CN108969404A - A kind of preparation method of the mixed fragrant cold-type yellow (clear) essential oil perfume of peppermint lemon bergamot - Google Patents

A kind of preparation method of the mixed fragrant cold-type yellow (clear) essential oil perfume of peppermint lemon bergamot Download PDF

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Publication number
CN108969404A
CN108969404A CN201710395244.8A CN201710395244A CN108969404A CN 108969404 A CN108969404 A CN 108969404A CN 201710395244 A CN201710395244 A CN 201710395244A CN 108969404 A CN108969404 A CN 108969404A
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Prior art keywords
perfume
lemon
bergamot
moschus
peppermint
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CN201710395244.8A
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Chinese (zh)
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闫战军
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Individual
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Individual
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Priority to CN201710395244.8A priority Critical patent/CN108969404A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations

Abstract

The invention discloses a kind of preparation methods of the mixed fragrant cold-type yellow (clear) essential oil perfume of peppermint lemon bergamot, are made of Peppermint essential oil, lemon, Bergamot, Moschus, 95% top grade glutinous rice edible alcohol, pure water;Peppermint volatility is high, fragrance is clearly cooled off oneself, with refrigerant and quelling effect, lemon volatility is high, with pure and fresh fruity, based on 3 kinds of compound perfume, the fixastive of low volatility Moschus group cost perfume, the feeling that preceding taste is clearly cooled off oneself to people, increase mature clean hygiene glamour, attract attention, middle taste shows to mix the refrigerant fragrant hybrid agent fragrance indistinct for main Moschus, after 8~10hr, taste perfume under the action of Moschus hearing the fragrance remaining time on fragrant paper with temperature change is 5~7 days afterwards, it is lasting with lasting, the advantages of improving social life grade.

