CN107898695B - Preparation method of tea toothpaste - Google Patents
Preparation method of tea toothpaste Download PDFInfo
- Publication number
- CN107898695B CN107898695B CN201711306700.3A CN201711306700A CN107898695B CN 107898695 B CN107898695 B CN 107898695B CN 201711306700 A CN201711306700 A CN 201711306700A CN 107898695 B CN107898695 B CN 107898695B
- Authority
- CN
- China
- Prior art keywords
- tea
- nano
- parts
- toothpaste
- particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
Abstract
A preparation method of tea toothpaste belongs to the technical field of tea deep processing. Which comprises the following steps: crushing tea raw materials into tea powder of 100-500nm at low temperature to obtain nano tea powder; processing tea raw materials by a food oriented manufacturing technology to obtain a high-activity tea extract; processing the nano tea powder and/or the high-activity tea extract into nano tea particles by a microcapsule preparation technology; adding the nano tea particles into a toothpaste base material; and filling the uniformly stirred paste into a vertical pressing type package or other package forms to prepare the tea toothpaste product. The toothpaste has fresh and fine taste, and has effects of strengthening gum, protecting teeth, resisting inflammation, preventing oral bacteria breeding, etc., and especially greatly improves antibacterial effect of toothpaste.
Description
Technical Field
The invention belongs to the technical field of tea deep processing, and particularly relates to a preparation method of tea toothpaste.
Background
The toothpaste is an important oral care product for cleaning teeth, maintaining oral hygiene and preventing oral diseases, and is closely related to the daily life of people. The toothpaste industry is one of the important daily chemical industries, the production level of the toothpaste industry reflects the development of the national industrial civilization, and marks and influences the level of the consumption level of people. With the development of economy and the improvement of living standard, people need the toothpaste with the effects of bacteriostasis, diminishing inflammation, whitening, removing dirt, strengthening gum, protecting teeth, repairing and preventing oral diseases and the like besides the basic functions of cleaning teeth, removing halitosis and the like, and the market products of the toothpaste are more and more abundant. At present, in order to achieve certain effects and favor of consumers, certain chemosynthetic industrial raw materials or synthetic essence and certain medicinal ingredients are added into toothpaste, certain potential safety hazards exist, the situation is contrary to the growing health consciousness of people, the requirements of the toothpaste market on the selection of raw materials and auxiliary materials are higher and higher, and the demand of products with certain natural health care effects is larger.
Tea leaves contain more than 350 organic compounds and more than 700 aromatic substances, and the substances have various nutritional values and pharmacological effects. The tea polyphenol has strong effects of preventing dental caries and resisting inflammation, and especially has ideal effects of reducing swelling of gum, resisting inflammation, reducing internal heat and the like by the white tea essence factor. In recent years, tea toothpaste such as tea toothpaste brands of dark tea, Konjac, Jiajieshei, Qingyi beauty and the like is also available in the market. The CN102764207A, CN100584309C, CN102085166A, CN02106802A and other patents disclose some tea toothpaste and a preparation method thereof, extracts such as green tea, Pu' er tea and the like are simply added, although the tea toothpaste has the concept of natural tea, the effects of diminishing inflammation and resisting bacteria, removing stains and dirt, refreshing breath, reducing decayed teeth and the like are not obvious, the use of some synthetic essences and chemical raw materials is not excluded, some processes are complex, the stability of the product is poor, and a product which is really natural, healthy, highly effective in diminishing inflammation, refreshing breath and has tea health care factors is extremely needed in the market.
Disclosure of Invention
Aiming at the problems in the prior art, the invention aims to design and provide a technical scheme of a preparation method of tea toothpaste. The tea toothpaste has fresh and fine taste, and has effects of strengthening gum, protecting teeth, resisting inflammation, preventing oral bacteria breeding, etc.
