material components is prevented, and microorganisms in the precipitate C can be fully fermented by a constant-temperature preservation step, so that the essence is mellow.
Drawings
Fig. 1 is a schematic flow structure diagram of a preparation method of a perfume type essence with lasting fragrance provided by the invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
Referring to fig. 1, a method for preparing a perfume type essence with lasting fragrance comprises the following steps:
s1: the method comprises the following steps of preparing raw materials, namely 20 parts of deionized water, 15 parts of dried passion fruit, 20 parts of dried rose petals, 5 parts of dried tulip petals, 5 parts of dried orchid, 40 parts of a composite solvent, 16 parts of auxiliary materials, 7 parts of whitening talcum powder, 12 parts of absolute ethyl alcohol and 12 parts of microcapsule essence, wherein the raw materials are reasonable in proportion, each condition is precisely controlled in the preparation process, the process is simple, and the prepared perfume essence is mellow in fragrance, strong in durability and strong in applicability and has a good market prospect;
s2: grinding and dissolving, namely putting the passion fruit, the rose petal, the tulip petal and the orchid in a ball mill for grinding for 30 minutes, screening to remove impurities, adding a composite solvent and deionized water, stirring and mixing to obtain a mixture A, heating while stirring and mixing by using a 300-mesh screen during screening, keeping constant temperature at 50 ℃, removing impurities with larger particles through the screening step, and enabling the raw materials to be mixed more fully without damaging the performance through the heating and constant-temperature stirring step;
s3: standing and drying, standing the obtained mixture A for 15 minutes, and then drying at high temperature to obtain a mixture B;
s4: mixing, putting the whitening talcum powder, the absolute ethyl alcohol, the microcapsule essence and the mixture B into a stirrer together for stirring, wherein the stirring speed is controlled at 1700 r/min;
s5: ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion for 37 minutes, then standing for 19 minutes, and collecting the precipitate C at the lower layer after standing;
s6: adding auxiliary materials, adding the auxiliary materials and the precipitate C into a stirrer, and stirring for 20 minutes to obtain a mixture D;
s7: drying again, namely putting the mixture D into a drying chamber for vacuum freeze drying, and then grinding to obtain a finished product;
s8: collecting and packaging, and packaging the finished product under aseptic condition for later use.
The composite solvent in the S1 is prepared by mixing propylene glycol, dichloromethane, menthyl lactate and diethyl ether, wherein the ratio of the propylene glycol: dichloromethane: menthyl lactate: the ethyl ether is 1:2:3:1, the auxiliary materials in the S6 are one or more of schizandrol, cassia seed alcohol, cedrol and sterculia alcohol, the auxiliary materials are ground, sieved after grinding, impurities are removed, then ultraviolet sterilization is carried out, the product has the effects of calming the nerves, benefiting intelligence, regulating nerves, clearing away the heart fire, soothing the nerves and refreshing the brain by adding the auxiliary materials, the purity and the safety of the auxiliary materials can be ensured after grinding, sieving and ultraviolet sterilization, the overall quality of the product is improved, the microcapsule essence in the S4 is one or more of passion fruit microcapsule essence, rose petal microcapsule essence, tulip petal microcapsule essence, orchid microcapsule essence and apple microcapsule essence, the types of the essence fragrance can be enriched by adding the microcapsule essence, and the microcapsule essence can be fused with the raw materials to slowly release the fragrance, the durability of the essence is improved.
Example 2
Referring to fig. 1, a method for preparing a perfume type essence with lasting fragrance comprises the following steps:
s1: the method comprises the following steps of preparing raw materials, namely 25 parts of deionized water, 14 parts of dried passion fruit, 26 parts of dried rose petals, 6 parts of dried tulip petals, 5 parts of dried orchid, 33 parts of a composite solvent, 16 parts of auxiliary materials, 7 parts of whitening talcum powder, 12 parts of absolute ethyl alcohol and 12 parts of microcapsule essence, wherein the raw materials are reasonable in proportion, each condition is precisely controlled in the preparation process, the process is simple, and the prepared perfume essence is mellow in fragrance, strong in durability and strong in applicability and has a good market prospect;
s2: grinding and dissolving, namely putting the passion fruit, the rose petal, the tulip petal and the orchid in a ball mill for grinding for 30 minutes, screening to remove impurities, adding a composite solvent and deionized water, stirring and mixing to obtain a mixture A, heating while stirring and mixing by using a 300-mesh screen during screening, keeping constant temperature at 50 ℃, removing impurities with larger particles through the screening step, and enabling the raw materials to be mixed more fully without damaging the performance through the heating and constant-temperature stirring step;
s3: standing and drying, standing the obtained mixture A for 15 minutes, and then drying at high temperature to obtain a mixture B;
s4: mixing, putting the whitening talcum powder, the absolute ethyl alcohol, the microcapsule essence and the mixture B into a stirrer together for stirring, wherein the stirring speed is controlled at 1700 r/min;
s5: ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion for 37 minutes, then standing for 22 minutes, and collecting the precipitate C at the lower layer after standing;
s6: adding auxiliary materials, adding the auxiliary materials and the precipitate C into a stirrer, and stirring for 20 minutes to obtain a mixture D;
s7: drying again, namely putting the mixture D into a drying chamber for vacuum freeze drying, and then grinding to obtain a finished product;
s8: collecting and packaging, and packaging the finished product under aseptic condition for later use.
