CN106666823B - A kind of cigarette composite extract and the microcapsules with the extract and preparation method thereof - Google Patents
A kind of cigarette composite extract and the microcapsules with the extract and preparation method thereof Download PDFInfo
- Publication number
- CN106666823B CN106666823B CN201611170742.4A CN201611170742A CN106666823B CN 106666823 B CN106666823 B CN 106666823B CN 201611170742 A CN201611170742 A CN 201611170742A CN 106666823 B CN106666823 B CN 106666823B
- Authority
- CN
- China
- Prior art keywords
- cigarette
- composite extract
- extract
- microcapsules
- adsorbent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn - After Issue
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- 239000000284 extract Substances 0.000 title claims abstract description 144
- 239000002131 composite material Substances 0.000 title claims abstract description 115
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 101
- 239000003094 microcapsule Substances 0.000 title claims abstract description 65
- 238000000605 extraction Methods 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 30
- 235000011925 Passiflora alata Nutrition 0.000 claims abstract description 15
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- 235000013750 Passiflora mixta Nutrition 0.000 claims abstract description 15
- 235000013731 Passiflora van volxemii Nutrition 0.000 claims abstract description 15
- 240000002690 Passiflora mixta Species 0.000 claims abstract description 14
- 240000004307 Citrus medica Species 0.000 claims abstract description 13
- 235000011511 Diospyros Nutrition 0.000 claims abstract description 13
- 235000006662 Lansium Nutrition 0.000 claims abstract description 13
- 241001156382 Lansium Species 0.000 claims abstract description 13
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- 235000008708 Morus alba Nutrition 0.000 claims abstract description 13
- 244000183331 Nephelium lappaceum Species 0.000 claims abstract description 13
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- 239000003463 adsorbent Substances 0.000 claims description 41
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- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
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- 239000007788 liquid Substances 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
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- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 4
- NXMUXTAGFPJGTQ-UHFFFAOYSA-N decanoic acid;octanoic acid Chemical compound CCCCCCCC(O)=O.CCCCCCCCCC(O)=O NXMUXTAGFPJGTQ-UHFFFAOYSA-N 0.000 claims description 4
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- 229920002774 Maltodextrin Polymers 0.000 claims description 3
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical group [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 3
- 150000001720 carbohydrates Chemical class 0.000 claims description 3
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- 229910052799 carbon Inorganic materials 0.000 claims description 3
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- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 3
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 3
- 229920000159 gelatin Polymers 0.000 claims description 3
- 239000008273 gelatin Substances 0.000 claims description 3
- 235000019322 gelatine Nutrition 0.000 claims description 3
- 235000011852 gelatine desserts Nutrition 0.000 claims description 3
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- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 3
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 3
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- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 2
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- 229910021641 deionized water Inorganic materials 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
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- 230000000694 effects Effects 0.000 abstract description 12
- 230000000391 smoking effect Effects 0.000 abstract description 9
- 230000001737 promoting effect Effects 0.000 abstract description 8
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 7
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/44—Ebenaceae (Ebony family), e.g. persimmon
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/60—Moraceae (Mulberry family), e.g. breadfruit or fig
- A61K36/605—Morus (mulberry)
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K36/75—Rutaceae (Rue family)
- A61K36/752—Citrus, e.g. lime, orange or lemon
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/77—Sapindaceae (Soapberry family), e.g. lychee or soapberry
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/48—Preparations in capsules, e.g. of gelatin, of chocolate
- A61K9/4841—Filling excipients; Inactive ingredients
- A61K9/4875—Compounds of unknown constitution, e.g. material from plants or animals
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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Abstract
A kind of cigarette composite extract and the microcapsules with the extract and preparation method thereof, a kind of cigarette composite extract is by passionflower, rambutan, citron, Calusena lansium, sea-buckthorn, pyracantha fortuneana leaf, persimmon leaves, mulberry leaves are mixed to prepare, then it is prepared into microcapsules again, it is applied in cigarette filter rod, it can assign cigarette tropical fruit fragrance abundant, mutually coordinate with cigarette smoke, increase the sweet sense for inhaling taste and fine and smooth sense, reduce irritation, simultaneously, effective component in composite extract has effects that throat soothing of promoting the production of body fluid, oral cavity is brought by flue gas, it can overcome the disadvantages that dry throat problem brought by cigarette smoking, improve the pleasant degree of smoking property of cigarette, preparation method can greatly improve the recovery rate of plant and the application of effective component, avoid dissolving in for its functionality, the effect in cigarette application improved.