The preparation method of the tea toothpaste is characterized by comprising the following steps of:
1) crushing tea raw materials into tea powder of 100-500nm at low temperature to obtain nano tea powder;
2) processing tea raw materials by a food oriented manufacturing technology to obtain a high-activity tea extract;
3) processing the nano tea powder and/or the high-activity tea extract into nano tea particles by a microcapsule preparation technology;
4) adding the nano tea particles into a toothpaste base material according to the following parts by weight: 0.1-4 parts of nano tea particles, 15-40 parts of wetting agent, 20-50 parts of abrasive, 1-5 parts of surfactant, 0.1-0.5 part of sweetening agent, 1-6 parts of thickening agent and 8-40 parts of deionized water;
5) and (3) filling the paste uniformly stirred in the step 3) into a vertical pressing type package or other package forms to prepare the tea toothpaste product.
The preparation method of the tea toothpaste is characterized in that the tea leaves in the step 1) are dry tea prepared by picking high-quality and safe fresh tea leaves according to a six-tea process; or scented tea prepared by multiple scenting with flos Jasmini sambac, flos Rosae Rugosae, and flos Magnoliae; or the high-quality tea leaves with more than two levels of standard sold in the market.
The preparation method of the tea toothpaste is characterized in that the preparation of the nano tea powder in the step 1) is specifically as follows: pre-freezing tea leaves for 15-300 seconds by using liquid nitrogen, then performing multi-stage crushing by using a multi-dimensional high-energy nano impact ball mill, wherein the first-stage crushing is performed to 20-120 meshes, the second-stage crushing is performed to 10-150 mu m, the third-stage crushing is performed to 100-plus-material 500nm, and the constant temperature of the materials is controlled to be 5-20 ℃ by using jacket circulating cooling water.
The preparation method of the tea toothpaste is characterized in that the preparation of the high-activity tea extract in the step 2) is specifically as follows: tea leaves are subjected to multi-stage countercurrent extraction and directional extraction: the extraction temperature is 20-70 ℃, and the extraction time is 10-60 min; multi-stage membrane separation technology: the aperture of the primary membrane is 0.1-0.3nm, the aperture of the secondary membrane is 100-300KD, and the filtering temperature is 15-30 ℃; concentrating with DT membrane to 10-20Brix to obtain concentrated tea solution or lyophilizing to obtain high activity tea extract.
The preparation method of the tea toothpaste is characterized in that the preparation of the nano tea particles in the step 3) is specifically as follows: adding 5-30 parts of one or two of porous modified starch and gamma-cyclodextrin, 1-5 parts of one or more of sodium lauryl sulfate, monoglyceride and propylene glycol into nano tea powder or high-activity tea extract, shearing, homogenizing, embedding, and performing ultrasonic microemulsion to obtain nano particles, wherein the microemulsion rotation speed is 300-1200rpm, and the ultrasonic frequency is 20-60 KHz.
The wetting agent, abrasive, surfactant, sweetener and thickener used in the present application are all conventional adjuvants in toothpaste.
The preparation method of the tea toothpaste is reasonable in design, and the nano tea particles and/or the high-activity tea extract prepared under specific conditions are added into the toothpaste, so that the toothpaste is fresh and fine in taste, has the effects of strengthening and protecting the gums and the teeth, resisting inflammation efficiently, preventing oral bacteria from breeding and the like, and particularly greatly improves the antibacterial effect of the toothpaste.
Detailed Description
The present invention is further illustrated by the following examples.
Example 1
1) Purchasing 3kg of special grade jasmine white tea of tea company, pre-freezing with liquid nitrogen for 60 seconds, then performing multi-stage crushing by a multi-dimensional high-energy nano impact ball milling machine, performing first-stage crushing to 100 meshes, performing second-stage crushing to 100um, performing third-stage crushing to 250nm, and controlling the constant temperature of materials to 15 ℃ by using jacket circulating cooling water to obtain nano tea powder;
2) adding 18 parts of porous modified starch, 2 parts of sodium lauryl sulfate and 1 part of propylene glycol into the nano tea powder prepared in the step 1), shearing, homogenizing and embedding, and then carrying out ultrasonic micro-emulsification to obtain nano particles, wherein the rotation speed of the micro-emulsion is 800rpm, and the ultrasonic frequency is 60KHz, so as to obtain the nano tea particles;
3) uniformly mixing the nano tea particles obtained in the step 2) with the following toothpaste, wherein the raw materials comprise the following components in parts by weight: 0.5 part of nano tea particles, 40 parts of wetting agent, 30 parts of abrasive, 4 parts of surfactant, 0.5 part of sweetening agent, 6 parts of thickening agent and 19 parts of deionized water;
4) and (3) filling the paste uniformly stirred in the step 3) into a vertical pressing type package or other package forms to prepare the tea toothpaste product.
