CN104611136A - Cigarette essence prepared by utilization of passion fruit and preparing method thereof - Google Patents
Cigarette essence prepared by utilization of passion fruit and preparing method thereof Download PDFInfo
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- CN104611136A CN104611136A CN201410813305.4A CN201410813305A CN104611136A CN 104611136 A CN104611136 A CN 104611136A CN 201410813305 A CN201410813305 A CN 201410813305A CN 104611136 A CN104611136 A CN 104611136A
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- passion fruit
- tobacco
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Abstract
The invention belongs to the field of daily essence processing, and particularly relates to cigarette essence prepared by utilization of passion fruit and a preparing method thereof. The essence is prepared by mixing following raw material components by weight: 20-30 parts of the passion fruit, 1-3 parts of rose petals, 1-3 parts of sweet osmanthus petals, 5-10 parts of ethyl acetate, 3-8 parts of butyl butyrate, 2-5 parts of ethyl 2-methylbutyrate, 10-15 parts of cinnamyl alcohol and 40-60 parts of ethanol. The essence prepared by the method has advantages of unique fragrance, good effects on smoke, a low cost, a simple preparation process, and the like. In addition, the deep-processing route of the industry of the passion fruit in China is broadened, the value of the passion fruit is increased, and the income of orchard workers is increased.
Description
Technical field
The present invention relates to a kind of daily essence manufacture field, especially a kind of flavouring essence for tobacco utilizing passion fruit to prepare and preparation method thereof.
Background technology
(passion fruit has another name called Herba Passiflorae Caeruleae to passion fruit, Purple Granadilla), passion fruit has strong unique perfume because the aroma component being permitted various fruits containing piscidia, mango, apple, pineapple etc. is described as " passion fruit ", acidity is higher, passion fruit fruit contains the aromatoising substance more than more than 132 kinds, be one of the most fragrant known fruit in the world, have the good reputation of " king of fruit juice ".A large amount of plantations is all had on China Guangdong, Guangxi, Hainan, Yunnan and other places.Passion fruit is rich in the multivitamins such as VC, mineral element, essential amino acid and has alkaloid and the Flavonoid substances of pharmaceutical use.Normal edible passion fruit has and produces refreshing effect to the mind, skin maintenance, anti-cancer, aid digestion, preventing phlegm from forming and stopping coughing, relief of constipation, invigorates blood circulation and keep fit, improve immune function of human body, enriching yin and nourishing kidney, Ginseng Extract, hypertension and hyperlipemia, effect of delaying senility.The root of passion fruit, stem, leaf have the effect such as anti-inflammatory analgetic, blood fat-reducing blood pressure-decreasing.
Flavouring essence for tobacco is redeployed by multiple spices, has certain odor type, can be directly used in the mixture of tobacco flavoring.At present, the tobacco aromatics using of China's cigarettes plus, general adopts two large classes: a class is natural extract spices, utilizes that contain in natural perfume or the potential natural component coordinated with flue gas; Another kind of is exactly synthetic perfume, utilizes coordinating with flue gas of synthesis, flue gas is had to the perfume monomer of certain effect.Separately or allocate the flavouring essence for tobacco made, although technique is simple, owing to there is fragrance dullness, effect single to the effect of flue gas be not fine to this two large class spices.Flavouring essence for tobacco requires with bread and cheese essence different, and therefore the essence of numerous food product, beverage, makeup etc. can not be directly used in production of cigarettes.
Along with the taste of the raising cigarette of modern life level constantly gets a promotion, taste is also constantly improved, and the requirement of smoking personage to cigarette fragrance is also more and more higher.At present, China's flavouring essence for tobacco major part used is all import, and the flavouring essence for tobacco of import exists the high problem of price.In recent years, a lot of researchist of China have also been made many research to flavouring essence for tobacco, and the pertinent literature found is as follows:
1. denomination of invention: the preparation method of flavouring essence for tobacco, publication number: CN 103103017 A.The present invention relates to the preparation method of flavouring essence for tobacco, by weight, get 100 parts, tobacco leaf in flask, add 1 part of glycine respectively, 1 part of L-Ala and 1 part of L-glutamic acid; 80-100 DEG C, stirs 30-60min; Heat filter, filtrate reduced in volume, to obtain final product.Preparation technology of the present invention is simple, but there is fragrance dullness, poor effect single to the effect of flue gas, cannot meet the needs of human consumer to cigarette fragrance.