The composite solvent in the S1 is prepared by mixing propylene glycol, dichloromethane, menthyl lactate and diethyl ether, wherein the ratio of the propylene glycol: dichloromethane: menthyl lactate: the ethyl ether is 1:2.5:3:2, the auxiliary materials in the S6 are one or more of schizandrol, cassia seed alcohol, cedrol and sterculia alcohol, the auxiliary materials are ground before being added, and are sieved after being ground to remove impurities, and then are subjected to ultraviolet sterilization treatment, so that the product has the effects of calming the nerves and improving intelligence, regulating nerves, clearing away the heart-fire and soothing the nerves and refreshing the brain by adding the auxiliary materials, and the purity and the safety of the auxiliary materials can be ensured after grinding and sieving and ultraviolet sterilization, so that the overall quality of the product is improved, the microcapsule essence in the S4 is one or more of passion fruit microcapsule essence, rose petal microcapsule essence, tulip petal microcapsule essence, orchid microcapsule essence and apple microcapsule essence, the types of essence can be enriched by adding the microcapsule essence, and the microcapsule essence can be fused with the raw materials to slowly release the fragrance, the durability of the essence is improved.
It should be particularly noted that menthol and mint essential oil are added in the step S2 during mixing, the menthol and mint essential oil can refresh the brain and refresh the brain during use, and the essence can be enriched, the temperature for high-temperature drying in the step S3 is 50 ℃, the circulation of air is maintained during drying, and the excessive volatilization of the components in the essence can be prevented by controlling the drying temperature, so that the waste of the components of the raw materials is prevented.
Example 3
Referring to fig. 1, a method for preparing a perfume type essence with lasting fragrance comprises the following steps:
s1: the method comprises the following steps of preparing raw materials, namely 30 parts of deionized water, 22 parts of dried passion fruit, 24 parts of dried rose petals, 6 parts of dried tulip petals, 5 parts of dried orchid, 30 parts of a composite solvent, 16 parts of auxiliary materials, 3 parts of whitening talcum powder, 11 parts of absolute ethyl alcohol and 8 parts of microcapsule essence, wherein the raw materials are reasonable in proportion, each condition is precisely controlled in the preparation process, the process is simple, and the prepared perfume type essence is mellow in fragrance, strong in durability and strong in applicability and has a good market prospect;
s2: grinding and dissolving, namely putting the passion fruit, the rose petal, the tulip petal and the orchid in a ball mill for grinding for 30 minutes, screening to remove impurities, adding a composite solvent and deionized water, stirring and mixing to obtain a mixture A, heating while stirring and mixing by using a 300-mesh screen during screening, keeping constant temperature at 50 ℃, removing impurities with larger particles through the screening step, and enabling the raw materials to be mixed more fully without damaging the performance through the heating and constant-temperature stirring step;
s3: standing and drying, standing the obtained mixture A for 20 minutes, and then drying at high temperature to obtain a mixture B;
s4: mixing, putting the whitening talcum powder, the absolute ethyl alcohol, the microcapsule essence and the mixture B into a stirrer together for stirring, wherein the stirring speed is controlled at 1800 r/min;
s5: ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion for 37 minutes, then standing for 24 minutes, and collecting the precipitate C at the lower layer after standing;
s6: adding auxiliary materials, adding the auxiliary materials and the precipitate C into a stirrer, and stirring for 20 minutes to obtain a mixture D;
s7: drying again, namely putting the mixture D into a drying chamber for vacuum freeze drying, and then grinding to obtain a finished product;
s8: collecting and packaging, and packaging the finished product under aseptic condition for later use.