The bacteriostatic effect is shown in the following table:
note: the toothpaste ingredients prepared from the conventional ultrafine tea powder were the same as those in example 1 except for the conventional ultrafine tea powder.
Example 2
1) Picking fresh leaves of No. 43 variety of Hangzhou Meijia depressed dragon well, and stir-frying with the dragon well tea process to obtain West lake dragon well tea;
2) pre-freezing the tea leaves in the step 1) for 90 seconds by using liquid nitrogen, then performing multi-stage crushing by using a multi-dimensional high-energy nano impact ball milling machine, wherein the first-stage crushing is performed to 120 meshes, the second-stage crushing is performed to 150 mu m, the third-stage crushing is performed to 300nm, and the constant temperature of the materials is controlled by using jacket circulating cooling water to be 10 ℃ to obtain nano tea powder;
3) adding 10 parts of gamma cyclodextrin, 3 parts of sodium lauryl sulfate and 2 parts of propylene glycol into the nano tea powder prepared in the step 2), shearing, homogenizing and embedding, and then carrying out ultrasonic micro-emulsification to obtain nano particles, wherein the micro-emulsion rotation speed is 1200rpm, and the ultrasonic frequency is 20KHz, so as to obtain the nano tea particles;
4) uniformly mixing the nano tea particles obtained in the step 3) with the following toothpaste, wherein the raw materials comprise the following components in parts by weight: 4 parts of nano tea particles, 30 parts of wetting agent, 30 parts of abrasive, 4 parts of surfactant, 0.1 part of sweetening agent, 1.9 parts of thickening agent and 30 parts of deionized water;
5) and (3) filling the paste uniformly stirred in the step (4) into a vertical pressing type package or a package in other package forms to prepare the tea toothpaste product.
The mouthfeel and the antibacterial effect of the toothpaste are shown in the following table:
note: the toothpaste ingredients prepared from the conventional ultrafine tea powder were the same as those in example 2 except for the conventional ultrafine tea powder.
Example 3
1) Picking fresh leaves with one bud and two leaves of the Zhejiang Lin' an Ying frost variety, and preparing black tea by the processes of withering, fermentation, drying and the like;
2) pre-freezing the tea leaves in the step 1) by using liquid nitrogen for 15 seconds, then performing multi-stage crushing by using a multi-dimensional high-energy nano impact ball milling machine, wherein the first-stage crushing is performed to 20 meshes, the second-stage crushing is performed to 10 mu m, the third-stage crushing is performed to 200nm, and the constant temperature of the materials is controlled by using jacket circulating cooling water to be 5 ℃ to obtain nano tea powder;
3) adding 5 parts of porous modified starch, 3 parts of gamma cyclodextrin and 5 parts of sodium lauryl sulfate into the nano tea powder prepared in the step 2), shearing, homogenizing and embedding, and then carrying out ultrasonic micro-emulsification to obtain nano particles, wherein the micro-emulsion rotation speed is 300rpm, and the ultrasonic frequency is 48KHz, so as to obtain the nano tea particles;
4) uniformly mixing the nano tea particles obtained in the step 3) with the following toothpaste, wherein the raw materials comprise the following components in parts by weight: 1 part of nano tea particles, 15 parts of wetting agent, 50 parts of abrasive, 4.5 parts of surfactant, 0.5 part of sweetening agent, 6 parts of thickening agent and 26 parts of deionized water;
5) and (3) filling the paste uniformly stirred in the step (4) into a vertical pressing type package or a package in other package forms to prepare the tea toothpaste product.