2. denomination of invention: the preparation method of flavouring essence for tobacco prepared by a kind of pears, publication number: CN 102994230 A, the present invention discloses the preparation method that flavouring essence for tobacco prepared by a kind of pears, get concentrated pear juice 100. 00g that content is 20-40%, add 4-8g kilnitamin, 3-10g brown sugar, 20-40mL propylene glycol, 1mL ammoniacal liquor and 20-60mL water, temperature of reaction is 100-120 DEG C, and the reaction times is 1-2h; Filter, concentrated, to obtain final product.Fragrance of the present invention is single, not good to the action effect of flue gas.
In a word, up to the present, disclosed flavouring essence for tobacco, or fragrance is single, not good to the action effect of flue gas, or complex process, cost is high, and raw material sources are extensive.Therefore, need to provide a kind of fragrance uniqueness, good to flue gas action effect, cost is low, the simple flavouring essence for tobacco of preparation technology.
Passion fruit is described as " passion fruit " has strong unique perfume because permitting the aroma component of various fruits containing piscidia, mango, apple, pineapple etc., passion fruit also have produce refreshing effect to the mind, skin maintenance, anti-cancer, preventing phlegm from forming and stopping coughing, hypertension and hyperlipemia, the effect such as delay senility, the present invention will utilize passion fruit to prepare flavouring essence for tobacco.
Summary of the invention
The object of the invention is exactly that to there is fragrance for existing flavouring essence for tobacco single, not good to the action effect of flue gas, complex process, cost is high, raw material sources extensively wait not enough, a kind of full aroma is provided, there is the dense fragrance of passion fruit uniqueness, raw material is easy to get, prepare flavouring essence for tobacco simple, with low cost, the lifting of the essence prepared to the mouthfeel of cigarette has good effect, enjoys consumers in general to like.
For realizing above object, the technical solution used in the present invention is:
Utilize a flavouring essence for tobacco prepared by passion fruit, mixed by ratio of weight and the number of copies by following raw material components:
Passion fruit 20-30 part, roseleaf 1-3 part, jasmine petal 1-3 part, ethyl acetate 5-10 part, butyl butyrate 3-8 part, ethyl 2-methylbutyrate 2-5 part, styryl carbinol 10-15 part, ethanol 40-60 part.
Further, the concentration of described ethanol is 55%-70%.
A preparation method for the flavouring essence for tobacco utilizing passion fruit to prepare, the method comprises the following steps:
(1) supercritical carbon dioxide extraction petal: the roseleaf of above-mentioned parts by weight and jasmine petal are dried, pulverizes, obtains petal powder; Loaded by petal powder in extraction batch can, extraction batch can is placed in extraction axe, sealing extraction axe, passes into and is in supercritical carbon dioxide, uses ethanol to carry out supercritical carbon dioxide extraction as entrainment agent, obtains petal extracting solution;
(2) preparation of passion fruit fruit juice: fresh passion fruit will be selected, cleaning, fragmentation, put into pressure pan, add ethanol, be forced into 25-35MPa, keeps 20-30min, recovers normal pressure, obtain Passion Fruit Juice;
(3) preparation of essence: petal extracting solution obtained above, Passion Fruit Juice, ethyl acetate, butyl butyrate, ethyl 2-methylbutyrate, styryl carbinol and ethanol are mixed, obtains essence; Mixed solution is added in pipe tobacco and is rolled into cigarette.
Further, the pulverizing of described step (1) is that roseleaf and jasmine petal are crushed to 10-30 order.
Further, the supercritical carbon dioxide extraction pressure of described step (1) is 25-40Mpa, and extraction temperature is 40-55 DEG C, and extraction time is 2.5-4h.
Further, described step (1) ethanol is 2-3:1 as its consumption of entrainment agent and petal powder quality ratio.
Further, described step (1) use ethanol for its concentration of entrainment agent be 75%-95%.
Further, the flow of described step (1) carbonic acid gas is 15-25L/h.
Further, described step (2) adds the weight ratio of ethanol and passion fruit is 1-1.5:1.
Further, the consumption of described flavouring essence for tobacco is the 0.5-1.5% accounting for tobacco quality.
Compared with prior art, the beneficial effect that the present invention obtains is:
(1) passion fruit contains piscidia, mango, apple, pineapple etc. and is permitted the aroma component of various fruits and had strong unique perfume, and passion fruit also has the effects such as preventing phlegm from forming and stopping coughing, refreshment and brain nourishing, hypertension and hyperlipemia; Passion fruit is used in flavouring essence for tobacco and makes fragrance unique, and cost is also lower simultaneously; Widen the intensive processing approach of China's passion fruit industry, add the value of passion fruit, improve the income of orchard worker.
(2) the present invention's essence of utilizing passion fruit, Flower of Arabian Jasmine and Rose etc. to prepare and the fragrant Harmony of cigarette good, have the peculiar fragrance of passion fruit, Rose and Flower of Arabian Jasmine, the flavouring essence for tobacco cost of gained of the present invention is low, preparation technology is simple.
Embodiment
Below in conjunction with embodiment, the present invention is further described, but protection scope of the present invention is not limited only to embodiment.
embodiment 1
A preparation method for the flavouring essence for tobacco utilizing passion fruit to prepare, the method comprises the following steps:
(1) supercritical carbon dioxide extraction petal: 1 part of roseleaf and 1 part of jasmine petal are dried, is crushed to 10 orders, obtains petal powder; Petal powder is loaded in extraction batch can, extraction batch can is placed in extraction axe, sealing extraction axe, pass into and be in supercritical carbon dioxide, the flow of its carbonic acid gas is 15L/h, and using 6 parts of concentration to be 75% ethanol as entrainment agent (its consumption and petal powder quality are than being 3:1), is 25Mpa in extracting pressure, extraction temperature is 40 DEG C of supercritical carbon dioxide extraction 4h, obtains petal extracting solution;
(2) preparation of passion fruit fruit juice: fresh passion fruit 20 parts will be selected, remove fruit that rot, ill worm, first with washing water of rice again with tap water clean up, broken, put into pressure pan, adding 30 parts of concentration is 55% ethanol (weight ratio of ethanol and passion fruit is 1.5:1), is forced into 25MPa, keeps 30min, recover normal pressure, obtain Passion Fruit Juice;
(3) preparation of essence: by petal extracting solution obtained above, Passion Fruit Juice, ethyl acetate 5 parts, butyl butyrate 3 parts, ethyl 2-methylbutyrate 2 parts, styryl carbinol 10 parts is that 55% ethanol mixes with adding 10 parts of concentration, obtains essence; The essence of account for tobacco quality 1.0% is added in pipe tobacco and is rolled into cigarette.
embodiment 2
A preparation method for the flavouring essence for tobacco utilizing passion fruit to prepare, the method comprises the following steps:
(1) supercritical carbon dioxide extraction petal: 2 parts of roseleafs and 2 parts of jasmine petals are dried, is crushed to 20 orders, obtains petal powder; Petal powder is loaded in extraction batch can, extraction batch can is placed in extraction axe, sealing extraction axe, pass into and be in supercritical carbon dioxide, the flow of its carbonic acid gas is 20L/h, and using 10 parts of concentration to be 85% ethanol as entrainment agent (its consumption and petal powder quality are than being 2.5:1), is 30Mpa in extracting pressure, extraction temperature is 45 DEG C of supercritical carbon dioxide extraction 3h, obtains petal extracting solution;
(2) preparation of passion fruit fruit juice: fresh passion fruit 25 parts will be selected, remove fruit that rot, ill worm, first with washing water of rice again with tap water clean up, broken, put into pressure pan, adding 25 parts of concentration is 60% ethanol (weight ratio of ethanol and passion fruit is 1:1), is forced into 30MPa, keeps 25min, recover normal pressure, obtain Passion Fruit Juice;
(3) preparation of essence: by petal extracting solution obtained above, Passion Fruit Juice, ethyl acetate 8 parts, butyl butyrate 5 parts, ethyl 2-methylbutyrate 4 parts, styryl carbinol 10 parts is that 60% ethanol mixes with adding 30 parts of concentration, obtains essence; The essence of account for tobacco quality 0.5% is added in pipe tobacco and is rolled into cigarette.
embodiment 3
A preparation method for the flavouring essence for tobacco utilizing passion fruit to prepare, the method comprises the following steps:
(1) supercritical carbon dioxide extraction petal: 3 parts of roseleafs and 3 parts of jasmine petals are dried, is crushed to 30 orders, obtains petal powder; Petal powder is loaded in extraction batch can, extraction batch can is placed in extraction axe, sealing extraction axe, pass into and be in supercritical carbon dioxide, the flow of its carbonic acid gas is 25L/h, and making 12 parts of concentration be 95% ethanol as entrainment agent (its consumption and petal powder quality are than being 2:1), is 35Mpa in extracting pressure, extraction temperature is 55 DEG C of supercritical carbon dioxide extraction 2.5h, obtains petal extracting solution;
(2) preparation of passion fruit fruit juice: fresh passion fruit 30 parts will be selected, remove fruit that rot, ill worm, first with washing water of rice again with tap water clean up, broken, put into pressure pan, adding 30 parts of concentration is 70% ethanol (weight ratio of ethanol and passion fruit is 1:1), is forced into 35MPa, keeps 20min, recover normal pressure, obtain Passion Fruit Juice;
(3) preparation of essence: by petal extracting solution obtained above, Passion Fruit Juice, ethyl acetate 10 parts, butyl butyrate 8 parts, ethyl 2-methylbutyrate 5 parts, styryl carbinol 15 parts is that 70% ethanol mixes with adding 30 parts of concentration, obtains essence; The essence of account for tobacco quality 1.5% is added in pipe tobacco and is rolled into cigarette.
Claims (10)
1. the flavouring essence for tobacco utilizing passion fruit to prepare, is characterized in that: mixed by ratio of weight and the number of copies by following raw material components:
Passion fruit 20-30 part, roseleaf 1-3 part, jasmine petal 1-3 part, ethyl acetate 5-10 part, butyl butyrate 3-8 part, ethyl 2-methylbutyrate 2-5 part, styryl carbinol 10-15 part, ethanol 40-60 part.
2. a kind of flavouring essence for tobacco utilizing passion fruit to prepare according to claim 1, is characterized in that: it is characterized in that: the concentration of described ethanol is 55%-70%.
3. a kind of preparation method of the flavouring essence for tobacco utilizing passion fruit to prepare as described in as arbitrary in claim 1-2, is characterized in that: the method comprises the following steps:
Supercritical carbon dioxide extraction petal: the roseleaf of above-mentioned parts by weight and jasmine petal are dried, pulverizes, obtains petal powder; Loaded by petal powder in extraction batch can, extraction batch can is placed in extraction axe, sealing extraction axe, passes into and is in supercritical carbon dioxide, uses ethanol to carry out supercritical carbon dioxide extraction as entrainment agent, obtains petal extracting solution;
The preparation of passion fruit fruit juice: fresh passion fruit will be selected, cleaning, fragmentation, put into pressure pan, add ethanol, be forced into 25-35MPa, keeps 20-30min, recovers normal pressure, obtain Passion Fruit Juice;
The preparation of essence: petal extracting solution obtained above, Passion Fruit Juice, ethyl acetate, butyl butyrate, ethyl 2-methylbutyrate, styryl carbinol and ethanol are mixed, obtains essence; Mixed solution is added in pipe tobacco and is rolled into cigarette.
4. the preparation method of a kind of flavouring essence for tobacco utilizing passion fruit to prepare according to claim 3, is characterized in that: the pulverizing of described step (1) is that roseleaf and jasmine petal are crushed to 10-30 order.
5. the preparation method of a kind of flavouring essence for tobacco utilizing passion fruit to prepare according to claim 3, is characterized in that: the supercritical carbon dioxide extraction pressure of described step (1) is 25-40Mpa, and extraction temperature is 40-55 DEG C, and extraction time is 2.5-4h.
6. the preparation method of a kind of flavouring essence for tobacco utilizing passion fruit to prepare according to claim 5, is characterized in that: described step (1) ethanol as its consumption of entrainment agent and petal powder quality than being 2-3:1.
7. the preparation method of a kind of flavouring essence for tobacco utilizing passion fruit to prepare according to claim 6, is characterized in that: described step (1) use ethanol for its concentration of entrainment agent be 75%-95%.
8. the preparation method of a kind of flavouring essence for tobacco utilizing passion fruit to prepare according to claim 7, is characterized in that: the flow of described step (1) carbonic acid gas is 15-25L/h.