Description
Technical field
The present invention relates to cigarette additives technical fields, and in particular to a kind of cigarette composite extract and has the extraction
Microcapsules of object and preparation method thereof.
Background technique
Plant extracts refers to using solvent appropriate or method, with plant (plant is all or certain is a part of) for raw material
The substance for extracting or being process can be used for pharmaceuticals industry, food service industry, healthy industry, beauty industry and other industries.?
Tobacco business, with the growing interest to cigarette consumption person's health, the research and development of low-coke tar cigarette product become China's cigarette industry
The inexorable trend of development, but while tar content in cigarette reduces, the perfume quantity of cigarette, concentration, it is jealous be greatly reduced, select
Suitable plant extracts is added in low-coke tar cigarette, is a kind of effective way for carrying out cigarette compensating aroma, to improvement cigarette
The quality of grass has important role, and therefore, tobacco business has also more and more used natural plant extracts.Have in plant
Abundant and complicated effect ingredient, such as saponin, alkaloid, polysaccharide, polyphenol, flavonoids and volatile oil have and remove freely
The bioactive functions such as base, bidirectional modulation immunity of organism, antiviral, antibacterial, anti-oxidant, cigarette can be reduced in cigarette by applying
Harm reduces disease caused by smoking.It is environmentally protective using natural plants as raw material, meet the low burnt drop evil of China's cigarette industry
Developing direction, meet China modern people pursuit natural theory.
But the readily volatilized loss of effective component in extract, vulnerable to the environmental factors such as light, oxygen, heat influence and become
Matter influences product quality, and extract microcapsules can effectively solve the above problem.Microencapsulation refers to solid, liquid even
Gas wrapping is isolated it with external environment, can not only protect effective component in a sealing or semipermeable tiny capsules,
Volatilization is reduced, Shelf-life also easily facilitates processing, uses and store.Currently, microcapsule essence is applied to cigarette filter rod
It is considered as ideal cigarette-flavoring method, because directly adding essence or the flavoring line in filter stick in the tobacco, all deposits
Shorter in the essence residence time, essence discharges non-uniform disadvantage, and microcapsule essence just compensates for this defect, and adds
Being avoided that chemical substance is directly burnt in filter stick gives cigarette bring miscellaneous taste.Patent CN103396886A discloses a kind of spraying
The flavouring essence for tobacco microcapsules of seasoning preparation, but the microcapsules of spray drying process preparation are powdery form, when processing and aspirating
It is easy to bring dust, it has not been convenient to which addition is in filter stick.Patent CN104178356A also discloses that a kind of spray drying is resulting thin
Lotus essential oil microcapsules and its application in tobacco, but its needs be diluted with water after can just be added in filter stick, to processing and
Storage is made troubles.
Summary of the invention
In order to overcome shortcoming and defect existing in the prior art, the purpose of the present invention is to provide a kind of cigarette with compound
Extract and capsule containing the composite extract, are applied in cigarette filter rod, can assign cigarette tropical fruit (tree) abundant
Fragrance is mutually coordinated with cigarette smoke, increases the sweet sense for inhaling taste and fine and smooth sense, reduces irritation, meanwhile, in composite extract
Effective component has effects that throat soothing of promoting the production of body fluid, and brings oral cavity by flue gas, can overcome the disadvantages that dry throat brought by cigarette smoking is asked
Topic, improves the pleasant degree of smoking property of cigarette.
The purpose of the present invention is to provide a kind of preparation method of cigarette composite extract, obtained composite extract
Natural active principle content is high, and the good drug efficacy of active principle can assign cigarette tropical fruit fragrance abundant, with cigarette smoke
Mutually coordinate, increase the sweet sense for inhaling taste and fine and smooth sense, reduces irritation, meanwhile, the effective component in composite extract has life
The effect of saliva throat soothing, brings oral cavity by flue gas, can overcome the disadvantages that dry throat problem brought by cigarette smoking, improves cigarette suction
The pleasant degree of food.