The mouthfeel and the antibacterial effect of the toothpaste are shown in the following table:
note: the toothpaste ingredients prepared from the conventional ultrafine tea powder were the same as those in example 3 except for the conventional ultrafine tea powder.
Example 4
1) Purchasing royal Puer tea (aged for three years) of Yunnan division of Chinese tea, pre-freezing with liquid nitrogen for 300 s, performing multi-stage pulverization by a multi-dimensional high-energy nano impact ball mill, performing primary pulverization to 120 meshes, performing secondary pulverization to 150um, performing tertiary pulverization to 500nm, and controlling the constant temperature of the materials to be 20 ℃ by using jacket circulating cooling water;
2) adding 30 parts of porous modified starch and 5 parts of propylene glycol into the nano tea powder prepared in the step 1), shearing, homogenizing and embedding, and then carrying out ultrasonic micro-emulsification to obtain nano particles, wherein the micro-emulsion rotation speed is 1000rpm, and the ultrasonic frequency is 48KHz, so as to obtain nano tea particles;
3) uniformly mixing the nano tea particles obtained in the step 2) with the following toothpaste, wherein the raw materials comprise the following components in parts by weight: 2 parts of nano tea particles, 40 parts of wetting agent, 30 parts of abrasive, 2 parts of surfactant, 0.2 part of sweetening agent, 1.8 parts of thickening agent and 24 parts of deionized water;
4) and (3) filling the paste uniformly stirred in the step 3) into a vertical pressing type package or other package forms to prepare the tea toothpaste product.
The bacteriostatic effect is shown in the following table:
note: the toothpaste ingredients prepared from the conventional ultrafine tea powder were the same as those in example 4 except for the conventional ultrafine tea powder.
Example 5
1) The method comprises the following steps of purchasing faint scent oolong tea of Fujian Bama group, and performing multi-stage countercurrent extraction and directional extraction on the tea: the extraction temperature is 50 ℃, and the extraction time is 30 min; multi-stage membrane separation technology: the aperture of the primary membrane is 0.2nm, the aperture of the secondary membrane is 200KD, and the filtering temperature is 25 ℃; concentrating with DT membrane to 15Brix to obtain concentrated tea solution or lyophilizing to obtain high activity tea extract;
2) adding 30 parts of porous modified starch and 5 parts of propylene glycol into the high-activity tea extract prepared in the step 1), shearing, homogenizing and embedding, and then carrying out ultrasonic micro-emulsification to obtain nano-particles, wherein the rotation speed of the micro-emulsion is 500rpm, and the ultrasonic frequency is 30KHz, so as to obtain the nano-tea particles;
3) uniformly mixing the nano tea particles obtained in the step 2) with the following toothpaste, wherein the raw materials comprise the following components in parts by weight: 0.2 part of nano tea particles, 30 parts of wetting agent, 25 parts of abrasive, 1.5 parts of surfactant, 0.3 part of sweetening agent, 3 parts of thickening agent and 40 parts of deionized water;
4) and (3) filling the paste uniformly stirred in the step 3) into a vertical pressing type package or other package forms to prepare the tea toothpaste product.
The mouthfeel and the antibacterial effect of the toothpaste are shown in the following table:
note: the toothpaste ingredients prepared from the conventional ultrafine tea powder were the same as those in example 5 except for the conventional ultrafine tea powder.