9. the preparation method of a kind of flavouring essence for tobacco utilizing passion fruit to prepare according to claim 3, its feature
Be: the weight ratio that described step (2) adds ethanol and passion fruit is 1-1.5:1.
10., according to the preparation method of the arbitrary described a kind of flavouring essence for tobacco utilizing passion fruit to prepare of claim 1-9, it is characterized in that: the consumption of described flavouring essence for tobacco is the 0.5-1.5% accounting for tobacco quality.
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| CN201410813305.4A CN104611136A (en) | 2014-12-24 | 2014-12-24 | Cigarette essence prepared by utilization of passion fruit and preparing method thereof |
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Cited By (9)
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| CN106418665A (en) * | 2016-09-27 | 2017-02-22 | 湖北中烟工业有限责任公司 | Cassia flavor cigarette paper essence and preparation method and application |
| CN106617289A (en) * | 2017-02-14 | 2017-05-10 | 广西中烟工业有限责任公司 | Harm-reducing cigarette filter additive and filter preparation method |
| CN106666823A (en) * | 2016-12-16 | 2017-05-17 | 东莞波顿香料有限公司 | Compound extract for cigarette, microcapsule containing extract and preparation methods thereof |
| CN107495463A (en) * | 2017-08-15 | 2017-12-22 | 中山市博林树投资管理有限公司 | A kind of preparation method of fruit cigarette |
| CN110819458A (en) * | 2019-11-08 | 2020-02-21 | 湖北中烟工业有限责任公司 | Preparation method and application of passion fruit tobacco essence |
| CN112094693A (en) * | 2020-09-17 | 2020-12-18 | 湖北中烟工业有限责任公司 | Passion fruit bead-blasting essence and application thereof |
| CN112725084A (en) * | 2020-11-19 | 2021-04-30 | 江苏利田科技股份有限公司 | Passion fruit essence and preparation method and application thereof |
| CN113462473A (en) * | 2021-07-13 | 2021-10-01 | 广州芬豪香精有限公司 | Preparation method of perfume type essence with lasting fragrance |
| CN113563972A (en) * | 2021-07-17 | 2021-10-29 | 广州芬豪香精有限公司 | Preparation method of daily chemical essence with fruit fragrance |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106418665A (en) * | 2016-09-27 | 2017-02-22 | 湖北中烟工业有限责任公司 | Cassia flavor cigarette paper essence and preparation method and application |
| CN106666823A (en) * | 2016-12-16 | 2017-05-17 | 东莞波顿香料有限公司 | Compound extract for cigarette, microcapsule containing extract and preparation methods thereof |
| CN106666823B (en) * | 2016-12-16 | 2019-07-12 | 东莞波顿香料有限公司 | A kind of cigarette composite extract and the microcapsules with the extract and preparation method thereof |
| CN106617289A (en) * | 2017-02-14 | 2017-05-10 | 广西中烟工业有限责任公司 | Harm-reducing cigarette filter additive and filter preparation method |
| CN107495463A (en) * | 2017-08-15 | 2017-12-22 | 中山市博林树投资管理有限公司 | A kind of preparation method of fruit cigarette |
| CN110819458A (en) * | 2019-11-08 | 2020-02-21 | 湖北中烟工业有限责任公司 | Preparation method and application of passion fruit tobacco essence |
| CN112094693A (en) * | 2020-09-17 | 2020-12-18 | 湖北中烟工业有限责任公司 | Passion fruit bead-blasting essence and application thereof |
| CN112094693B (en) * | 2020-09-17 | 2022-11-04 | 湖北中烟工业有限责任公司 | Passion fruit bead-blasting essence and application thereof |
| CN112725084A (en) * | 2020-11-19 | 2021-04-30 | 江苏利田科技股份有限公司 | Passion fruit essence and preparation method and application thereof |
| CN113462473A (en) * | 2021-07-13 | 2021-10-01 | 广州芬豪香精有限公司 | Preparation method of perfume type essence with lasting fragrance |
| CN113563972A (en) * | 2021-07-17 | 2021-10-29 | 广州芬豪香精有限公司 | Preparation method of daily chemical essence with fruit fragrance |
| CN113563972B (en) * | 2021-07-17 | 2023-08-25 | 广州芬豪香精有限公司 | Preparation method of daily chemical essence with fruit fragrance |
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Application publication date: 20150513 |