The purpose of the invention is achieved by the following technical solution:
A kind of cigarette composite extract, is prepared by the raw material of following parts by weight:
40-50 parts of passionflower
10-15 parts of rambutan
5-15 parts of citron
10-20 parts of Calusena lansium
5-10 parts of sea-buckthorn
5-10 parts of pyracantha fortuneana leaf
5-10 parts of persimmon leaves
5-10 parts of mulberry leaves.
The passionflower, rambutan, citron, Calusena lansium, sea-buckthorn are the fruits raw material with certain health care functions, pyracantha fortuneana tree
Leaf, persimmon leaves, mulberry leaves are the herbaceous plant raw materials with medical value, and specific effect is as shown in the table:
| Raw material | Effect |
| Passionflower | Anti-inflammatory analgetic, promoting blood circulation, blood fat-reducing blood pressure-decreasing, toxin-expelling and face nourishing, strengthen immunity |
| Rambutan | Improve mouth group inflammation and diarrhea, fall fire is antipyretic, has significant effect to tongue inflammation |
| Citron | Treat stomach abdominal distention and pain, indigestion, circulation of vital energy in the wrong direction vomiting, phlegmatic cough |
| Calusena lansium | Promoting the circulation of qi helps digestion, resolving sputum |
| Sea-buckthorn | Relieving cough and reducing sputum, stomach strengthening and digestion promoting, reduces cholesterol, allevating angina pectoris at promoting blood circulation to remove blood stasis |
| Pyracantha fortuneana leaf | It is clearing heat and detoxicating |
| Persimmon leaves | It slakes thirst and help produce saliva, the lung qi that disappears is swollen, reduces blood pressure, softens blood vessel, purifying the blood and anti-inflammatory |
| Mulberry leaves | Dispelling wind and heat, cooling blood and hemostasis are clear liver and improved vision, moistening lung to arrest cough |
In the raw material, passionflower is that a kind of tropical liana seeks connections with fruit tree, and sweet fruit acid is palatable, and with rich flavor, fragrance is happy
People has the refined title of " fruit of enthusiasm ".It according to surveying and determination, is in the world containing the aromatic substance for having more than 132 kinds or more in passion flower fruit
Known most fragrant one of fruit, based on passionflower, cooperation rambutan, citron, Calusena lansium these tropical fruit (tree)s can assign cigarette
The compound fruit breath in the torrid zone of fresh and comfortable, enriches cigarette perfume, improves mouthfeel, keep flue gas submissive, fine and smooth, increase the sweet of oral cavity
Sense, increases that cigarette is sweet, profit, the organoleptic quality of alcohol, perfume (or spice).These fruit also have certain medical value, can anti-inflammatory, fall fire, change
Phlegm, meanwhile, pyracantha fortuneana leaf, persimmon leaves, mulberry leaves also have it is clearing heat and detoxicating, promote the production of body fluid to quench thirst, the medicinal efficacy of moistening lung to arrest cough, these
Functional component brings oral cavity by flue gas, can be reduced the irritation of flue gas, throat soothing of promoting the production of body fluid, and alleviates caused by smoking to a certain extent
The adverse reactions such as throat is dry to itch, coughs, panting, silt phlegm, protect the throat of smoking population.
A kind of preparation method of cigarette composite extract, comprising the following steps:
(1) it is dry that fresh passionflower, rambutan, citron, Calusena lansium, sea buckthorn fruit are carried out to whole fruit freezing after weighing proportionally
Dry processing, the dry moisture content to whole fruit are lower than 10%；
(2) fruit after drying is crushed, grinding particle size is 10-20 mesh；
(3) smashed raw material is put into extraction kettle and carries out supercritical carbon dioxide extracting, extraction conditions are as follows: extraction kettle
Temperature: 40-50 DEG C, pressure: 25-35MPa；Separating still temperature: 30-40 DEG C, pressure: 5-8MPa；Extraction time: 2.5-3.5h；
(4) after supercritical extract from separating still isolated resin-like liquid, the anhydrous second of 3-5 times of its weight is added
Alcohol, 16-24h under the conditions of placing -20 DEG C after dissolution filter to obtain supernatant, obtain grease A after removal solvent is concentrated under reduced pressure；
(5) pyracantha fortuneana leaf, persimmon leaves, mulberry leaves are weighed in proportion, 90-100 DEG C of hot water scalding 10- is put into after mixing
30 seconds, 4-10 DEG C of cold water boshing being put into immediately, dries, extracts, Extraction solvent is the deionization of 8-12 times of leaf weight
Water, Extracting temperature are 60-80 DEG C, time 2.5-3.5h, repeat to extract once, filtering, filtrate is concentrated into relative density and is
1.200-1.300 medicinal extract B；
(6) grease A and medicinal extract B is mixed, the hydrophily pungent last of the ten Heavenly stems of the mixed weight of 1 times of 2 grease A and medicinal extract B is added
Acid glyceride filters after being dispersed with stirring, obtains composite extract.
A kind of cigarette composite extract microcapsules, it is the spherical shape or irregular shape particle that granularity is 0.1-3mm, with institute
The composite extract stated is core material, is prepared by the raw material of following weight percent:
Composite extract 0.01~40%
Adsorbent 0.01~40%
Vehicle 20~90%
Binder 0.01~1%.
Preferably, a kind of composite extract microcapsules, are prepared by the raw material of following weight percent:
Composite extract 5~30%
Adsorbent 5~30%
Vehicle 40~90%
Binder 0.1~1%
The ratio of a kind of cigarette composite extract microcapsules, the composite extract and adsorbent is 1:0.8~1.5.
A kind of cigarette composite extract microcapsules, the adsorbent are commercially available porous, inorganic or organic material.
A kind of cigarette composite extract microcapsules, the adsorbent be porous-starch, porous silica, active carbon,
The mixture of one or more of corncob, poriferous titanium dioxide, carbon nanotube.
A kind of cigarette composite extract microcapsules, the vehicle include microcrystalline cellulose, starch, maltodextrin,
The mixing of one or more of sucrose, lactose, chitosan, carragheen, gelatin, pectin, methylcellulose, ethyl cellulose
Object.
A kind of cigarette composite extract microcapsules, the binder include sodium carboxymethylcellulose, hydroxypropyl methyl fibre
Tie up any of element, carbohydrate etc..
A kind of preparation method of cigarette composite extract microcapsules, comprising the following steps:
A, composite extract is slowly added in adsorbent, 10-30min is mixed, adsorbs adsorbent sufficiently compound
Extract；
B, vehicle, binder are added in the adsorbent for having adsorbed composite extract described in step A, are sufficiently mixed
Uniformly；
C, it is granulated, prepares composite extract microcapsules.
A kind of preparation method of cigarette composite extract microcapsules, prilling process described in the step C are fluidisation
Bed is granulated, squeezes out-and it is round as a ball granulation, wet granulation, any in non-slurry pelletizing.
The purpose of microencapsulation is effect ingredient sensitive in protection composite extract, it is avoided directly to contact extraneous ring
Light, oxygen, heat in border etc., prevent effective component oxidation deterioration, while reducing volatility, slow down the rate of release of effective component,
Extend fragrance remaining time, and the composite extract of liquid is transformed into solid-state form, is conducive to storage and transport.
Composite extract of the present invention can be used as tobacco aromaticss and directly apply in cigarette product, addition manner include but
It is not limited to the addition in cigarette making process to add in paper pulp on pipe tobacco, or in cigarette paper manufacturing process, or in acetic acid
It is added in fibre bundle forming process in plasticizers, or is made into fragrant line addition in cigaratte filter, or directly make an addition to cigarette
In filter tip etc..
Composite extract microcapsules of the present invention can be used as tobacco aromaticss and be preferably applied in cigarette filter rod.
Compared with prior art, the present invention has the following beneficial effects:
(1) composite extract of the invention uses natural fruit, herbaceous plant for raw material preparation, environmentally protective harmless, symbol
Close the development trend of Chinese-style cigarette.Composite extract has a tropical fruit (tree) breath, soft aroma and full rich in level, is applied to volume
In smoke product, it can assign cigarette unique style, taste satisfaction is coordinated with tobacco taste, improves the sophistication of cigarette taste
With soft degree, cigarette quality is promoted, and effect ingredient in composite extract has clearing heat, relieving sore-throat, cough-relieving of promoting the production of body fluid, anti-inflammatory anti-anaphylaxis
Medicinal efficacy, effective component brings oral cavity by flue gas, has a constant current modulation to the throat and tunica mucosa tracheae of protection smoking population
Effect.
(2) effect ingredient in composite extract microcapsules energy effective protection composite extract of the invention, prevents its oxygen
Change and go bad, keeps tobacco product mouthfeel more preferably lasting.Composite extract microcapsules are applied in cigarette filter rod, and it is direct to avoid wall material
Influence of the peculiar smell to cigarette quality brought by burning, and granular form is compared to the microcapsule product of powder type,
Dust pollution will not be generated in production and application process, it is easier to processing and storage.
Specific embodiment
For the ease of the understanding of those skilled in the art, below with reference to embodiment, the present invention is further illustrated, real
The content that the mode of applying refers to not is limitation of the invention.
Embodiment 1
A kind of cigarette composite extract, is prepared by the raw material of following parts by weight:
40 parts of passionflower
15 parts of rambutan
5 parts of citron
20 parts of Calusena lansium
5 parts of sea-buckthorn
10 parts of pyracantha fortuneana leaf
5 parts of persimmon leaves
10 parts of mulberry leaves.
A kind of preparation method of cigarette composite extract, comprising the following steps:
(1) it is dry that fresh passionflower, rambutan, citron, Calusena lansium, sea buckthorn fruit are carried out to whole fruit freezing after weighing proportionally
Dry processing, and it is dry to constant weight；
(2) fruit after drying is crushed, grinding particle size is 10 mesh；
(3) smashed raw material is put into extraction kettle and carries out supercritical carbon dioxide extracting, extraction conditions are as follows: extraction kettle
Temperature: 50 DEG C, pressure: 25MPa；Separating still temperature: 40 DEG C, pressure: 8MPa；Extraction time: 2.5h；
(4) after supercritical extract from separating still isolated resin-like liquid, the dehydrated alcohol of 5 times of its weight is added,
Under the conditions of placing -20 DEG C after dissolution for 24 hours, supernatant is filtered to obtain, obtains grease A after removal solvent is concentrated under reduced pressure；
(5) fresh pyracantha fortuneana leaf, persimmon leaves, mulberry leaves are weighed in proportion, 90-100 DEG C of hot water leaching is put into after mixing
Scald 10-30 second, put into 4-10 DEG C of cold water boshing immediately, dry, extract, Extraction solvent for 8 times of leaf weight go from
Sub- water, Extracting temperature are as follows: 60 DEG C, time 2.5h, repeat to extract primary, filtering, it is 1.300 that filtrate, which is concentrated into relative density,
Medicinal extract B；
(6) grease A and medicinal extract B is mixed, the hydrophily Glycerin, mixed triester with caprylic acid capric acid of both 1 times mixed weight, stirring is added
It is filtered after dispersion, obtains composite extract.
Embodiment 2
A kind of cigarette composite extract, is prepared by the raw material of following parts by weight:
50 parts of passionflower
10 parts of rambutan
15 parts of citron
10 parts of Calusena lansium
10 parts of sea-buckthorn
5 parts of pyracantha fortuneana leaf
10 parts of persimmon leaves
5 parts of mulberry leaves.
A kind of preparation method of cigarette composite extract, comprising the following steps:
(1) it is dry that fresh passionflower, rambutan, citron, Calusena lansium, sea buckthorn fruit are carried out to whole fruit freezing after weighing proportionally
Dry processing, and it is dry to constant weight；
(2) fruit after drying is crushed, grinding particle size is 20 mesh；
(3) smashed raw material is put into extraction kettle and carries out supercritical carbon dioxide extracting, extraction conditions are as follows: extraction kettle
Temperature: 40 DEG C, pressure: 35MPa；Separating still temperature: 30 DEG C, pressure: 5MPa；Extraction time: 3.5h；
(4) after supercritical extract from separating still isolated resin-like liquid, the anhydrous second of 3-5 times of its weight is added
Alcohol, 16h under the conditions of placing -20 DEG C after dissolution filter to obtain supernatant, obtain grease A after removal solvent is concentrated under reduced pressure；
(5) fresh pyracantha fortuneana leaf, persimmon leaves, mulberry leaves are weighed in proportion, 90-100 DEG C of hot water leaching is put into after mixing
Scald 10-30 second, put into 4-10 DEG C of cold water boshing immediately, dry, extract, Extraction solvent for 12 times of leaf weight go from
Sub- water, Extracting temperature are as follows: 80 DEG C, time 3.5h, repeat to extract primary, filtering, it is 1.200 that filtrate, which is concentrated into relative density,
Medicinal extract B；
(6) grease A and medicinal extract B is mixed, the hydrophily Glycerin, mixed triester with caprylic acid capric acid of both 1 times mixed weight, stirring is added
It is filtered after dispersion, obtains composite extract.
Embodiment 3
A kind of cigarette composite extract, is prepared by the raw material of following parts by weight:
45 parts of passionflower
12 parts of rambutan
10 parts of citron
15 parts of Calusena lansium
8 parts of sea-buckthorn
7 parts of pyracantha fortuneana leaf
8 parts of persimmon leaves
7 parts of mulberry leaves.
A kind of preparation method of cigarette composite extract, comprising the following steps:
(1) it is dry that fresh passionflower, rambutan, citron, Calusena lansium, sea buckthorn fruit are carried out to whole fruit freezing after weighing proportionally
Dry processing, and it is dry to constant weight；
(2) fruit after drying is crushed, grinding particle size is 15 mesh；
(3) smashed raw material is put into extraction kettle and carries out supercritical carbon dioxide extracting, extraction conditions are as follows: extraction kettle
Temperature: 45 DEG C, pressure: 30MPa；Separating still temperature: 35 DEG C, pressure: 7MPa；Extraction time: 3h；
(4) after supercritical extract from separating still isolated resin-like liquid, the dehydrated alcohol of 4 times of its weight is added,
20h under the conditions of placing -20 DEG C after dissolution filters to obtain supernatant, obtains grease A after removal solvent is concentrated under reduced pressure；
(5) fresh pyracantha fortuneana leaf, persimmon leaves, mulberry leaves are weighed in proportion, 90-100 DEG C of hot water leaching is put into after mixing
It scalds 10-30 seconds, puts into 4-10 DEG C of cold water boshing immediately, dry, extract, Extraction solvent is going for 8-12 times of leaf weight
Ionized water, Extracting temperature are as follows: 70 DEG C, time 3h, repeat to extract primary, filtering, it is 1.25 that filtrate, which is concentrated into relative density,
Medicinal extract B；
(6) grease A and medicinal extract B is mixed, the hydrophily Glycerin, mixed triester with caprylic acid capric acid of both 1 times mixed weight, stirring is added
It is filtered after dispersion, obtains composite extract.
Embodiment 4
A kind of cigarette composite extract microcapsules, it is the spherical shape or irregular shape particle that granularity is 0.1-3mm, with institute
The composite extract stated is core material, is prepared by the raw material of following weight percent:
Composite extract 5%
Adsorbent 7.5%
Vehicle 87.4%
Binder 0.1%.
The ratio of a kind of cigarette composite extract microcapsules, the composite extract and adsorbent is 1:1.5.
A kind of cigarette composite extract microcapsules, the adsorbent are commercially available porous, inorganic or organic material.
A kind of cigarette composite extract microcapsules, the adsorbent is by porous-starch, porous silica according to quality
It is mixed than 1:1.
A kind of cigarette composite extract microcapsules, the vehicle by microcrystalline cellulose, starch, maltodextrin according to
Mass ratio 4:2:1 mixing.
A kind of cigarette composite extract microcapsules, the binder are sodium carboxymethylcellulose.
A kind of preparation method of cigarette composite extract microcapsules, comprising the following steps:
A, composite extract is slowly added in adsorbent, 10-30min is mixed, adsorbs adsorbent sufficiently compound
Extract；
B, vehicle, binder are added in the adsorbent for having adsorbed composite extract described in step A, are sufficiently mixed
Uniformly；
C, it is granulated, prepares composite extract microcapsules.
Embodiment 5
A kind of cigarette composite extract microcapsules, it is the spherical shape or irregular shape particle that granularity is 0.1-3mm, with institute
The composite extract stated is core material, is prepared by the raw material of following weight percent:
Composite extract 30%
Adsorbent 24%
Vehicle 45%
Binder 1%.
The ratio of a kind of cigarette composite extract microcapsules, the composite extract and adsorbent is 1:0.8.
A kind of cigarette composite extract microcapsules, the adsorbent are commercially available porous, inorganic or organic material.
A kind of cigarette composite extract microcapsules, the adsorbent is by corncob, poriferous titanium dioxide according to mass ratio
2:1.5 mixing.
A kind of cigarette composite extract microcapsules, the vehicle is by chitosan, carragheen, gelatin, lactose, methyl
Cellulose is mixed according to quality 1.5:1.5:1:1:3.
A kind of cigarette composite extract microcapsules, the binder are hydroxypropyl methyl cellulose.
A kind of preparation method of cigarette composite extract microcapsules, comprising the following steps:
A, composite extract is slowly added in adsorbent, 10-30min is mixed, adsorbs adsorbent sufficiently compound
Extract；
B, vehicle, binder are added in the adsorbent for having adsorbed composite extract described in step A, are sufficiently mixed
Uniformly；
C, it is granulated, prepares composite extract microcapsules.
Embodiment 6
A kind of cigarette composite extract microcapsules, it is the spherical shape or irregular shape particle that granularity is 0.1-3mm, with institute
The composite extract stated is core material, is prepared by the raw material of following weight percent:
Composite extract 20%
Adsorbent 22%
Vehicle 57.5%
Binder 0.5%.
The ratio of a kind of cigarette composite extract microcapsules, the composite extract and adsorbent is 1:1.1.
A kind of cigarette composite extract microcapsules, the adsorbent are commercially available porous, inorganic or organic material.
A kind of cigarette composite extract microcapsules, the adsorbent are porous silica, corncob, porous silica
Titanium is mixed according to mass ratio 2:1:1.
A kind of cigarette composite extract microcapsules, the vehicle be microcrystalline cellulose, lactose, pectin in mass ratio
2:1:0.5 mixing.
A kind of cigarette composite extract microcapsules, the binder are hydroxypropyl methyl cellulose.
A kind of preparation method of cigarette composite extract microcapsules, comprising the following steps:
A, composite extract is slowly added in adsorbent, 25min is mixed, adsorbent is made sufficiently to adsorb compound collecting
Object；
B, vehicle, binder are added in the adsorbent for having adsorbed composite extract described in step A, are sufficiently mixed
Uniformly；
C, it is granulated, prepares composite extract microcapsules.
Embodiment 7
A kind of cigarette composite extract microcapsules, it is the spherical shape or irregular shape particle that granularity is 0.1-3mm, with institute
The composite extract stated is core material, is prepared by the raw material of following weight percent:
Composite extract 24.5%
Adsorbent 24.5%
Vehicle 50.4%
Binder 0.6%.
The ratio of a kind of cigarette composite extract microcapsules, the composite extract and adsorbent is 1:1.
A kind of cigarette composite extract microcapsules, the adsorbent are commercially available porous inorganic material.
A kind of cigarette composite extract microcapsules, the adsorbent are active carbon, carbon nanotube 2:1 in mass ratio mixing
It forms.
A kind of cigarette composite extract microcapsules, the vehicle are microcrystalline cellulose, chitosan, methylcellulose
3:1:1 is mixed in mass ratio.
A kind of cigarette composite extract microcapsules, the binder are carbohydrate.
A kind of preparation method of cigarette composite extract microcapsules, comprising the following steps:
A, composite extract is slowly added in adsorbent, 15min is mixed, adsorbent is made sufficiently to adsorb compound collecting
Object；
B, vehicle, binder are added in the adsorbent for having adsorbed composite extract described in step A, are sufficiently mixed
Uniformly；
C, it is granulated, prepares composite extract microcapsules.
Above-described embodiment is the preferable implementation of the present invention, and in addition to this, the present invention can be realized with other way,
Do not depart under the premise of present inventive concept it is any obviously replace it is within the scope of the present invention.
Claims (7)
1. a kind of cigarette composite extract microcapsules, it is characterised in that: it is the spherical shape or irregular shape that granularity is 0.1-3mm
Particle is prepared using composite extract as core material by the raw material of following weight percent:
The composite extract is prepared by the raw material of following parts by weight:
The preparation method of the composite extract, comprising the following steps:
(1) fresh passionflower, rambutan, citron, Calusena lansium, sea buckthorn fruit are carried out after weighing proportionally at whole fruit freeze-drying
It manages to constant weight；
(2) fruit after drying is crushed, grinding particle size is 10-20 mesh；
(3) smashed raw material is put into extraction kettle and carries out supercritical carbon dioxide extracting, extraction conditions are as follows: extraction kettle temperature
Degree: 40-50 DEG C, pressure: 25-35MPa；Separating still temperature: 30-40 DEG C, pressure: 5-8MPa；Extraction time: 2.5-3.5h；
(4) after supercritical extract from separating still isolated resin-like liquid, the dehydrated alcohol of 3-5 times of its weight is added, it is molten
16-24h under the conditions of placing -20 DEG C after solution filters to obtain supernatant, obtains grease A after removal solvent is concentrated under reduced pressure；
(5) pyracantha fortuneana leaf, persimmon leaves, mulberry leaves are weighed in proportion, 90-100 DEG C of hot water scalding 10-30 is put into after mixing
Second, 4-10 DEG C of cold water boshing is put into immediately, is dried, is extracted, Extraction solvent is the deionized water of 8-12 times of leaf weight,
Extracting temperature is 60-80 DEG C, time 2.5-3.5h, repeats to extract primary, filtering, it is 1.200- that filtrate, which is concentrated into relative density,
1.300 medicinal extract B；
(6) grease A and medicinal extract B is mixed, the hydrophily Glycerin, mixed triester with caprylic acid capric acid of both 1 times mixed weight is added, is dispersed with stirring
After filter, obtain composite extract.
2. a kind of cigarette composite extract microcapsules according to claim 1, it is characterised in that: the adsorbent is commercially available
Porous, inorganic or organic material.
3. a kind of cigarette composite extract microcapsules according to claim 2, it is characterised in that: the adsorbent is porous
The mixture of one or more of starch, porous silica, active carbon, corncob, poriferous titanium dioxide, carbon nanotube.
4. a kind of cigarette composite extract microcapsules according to claim 1, which is characterized in that the vehicle includes
Microcrystalline cellulose, starch, maltodextrin, sucrose, lactose, chitosan, carragheen, gelatin, pectin, methylcellulose, ethyl are fine
Tie up the mixture of one or more of element.
5. a kind of cigarette composite extract microcapsules according to claim 1, it is characterised in that: the binder includes carboxylic
It is sodium carboxymethylcellulose pyce, hydroxypropyl methyl cellulose, any in carbohydrate.
6. a kind of preparation method of cigarette as described in claim 1-5 any one with composite extract microcapsules, feature
It is: the following steps are included:
A, composite extract is slowly added in adsorbent, 10-30min is mixed, adsorbent is made sufficiently to adsorb compound collecting
Object；
B, vehicle, binder are added in the adsorbent for having adsorbed composite extract described in step A, are sufficiently mixed
It is even；
C, it is granulated, prepares composite extract microcapsules.
7. a kind of preparation method of cigarette composite extract microcapsules according to claim 6: being made described in step C
Grain method is fluidized bed prilling, squeeze out-it is round as a ball granulation, wet granulation, any in non-slurry pelletizing.
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| CN107212459B (en) * | 2017-05-31 | 2018-12-14 | 东南大学 | A kind of preparation method being sustained tobacco aromaticss microcapsules |
| CN108497546B (en) * | 2018-03-22 | 2021-03-19 | 宝可科技（上海）有限公司 | Additive for cigarette and preparation method and application thereof |
| CN109793269A (en) * | 2019-01-30 | 2019-05-24 | 湖北中烟工业有限责任公司 | Preparation method and application for the floral type tow in Novel heating not burning tobacco |
| CN109645561A (en) * | 2019-02-18 | 2019-04-19 | 重庆中烟工业有限责任公司 | Cigarette capsule and preparation method thereof and cigarette filter |
| CN109619673B (en) * | 2019-02-18 | 2022-02-18 | 重庆中烟工业有限责任公司 | Sustained-release capsule for cigarette, preparation method thereof and cigarette filter |
| CN110101130A (en) * | 2019-06-26 | 2019-08-09 | 红云红河烟草(集团)有限责任公司 | It is a kind of to heat the cigarette that do not burn |
| CN110564504A (en) * | 2019-08-30 | 2019-12-13 | 重庆中烟工业有限责任公司 | Cigarette essence containing clausena lansium extract, preparation method and application |
| CN115261133A (en) * | 2022-07-20 | 2022-11-01 | 深圳波顿香料有限公司 | Method for preparing natural spice refined substance for cigarettes with low Pb and As contents |
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Denomination of invention: Compound extract for cigarette, microcapsule containing extract and preparation methods thereof Effective date of registration: 20200727 Granted publication date: 20190712 Pledgee: China Co. truction Bank Corp Dongguan branch Pledgor: DONGGUAN BOTON FLAVORS & FRAGRANCES Co.,Ltd. Registration number: Y2020980004381 |
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