Example 6
1) The method comprises the following steps of purchasing faint scent oolong tea of Fujian Bama group, and performing multi-stage countercurrent extraction and directional extraction on the tea: the extraction temperature is 50 ℃, and the extraction time is 30 min; multi-stage membrane separation technology: the aperture of the primary membrane is 0.2nm, the aperture of the secondary membrane is 200KD, and the filtering temperature is 25 ℃; concentrating with DT membrane to 15Brix to obtain concentrated tea solution or lyophilizing to obtain high activity tea extract;
2) purchasing fragrant oolong tea of Fujian Bama group, prefreezing with liquid nitrogen for 60 s, performing multi-stage pulverization by a multi-dimensional high-energy nano impact ball mill, pulverizing to 100 mesh at the first stage, pulverizing to 120um at the second stage, pulverizing to 400nm at the third stage, and controlling the constant temperature of the materials by using jacket circulating cooling water to 15 deg.C to obtain nano tea powder;
2) adding 30 parts of porous modified starch and 5 parts of propylene glycol into the high-activity tea extract prepared in the step 1) and the nano tea powder prepared in the step 2), shearing, homogenizing and embedding, and then carrying out ultrasonic micro-emulsification to obtain nano particles, wherein the micro-emulsion rotation speed is 500rpm, and the ultrasonic frequency is 30KHz, so as to obtain the nano tea particles;
3) uniformly mixing the nano tea particles obtained in the step 2) with the following toothpaste, wherein the raw materials comprise the following components in parts by weight: 0.2 part of nano tea particles, 30 parts of wetting agent, 25 parts of abrasive, 1.5 parts of surfactant, 0.3 part of sweetening agent, 3 parts of thickening agent and 40 parts of deionized water;
4) and (3) filling the paste uniformly stirred in the step 3) into a vertical pressing type package or other package forms to prepare the tea toothpaste product.
The mouthfeel and the antibacterial effect of the toothpaste are shown in the following table:
note: the toothpaste ingredients prepared using the conventional ultrafine tea powder were the same as those of example 6 except for the conventional ultrafine tea powder.
Claims (2)
1. The preparation method of the tea toothpaste is characterized by comprising the following steps of:
1) crushing tea raw materials into tea powder of 100-500nm at low temperature to obtain nano tea powder, wherein the preparation of the nano tea powder specifically comprises the following steps: pre-freezing tea leaves for 15-300 seconds by using liquid nitrogen, then performing multi-stage crushing by using a multi-dimensional high-energy nano impact ball mill, wherein the first-stage crushing is performed to 20-120 meshes, the second-stage crushing is performed to 10-150 mu m, the third-stage crushing is performed to 100-plus-material 500nm, and the constant temperature of the materials is controlled to be 5-20 ℃ by using jacket circulating cooling water;
2) processing tea raw materials by a food oriented manufacturing technology to obtain a high-activity tea extract, wherein the preparation of the high-activity tea extract specifically comprises the following steps: tea leaves are subjected to multi-stage countercurrent extraction and directional extraction: the extraction temperature is 20-70 ℃, and the extraction time is 10-60 min; multi-stage membrane separation technology: the aperture of the primary membrane is 0.1-0.3nm, the aperture of the secondary membrane is 100-300KD, and the filtering temperature is 15-30 ℃; concentrating with DT membrane to 10-20Brix to obtain concentrated tea solution or lyophilizing to obtain high activity tea extract;
3) processing nano tea powder and/or a high-activity tea extract into nano tea particles by using a microcapsule preparation technology, wherein the preparation of the nano tea particles specifically comprises the following steps: adding 5-30 parts of one or two of porous modified starch and gamma-cyclodextrin, 1-5 parts of one or more of sodium lauryl sulfate, monoglyceride and propylene glycol into nano tea powder or high-activity tea extract, shearing, homogenizing and embedding, and performing ultrasonic microemulsion to obtain nano particles, wherein the microemulsion rotation speed is 300-1200rpm, and the ultrasonic frequency is 20-60 KHz;
4) adding the nano tea particles into a toothpaste base material according to the following parts by weight: 0.1-4 parts of nano tea particles, 15-40 parts of wetting agent, 20-50 parts of abrasive, 1-5 parts of surfactant, 0.1-0.5 part of sweetening agent, 1-6 parts of thickening agent and 8-40 parts of deionized water;
5) and (3) filling the paste uniformly stirred in the step 3) into a vertical pressing type package or other package forms to prepare the tea toothpaste product.