The composite solvent in the S1 is prepared by mixing propylene glycol, dichloromethane, menthyl lactate and diethyl ether, wherein the ratio of the propylene glycol: dichloromethane: menthyl lactate: the ethyl ether is 1:2:3:1, the auxiliary materials in the S6 are one or more of schizandrol, cassia seed alcohol, cedrol and sterculia alcohol, the auxiliary materials are ground, sieved after grinding, impurities are removed, then ultraviolet sterilization is carried out, the product has the effects of calming the nerves, benefiting intelligence, regulating nerves, clearing away the heart fire, soothing the nerves and refreshing the brain by adding the auxiliary materials, the purity and the safety of the auxiliary materials can be ensured after grinding, sieving and ultraviolet sterilization, the overall quality of the product is improved, the microcapsule essence in the S4 is one or more of passion fruit microcapsule essence, rose petal microcapsule essence, tulip petal microcapsule essence, orchid microcapsule essence and apple microcapsule essence, the types of the essence fragrance can be enriched by adding the microcapsule essence, and the microcapsule essence can be fused with the raw materials to slowly release the fragrance, the durability of the essence is improved.
It is particularly noted that menthol and mint essential oil are added in the step S2 during mixing, the menthol and mint essential oil can be added to refresh the brain and refresh the brain during use, and enrich the function of the essence, the temperature of high-temperature drying in the step S3 is 50 ℃, air circulation is kept during drying, excessive volatilization of components in the essence can be prevented by controlling the drying temperature, and waste of raw material components is prevented, the precipitate C obtained in the step S6 is stored at a constant temperature for 4 hours, the temperature is 46 ℃, then auxiliary materials are added, microorganisms in the precipitate C can be fully fermented through the step of constant-temperature storage, so that the essence is more mellow, 6 parts of defoaming agent is added in the step S4 during mixing, the raw materials are added while stirring is performed when the raw materials are added, and the stirring time is 40 minutes.
In the description herein, it is noted that relational terms such as first and second, and the like, are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. The preparation method of the perfume type essence with lasting fragrance is characterized by comprising the following steps:
s1: preparing raw materials, 20-50 parts of deionized water, 12-40 parts of passion fruit, 20-30 parts of dried rose petals, 2-8 parts of dried tulip petals, 3-6 parts of dried orchid, 30-60 parts of a composite solvent, 10-28 parts of auxiliary materials, 2-14 parts of whitening talcum powder, 8-22 parts of absolute ethyl alcohol and 8-16 parts of microcapsule essence;
s2: grinding and dissolving, namely putting the passion fruit, the rose petal, the tulip petal and the orchid in a ball mill for grinding for 30-50 minutes, then screening to remove impurities, adding a composite solvent and deionized water, stirring and mixing to obtain a mixture A, screening by using a 200-mesh and 500-mesh screen, heating while stirring and mixing, and keeping the constant temperature at 40-60 ℃;
s3: standing and drying, standing the obtained mixture A for 10-20 minutes, and then drying at high temperature to obtain a mixture B;
s4: mixing, namely putting the whitening talcum powder, the absolute ethyl alcohol, the microcapsule essence and the mixture B into a stirrer for stirring, wherein the stirring speed is controlled to be 1800 r/min;
s5: ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion for 30-50 minutes, standing for 10-30 minutes, and collecting the precipitate C at the lower layer after standing;
s6: adding auxiliary materials, adding the auxiliary materials and the precipitate C into a stirrer, and stirring for 10-25 minutes to obtain a mixture D;
s7: drying again, namely putting the mixture D into a drying chamber for vacuum freeze drying, and then grinding to obtain a finished product;
s8: collecting and packaging, and packaging the finished product under aseptic condition for later use.
2. The method for preparing the perfume type essence with lasting fragrance according to claim 1, wherein the compound solvent in the S1 is a mixture of propylene glycol, dichloromethane, menthyl lactate and diethyl ether, and the ratio of the propylene glycol: dichloromethane: menthyl lactate: ethyl ether 1-3:2-6:3-5: 1-4.
3. The method for preparing the perfume type essence with lasting fragrance according to claim 2, wherein the auxiliary materials in S6 are one or more of schizandrol, cassia seed alcohol, cedrol and fatty alcohol, and the auxiliary materials are ground, sieved after grinding, impurities are removed, and then ultraviolet sterilization treatment is performed before the auxiliary materials are added.
4. The method for preparing perfume type essence with lasting fragrance according to claim 1, wherein the microcapsule essence in S4 is one or more of passion fruit microcapsule essence, rose petal microcapsule essence, tulip petal microcapsule essence, orchid microcapsule essence and apple microcapsule essence.
5. The method of claim 4, wherein menthol and the mint essential oil are added in the step of mixing in the step of S2.
6. The method for preparing perfume type essence with lasting fragrance according to claim 1, wherein the temperature for high temperature drying in S3 is 40-70 ℃, and air circulation is maintained during drying.
7. The method for preparing perfume type essence with lasting fragrance according to claim 1, wherein the precipitate C obtained in S6 is first preserved at constant temperature of 30-60 deg.C for 2-5 hours, and then added with adjuvants.
8. The method for preparing a perfume type essence having a long lasting fragrance according to claim 1, wherein 2 to 8 parts of the antifoaming agent are added to S4 during the mixing, and the raw materials are added while stirring during the mixing, wherein the stirring time is 20 to 40 minutes.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115226876A (en) * | 2022-05-18 | 2022-10-25 | 广州芬豪香精有限公司 | Preparation method of composite essence |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101870922A (en) * | 2009-04-27 | 2010-10-27 | 巧立永 | Method for preparing essence from tulip and Chinese sacred lily |
| CN101870838A (en) * | 2009-04-21 | 2010-10-27 | 袁长常 | Method for preparing asparagus fern and violet essence-containing coating |
| CN104611136A (en) * | 2014-12-24 | 2015-05-13 | 杨秋慧 | Cigarette essence prepared by utilization of passion fruit and preparing method thereof |
| KR20160092829A (en) * | 2015-01-28 | 2016-08-05 | 천양피앤비 주식회사 | Method for manufacturing micro-capsules having long lasting aromatic |
| CN106137833A (en) * | 2016-07-14 | 2016-11-23 | 唐虎 | The preparation method of perfume |
| CN106580746A (en) * | 2016-12-24 | 2017-04-26 | 杭州心悦化妆品有限公司 | Perfume with long fragrance holding time |
| CN106580775A (en) * | 2016-12-11 | 2017-04-26 | 戴琪 | Preparation method of long-lasting refreshing consciousness-restoring balsam |
| CN106937920A (en) * | 2017-03-17 | 2017-07-11 | 上海名仕新材料有限公司 | Lasting high stability plant perfume of a kind of fragrant effect and preparation method thereof |
| CN107267289A (en) * | 2017-07-14 | 2017-10-20 | 新疆郁金香生物科技有限公司 | A kind of extracting method of root tuber of aromatic turmeric essential oil |
| KR20200085068A (en) * | 2019-01-04 | 2020-07-14 | (주)이미인 | Oil-in-water type cosmetic composition comprising petal |
-
2021
- 2021-07-13 CN CN202110787446.3A patent/CN113462473A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101870838A (en) * | 2009-04-21 | 2010-10-27 | 袁长常 | Method for preparing asparagus fern and violet essence-containing coating |
| CN101870922A (en) * | 2009-04-27 | 2010-10-27 | 巧立永 | Method for preparing essence from tulip and Chinese sacred lily |
| CN104611136A (en) * | 2014-12-24 | 2015-05-13 | 杨秋慧 | Cigarette essence prepared by utilization of passion fruit and preparing method thereof |
| KR20160092829A (en) * | 2015-01-28 | 2016-08-05 | 천양피앤비 주식회사 | Method for manufacturing micro-capsules having long lasting aromatic |
| CN106137833A (en) * | 2016-07-14 | 2016-11-23 | 唐虎 | The preparation method of perfume |
| CN106580775A (en) * | 2016-12-11 | 2017-04-26 | 戴琪 | Preparation method of long-lasting refreshing consciousness-restoring balsam |
| CN106580746A (en) * | 2016-12-24 | 2017-04-26 | 杭州心悦化妆品有限公司 | Perfume with long fragrance holding time |
| CN106937920A (en) * | 2017-03-17 | 2017-07-11 | 上海名仕新材料有限公司 | Lasting high stability plant perfume of a kind of fragrant effect and preparation method thereof |
| CN107267289A (en) * | 2017-07-14 | 2017-10-20 | 新疆郁金香生物科技有限公司 | A kind of extracting method of root tuber of aromatic turmeric essential oil |
| KR20200085068A (en) * | 2019-01-04 | 2020-07-14 | (주)이미인 | Oil-in-water type cosmetic composition comprising petal |
Non-Patent Citations (1)
| Title |
|---|
| 曾晓鹰等: "《卷烟调香体系构建——以云烟品牌为例》", 陕西师范大学出版总社有限公司, pages: 172 - 174 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115226876A (en) * | 2022-05-18 | 2022-10-25 | 广州芬豪香精有限公司 | Preparation method of composite essence |
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