Description

A kind of preparation method of the mixed fragrant cold-type yellow (clear) essential oil perfume of peppermint lemon bergamot
Technical field
The present invention relates to the technical field of all natural perfume, the mixed fragrant cold-type yellow (clear) essential oil of espespecially a kind of peppermint lemon bergamot is fragrant The preparation method of water.
Background technique
Country's perfume is generally used compound essence preparation at present, and fragrance is mainly by cyclamen aldehyde, n-octaldehyde, dihydro jasmine The proportions such as ketone, cyclopentadecanone, geranyl acetate, santalyl acetate are modulated, and these are matched by synthesizing aldehyde, ketone, esters The simulation fragrance of system is non-natural flower aroma, these chemical fragrance can make some people feel pungent dizzy and contradict, and is in addition sprayed It also has allergy and the negative interaction unfavorable to health, and compound essence is although at low cost, but has widened and world-renowned perfume Class, and use plant fragrance essential oil perfume have the natural fragrance of a flower, ingredient is healthier, safer, General Promotion The grade of social life.
Summary of the invention
A kind of preparation method of the mixed fragrant cold-type yellow (clear) essential oil perfume of peppermint lemon bergamot, using Peppermint essential oil, lemon, Bergamot, Moschus, 95% top grade glutinous rice edible alcohol, pure water are made, and the refrigerant fragrant and lemon bergamot with peppermint is clear New Rutaceae fruit flavor, lasting is lasting, improves the purpose of social life grade.
To achieve the goals above, the technical solution of the invention is as follows: a kind of mixed fragrant cold-type yellow (clear) of peppermint lemon bergamot The component of essential oil perfume: Peppermint essential oil 6.0%~8.0%, lemon 3.0%~5.0%, Bergamot 4.5%~5.0%, musk deer Perfume 1.0%~1.5%, 95% top grade glutinous rice edible alcohol (BG384-81) 65.0%~67.0%, pure water (TDS < 10ppm) 16.0% ~18.0%.
Preparation step is as follows:
(1) alcohol is aged: the glutinous rice alcohol of formula rate total amount 94.0% is taken, peppermint, lemon, Bergamot each 1.0% is put into, Moschus 0.3% stirs 15~30min with stainless steel blender, pours into stainless steel or not good merchantable glass container, close at 15 DEG C Envelope is placed 12 months;
(2) fragrance is mixed and is aged: after remaining peppermint, lemon, Bergamot, Moschus are mixed, formula rate total amount is added 6.0% glutinous rice alcohol stirs 15~30min with stainless steel blender, pours into stainless steel or not good merchantable glass container, 15 Sealing ageing 12 months at DEG C;
(3) it mixes: the alcohol after ageing, the mixing fragrance after ageing and pure water being mixed in proportion, with stainless steel blender 15~30min is stirred, is poured into stainless steel or not good merchantable glass container, ageing is sealed at 15 DEG C, the impurity in Moschus is allowed to fill Fractional precipitation, to reach the clarity of liquid, the mixing fragrance in aging period switchs to fine and smooth soft, digestion time by coarse gradually 24 months;
(4) cooling: mixed liquor being placed in -5 DEG C of freezings, wax insoluble in fragrance is precipitated out;
(5) it filters: using filter press, and super-cell is added with adsorption precipitation particle, prevent precipitate occlusion filter cloth hole Perfume is cooled to 0~3 DEG C after filter aid is added, and restored after maintaining this temperature, sediment to filter out in filtering to room by road It is Clear & Transparent to reach perfume using a fine-mesh cloths filtering for temperature;
(6) it mixes colours: being needed to modulate perfume color with oil-based liquid food grade pigment according to market;
(7) it bottles: finished product perfume being fitted into the glass scent flask of customization, reserve 10~15% gaps of bottle volume, prevent by swollen Swollen and broken bottle.
Peppermint, lemon, Bergamot in the mixed fragrant cold-type yellow (clear) essential oil perfume of peppermint lemon bergamot of the present invention with After Moschus is mixed and is aged, the pungent stiff sense of alcohol is reduced, and Moschus makes peppermint, lemon similar to the animal odor type of all sorts of flowers perfume Lemon, the mixing fragrance stereovision enhancing of bergamot and lasting are lasting, are saved using 95% top grade glutinous rice edible alcohol (BG384-81) The purifying pre-treatment step of alcohol, glutinous rice alcohol are more gentle than the smell of jowar or corn alcohol, and when preparing perfume, energy will be certainly Body smell minimizes, and is more suitable for protruding various fragrance aromas, in addition in edible alcohol without containing the benzene class toxic to human body and Methanol reduces stimulation and sensitivity to skin, is more advantageous to health, and the preparation pure water that water is that hyperfiltration obtains saves Water has been gone to go the pre-treatment step of metal ion, the use of glutinous rice alcohol and pure water improves perfume quality, safety, saves Pre-treatment step reduces cost, improves efficiency.
Peppermint lemon bergamot of the present invention mixes the characteristics of fragrant cold-type yellow (clear) essential oil perfume: peppermint volatility is high, and fragrance is clear It is refreshing pleasantly cool, there is refrigerant and quelling effect, lemon volatility is high, has pure and fresh fruity, peppermint lemon Buddhist of the present invention The mixed fragrant cold-type yellow (clear) essential oil perfume of hand mandarin orange uses based on 3 kinds of compound perfume, the fixastive of low volatility Moschus group cost perfume, preceding taste To the feeling that people clearly cools off oneself, increase mature clean hygiene glamour, attract attention, middle taste shows to mix refrigerant fragrant for main musk deer Fragrant indistinct hybrid agent fragrance, after 8~10hr, rear taste under the action of Moschus perfume hear the fragrance remaining time on fragrant paper with Temperature change is 5~7 days.
Specific embodiment
Embodiment 1
(1) component: Peppermint essential oil 6.0%, lemon 5.0%, Bergamot 4.5%, Moschus 1.5%, 95% top grade glutinous rice are edible Alcohol (BG384-81) 65.0%, pure water (TDS < 10ppm) 18.0%.
(2) preparation step is as follows:
1. alcohol is aged: the glutinous rice alcohol of formula rate total amount 94.0% is taken, peppermint, lemon, Bergamot each 1.0% is put into, Moschus 0.3% stirs 15~30min with stainless steel blender, pours into stainless steel or not good merchantable glass container, close at 15 DEG C Envelope is placed 12 months;
2. fragrance mixes and ageing: after remaining peppermint, lemon, Bergamot, Moschus are mixed, formula rate total amount is added 6.0% glutinous rice alcohol stirs 15~30min with stainless steel blender, pours into stainless steel or not good merchantable glass container, 15 Sealing ageing 12 months at DEG C;
3. mixing: the alcohol after ageing, the mixing fragrance after ageing and pure water being mixed in proportion, stirred with stainless steel blender 15~30min is mixed, is poured into stainless steel or not good merchantable glass container, ageing is sealed at 15 DEG C, makes the impurity in Moschus abundant Precipitating, to reach the clarity of liquid, the mixing fragrance in aging period switchs to fine and smooth soft, digestion time 24 by coarse gradually A month;
4. cooling down: mixed liquor being placed in -5 DEG C of freezings, wax insoluble in fragrance is precipitated out;
5. filtering: using filter press, and super-cell is added with adsorption precipitation particle, prevent precipitate occlusion filter cloth hole Perfume is cooled to 0~3 DEG C after filter aid is added, and restored after maintaining this temperature, sediment to filter out in filtering to room by road It is Clear & Transparent to reach perfume using a fine-mesh cloths filtering for temperature;
6. toning: being needed to modulate perfume color with oil-based liquid food grade pigment according to market;
7. bottling: finished product perfume being fitted into the glass scent flask of customization, reserve 10~15% gaps of bottle volume, prevent by swollen Swollen and broken bottle.
Embodiment 2
(1) component: Peppermint essential oil 8.0%, lemon 3.0%, Bergamot 5.0%, Moschus 1.0%, 95% top grade glutinous rice are edible Alcohol (BG384-81) 67.0%, pure water (TDS < 10ppm) 16.0%.
(2) preparation step is as follows:
1. alcohol is aged: the glutinous rice alcohol of formula rate total amount 94.0% is taken, peppermint, lemon, Bergamot each 1.0% is put into, Moschus 0.3% stirs 15~30min with stainless steel blender, pours into stainless steel or not good merchantable glass container, close at 15 DEG C Envelope is placed 12 months;
2. fragrance mixes and ageing: after remaining peppermint, lemon, Bergamot, Moschus are mixed, formula rate total amount is added 6.0% glutinous rice alcohol stirs 15~30min with stainless steel blender, pours into stainless steel or not good merchantable glass container, 15 Sealing ageing 12 months at DEG C;
3. mixing: the alcohol after ageing, the mixing fragrance after ageing and pure water being mixed in proportion, stirred with stainless steel blender 15~30min is mixed, is poured into stainless steel or not good merchantable glass container, ageing is sealed at 15 DEG C, makes the impurity in Moschus abundant Precipitating, to reach the clarity of liquid, the mixing fragrance in aging period switchs to fine and smooth soft, digestion time 24 by coarse gradually A month;
4. cooling down: mixed liquor being placed in -5 DEG C of freezings, wax insoluble in fragrance is precipitated out;
5. filtering: using filter press, and super-cell is added with adsorption precipitation particle, prevent precipitate occlusion filter cloth hole Perfume is cooled to 0~3 DEG C after filter aid is added, and restored after maintaining this temperature, sediment to filter out in filtering to room by road It is Clear & Transparent to reach perfume using a fine-mesh cloths filtering for temperature;
6. toning: being needed to modulate perfume color with oil-based liquid food grade pigment according to market;
7. bottling: finished product perfume being fitted into the glass scent flask of customization, reserve 10~15% gaps of bottle volume, prevent by swollen Swollen and broken bottle.
The above, embodiment is only that preferred embodiments of the present invention will be described, not to of the invention Range is defined, and under the premise of not departing from the spirit of the technology of the present invention, this field engineers and technicians are to skill of the invention The various changes and improvements that art scheme is made, should fall within the scope of protection determined by the claims of the present invention.

Claims (2)

1. the preparation method of the mixed fragrant cold-type yellow (clear) essential oil perfume of a kind of peppermint lemon bergamot, it is characterized in that: group is divided into Peppermint essential oil 6.0%~8.0%, lemon 3.0%~5.0%, Bergamot 4.5%~5.0%, Moschus 1.0%~1.5%, 95% top grade glutinous rice Edible alcohol (BG384-81) 65.0%~67.0%, pure water (TDS < 10ppm) 16.0%~18.0%.
2. preparation step is as follows:
(1) alcohol is aged: the glutinous rice alcohol of formula rate total amount 94.0% is taken, peppermint, lemon, Bergamot each 1.0% is put into, Moschus 0.3% stirs 15~30min with stainless steel blender, pours into stainless steel or not good merchantable glass container, close at 15 DEG C Envelope is placed 12 months;
(2) fragrance is mixed and is aged: after remaining peppermint, lemon, Bergamot, Moschus are mixed, formula rate total amount is added 6.0% glutinous rice alcohol stirs 15~30min with stainless steel blender, pours into stainless steel or not good merchantable glass container, 15 Sealing ageing 12 months at DEG C;
(3) it mixes: the alcohol after ageing, the mixing fragrance after ageing and pure water being mixed in proportion, with stainless steel blender 15~30min is stirred, is poured into stainless steel or not good merchantable glass container, ageing is sealed at 15 DEG C, the impurity in Moschus is allowed to fill Fractional precipitation, to reach the clarity of liquid, the mixing fragrance in aging period switchs to fine and smooth soft, digestion time by coarse gradually 24 months;
(4) cooling: mixed liquor being placed in -5 DEG C of freezings, wax insoluble in fragrance is precipitated out;
(5) it filters: using filter press, and super-cell is added with adsorption precipitation particle, prevent precipitate occlusion filter cloth hole Perfume is cooled to 0~3 DEG C after filter aid is added, and restored after maintaining this temperature, sediment to filter out in filtering to room by road It is Clear & Transparent to reach perfume using a fine-mesh cloths filtering for temperature;
(6) it mixes colours: being needed to modulate perfume color with oil-based liquid food grade pigment according to market;
(7) it bottles: finished product perfume being fitted into the glass scent flask of customization, reserve 10~15% gaps of bottle volume, prevent by swollen Swollen and broken bottle.
CN201710395244.8A 2017-05-31 2017-05-31 A kind of preparation method of the mixed fragrant cold-type yellow (clear) essential oil perfume of peppermint lemon bergamot Pending CN108969404A (en)

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Application Number Priority Date Filing Date Title
CN201710395244.8A CN108969404A (en) 2017-05-31 2017-05-31 A kind of preparation method of the mixed fragrant cold-type yellow (clear) essential oil perfume of peppermint lemon bergamot

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112391233A (en) * 2020-11-10 2021-02-23 上海应用技术大学 Citron-lemon essence and preparation method thereof
CN112516012A (en) * 2020-12-22 2021-03-19 茂名市瑜丰沉香创意产业有限公司 Soothing agilawood compound perfume and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112391233A (en) * 2020-11-10 2021-02-23 上海应用技术大学 Citron-lemon essence and preparation method thereof
CN112516012A (en) * 2020-12-22 2021-03-19 茂名市瑜丰沉香创意产业有限公司 Soothing agilawood compound perfume and preparation method thereof

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