2. The method for preparing tea toothpaste according to claim 1, wherein the tea leaves in step 1) are dry tea leaves obtained by picking fresh tea leaves with high quality and safety according to six major tea process; or scented tea prepared by multiple scenting of Laili flower, flos Rosae Rugosae, and flos Magnoliae; or the high-quality tea leaves with more than two levels of standard sold in the market.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711306700.3A CN107898695B (en) | 2017-12-11 | 2017-12-11 | Preparation method of tea toothpaste |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711306700.3A CN107898695B (en) | 2017-12-11 | 2017-12-11 | Preparation method of tea toothpaste |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107898695A CN107898695A (en) | 2018-04-13 |
| CN107898695B true CN107898695B (en) | 2021-04-06 |
Family
ID=61865120
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711306700.3A Active CN107898695B (en) | 2017-12-11 | 2017-12-11 | Preparation method of tea toothpaste |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107898695B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110664709A (en) * | 2019-11-13 | 2020-01-10 | 宜兴高等职业技术学校 | Natural shampoo |
| CN110680788A (en) * | 2019-11-20 | 2020-01-14 | 茗汲(浙江)生物科技有限公司 | Toothpaste containing tea extract and preparation process |
| CN111297790B (en) * | 2020-02-25 | 2023-02-17 | 暨南大学 | Application of tea outer vesicle |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105104590B (en) * | 2015-08-21 | 2019-08-13 | 中国农业科学院茶叶研究所 | Tealeaves flavor quality component foodization orientation manufacture Integration ofTechnology system and method |
| CN105748338A (en) * | 2015-11-27 | 2016-07-13 | 肖建国 | Toothpaste with dark tea extract and method for preparing toothpaste |
| CN105724627A (en) * | 2016-03-21 | 2016-07-06 | 中国农业科学院茶叶研究所 | Preparation method of low-agglomeration nanoscale tea powder |
-
2017
- 2017-12-11 CN CN201711306700.3A patent/CN107898695B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN107898695A (en) | 2018-04-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107898695B (en) | Preparation method of tea toothpaste | |
| KR101562560B1 (en) | Natural extract fermentation-maturity composition for preventing skin aging and improving skin wrinkle, Natural cosmetics containing that and Manufacturing method thereof | |
| CN103734474B (en) | Beautifying health-care tea and preparation method thereof | |
| KR101565778B1 (en) | Manufacturing Method of Antibiosis Soap Containing Xinc Oxide of Nano Size and Antibiosis Soap Thereof | |
| CN101416928A (en) | Matcha anti-senescence face mask added with superoxide dismutase and preparation method thereof | |
| CN101099547B (en) | Water soluble propolis extract with bioactivity and light-colored propolis extract | |
| CN106260268A (en) | A kind of eliminating toxin and beautifying the skin Herb Tea and preparation method thereof | |
| CN105078830A (en) | Natural preservative children plant sunscreen lotion and preparation method thereof | |
| CN109007163A (en) | A kind of lotus leaf bag bubble weight-reducing jasmine tea and preparation method thereof | |
| KR101239630B1 (en) | Soap and method for manufacturing thereof | |
| CN102423051A (en) | Preparation method for solanum tuberdsm powder | |
| CN107073053A (en) | The growth promoter of resident bacteria or intraoral flora improver and composition for oral cavity in non-pathogenic oral cavity | |
| KR20110118208A (en) | Oriental shampoo composition for scalp diseases and manufacturing process of oriental shampoo using the same | |
| CN107080168A (en) | A kind of vanilla method for making noodles | |
| CN101491488A (en) | Spot-removing facemask powder and production method thereof | |
| CN103642087A (en) | Rubber gloves with antibiotic and skin-care effects and preparation method thereof | |
| CN104248572A (en) | Lotus root-containing after-sun repair mask powder | |
| JP6271159B2 (en) | Skin external preparation composition containing honeysuckle vinegar extract | |
| CN104946434A (en) | Pure natural skin care perfumed soap and preparation method thereof | |
| CN107868733A (en) | A kind of sea cucumber perfumed soap and preparation method thereof | |
| CN106691975A (en) | Anti-allergy moisturized repair essence | |
| KR101423552B1 (en) | A composition for the treatment of xeroderma, and the method of manufacturing it | |
| CN106035800A (en) | Tea bag of tea capable of moistening skin and beautifying faces | |
| JP2002053434A (en) | Hair treatment and method for treating hair | |
| CN112315881A (en) | Collagen peptide mask liquid and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |