CN106617289A - Harm-reducing cigarette filter additive and filter preparation method - Google Patents
Harm-reducing cigarette filter additive and filter preparation method Download PDFInfo
- Publication number
- CN106617289A CN106617289A CN201710079036.7A CN201710079036A CN106617289A CN 106617289 A CN106617289 A CN 106617289A CN 201710079036 A CN201710079036 A CN 201710079036A CN 106617289 A CN106617289 A CN 106617289A
- Authority
- CN
- China
- Prior art keywords
- cigarette
- filter
- harm
- filter tip
- polyethylene glycol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a cigarette filter additive capable of reducing harmful ingredients in cigarette smoke and a filter preparation method thereof. The cigarette filter additive and the filter preparation method are mainly characterized in that raw materials, namely polyethylene glycol 200 (1-20 parts by weight) and a passion fruit extract (1-10 parts by weight) are uniformly sprayed on acetate cellulose tows (100 parts by weight) by virtue of a constant-flow pump, a cigarette filter is formed by coiling the tows and then the cigarette filter is spliced, so that a cigarette is obtained. With the application of the cigarette filter additive provided by the invention, release amount of such harm ingredients as tar, hydrogen cyanide, phenol and the like in the cigarette smoke and a cigarette harmful index can be obviously reduced, so that the spicy stimulation of the smoke to smokers' respiratory systems can be effectively relieved, respiratory diseases can be reduced and smoking harmfulness can be reduced.
Description
Technical field
The present invention relates to a kind of cigarette additives of filter tip and its filter tip preparation method for reducing harmful constituents in cigarette flue gas,
Specifically related to reduce the harmful constituents in cigarette flue gas such as additive of tar, Blausure (German), phenol etc. and its filter tip preparation method.
Technical background
Smoking is harmful to your health, it appears that is a well known fact.Because the Health cost that smoking is caused has for a long time
The characteristics of hysteresis quality, relevant disease could occur after smoking 10 years, 20 years or even longer time, so before disease occurs,
Smoker is often recognized less than harm of smoking.In fact, Cigarette burning is the chemical system of a complexity.Grind according to science
Study carefully discovery, during cigarette is lighted, when temperature rises to 300 DEG C, the volatile ingredient in tobacco shred starts to volatilize and shape
Into flue gas；When rising to 450 DEG C, tobacco shred starts coking；When temperature rises to 600 DEG C, cigarette is ignited and starts burning, burning
Produced chemical composition species is thousands of.Although most of chemical composition is harmless, it is harmful in flue gas
Divide such as Blausure (German), ammonia and phenol, it is very harmful although content is micro.In recent years, Chinese scholars are in Harm reduction techniques technology
Research field is done a lot of work, and certain effect is particularly achieved in terms of the filter plug of Medicated cigarette, but the achievement studied is being answered
Report that less, progress slows down with aspect.Trace it to its cause one be harm reduction material harm reduction effect it is limited, two be harm reduction material itself into
It is applied the restriction of this height enterprise, and three is that some effective harm reduction materials do not meet production of cigarettes safety licensing requirement.At present, I
The level of state's harm reduction technology can't fully meet the needs of China's current development Chinese-style cigarette, lack the selectivity of relative maturity
The strong selective harm reduction technology of height, good stability, industrial usability, using the Less harmful cigarette brand of harm reduction technical research achievement
Few, market share is little, and power of influence is weak.
From 2005, State Tobacco Monopoly Bureau organized Medicated cigarette hazardness index number system research work.Choose domestic
Outer 163 kinds of trades mark (specification) Medicated cigarette, determines the main harmful components of Hoffmann analytes (tar, CO, cigarette in its main flume
Alkali, hydrocyanic acid, ammonia, nitrogen oxides, 3 kinds of polycyclic aromatic hydrocarbons, 4 grow tobacco unique nitrosamine, 8 kinds of volatile carbonyl compounds and 7 kinds
Volatile phenolics) (test of animal acute fatal, antibacterial lure for 4 toxicologic index of burst size and cigarette mainstream flue gas
Become analysis, the mammalian cell analysis of cytogeneticss/mutation and cytotoxicity analysis).Various mathematical statistics methods are selected,
Analysis, the dependency relation for excavating main flume harmful components and toxicologic index, finally filter out CO, HCN, NNK, NH3, benzo
[α] pyrene, phenol, 7 indexs of crotonic aldehyde are characterizing cigarette mainstream flue gas biohazardous.At present, there is not yet reducing Medicated cigarette harm
The correlational study report of sex index.
The content of the invention
It is to disclose a kind of harm reduction type cigarette additives of filter tip that the present invention needs one of problem for solving, and is applied to energy in Medicated cigarette
Enough reduce the harmful constituents in cigarette flue gas such as composition such as tar, Blausure (German) and phenol and with CO, HCN, NNK, NH3, benzo [α]
Pyrene, phenol, 7 indexs of crotonic aldehyde are characterizing the harm sex index of cigarette mainstream flue gas biohazardous, improve cigarette smoking product
Matter, prevent or alleviate by smoking cause various diseases, with overcome prior art exist defect.
It is the preparation side for disclosing above-mentioned cigarette additives of filter tip and cigarette filter tip that the present invention needs the two of the problem for solving
Method, in order to industrialized production.
Preparing harm reduction type cigarette additives of filter tip and primary raw material used by cigarette filter tip is：
Passifolra edulis extractum (0.1～5 weight portion), polyethylene glycol 200 (1～20 weight portion) and acetate silk (100 weights
Amount part) etc. raw material composition.
The preparation method of Passifolra edulis extractum is：
(1) in 100 parts of fresh Passifolra edulis sarcocarp add 0.1-1 parts compound enzymic preparation (compound enzymic preparation for neutrality
One or more in protease, pectase, saccharifying enzyme), add 500-1000 part deionized waters, merceration 24- after stirring
48h.Clear liquid is leached, adds the ethanol of 300-500 parts 95%, the cold preservation 24-48h under -4 DEG C of environment to filter, by filtrate in filtrate
Concentration obtains final product Passifolra edulis extractum.
(2) taking a certain amount of Passifolra edulis extractum (1-10 parts), to be dissolved in a certain amount of polyethylene glycol 200 (50-200 parts) molten
In liquid, mix homogeneously forms cigarette filter-tip additive agent, by cigarette filter production and processing technology requirement, is uniformly sprayed at acetic acid
On fibre bundle and roll into cigarette.The usage amount of cigarette filter-tip additive agent is the 0.5～5% of cigarette filter weight.
The preparation method of cigarette additives of filter tip and cigarette filter tip is：
(1) by the polyethylene glycol 200 of different proportion and Passifolra edulis extractum mix homogeneously.
(2) acetate silk is loosed off with opener.
(3) polyethylene glycol 200 and Passifolra edulis extractum mixed liquor are sprayed on acetate silk with constant flow pump.
(4) acetate silk for being coated with polyethylene glycol 200 and Passifolra edulis extractum with filter forming machine rolls into cigarette
Use filter tip.
Cigarette additives of filter tip of the present invention is polyethylene glycol 200 and Passifolra edulis extractum, wherein polyethylene glycol 200
Purity is more than 99.5%.
The pharmacology and effect of the main constituents of cigarette additives of filter tip of the present invention be：
(1) polyethylene glycol 200
Polyethylene glycol 200, sterling is colourless liquid, nontoxic, nonirritant, with good water solublity, and is had with many
Machine thing component has good intermiscibility.They have excellent lubricity, moisture retention, dispersibility, bonding agent, antistatic additive and soft
Soft dose etc., in cosmetics, pharmacy, chemical fibre, rubber, plastics, papermaking, paint, plating, pesticide, intermetallic composite coating and food processing etc.
There is extremely wide application in industry.It is to reduce cigarette smoke to add the material purposes such as Polyethylene Glycol in cigarette filter
Middle harmful components, improve the quality of cigarette smoking, reduce harm of the smoking to human body.
(2) Passifolra edulis extractum
Passifolra edulis, also known as Passiflora edulis sims, are the herbaceous species plants of Passifloraceae Passiflora, can really eat raw or make vegetable,
Feedstuff.It is used as medicine with excited, strong effect.Seed extracts oil, can edible and soapmaking, liquefaction paint etc..Passifolra edulis contain abundant
Vitamin, superfluorescent fiber and protein, the most trickle part of the deep enough human body the intestines and stomach of superfluorescent fiber energy, by its active gene absorber
Interior harmful substance by its thorough discharge, and can improve the flora in intestinal composition, carry out profound level cleaning and toxin expelling, but and
There will not be any infringement to intestinal wall.The VC that is rich in Passifolra edulis in addition, carotene, SOD enzymes can remove interior free yl, rise
Face nourishing antidebilitation is acted on.
Therefore, effective ingredient shows that the human body mechanism of action it contributes to reducing main in cigarette smoke in Passifolra edulis extract
Want harmful components such as free radical, polycyclic aromatic hydrocarbon, nitrous ammonium etc..
The extraction process of Passifolra edulis extractum employs ferment treatment and combines decoction and alcohol sedimentation technique, on the one hand because of Passifolra edulis effective ingredient
Major part belongs to the hydrotrope, and water makees extractant can farthest be extracted effective ingredient, and adds a certain amount of multiple
Synthase preparation is to hydrolyze the macro-molecular protein in Passifolra edulis, contributes to the increase of fragrance matter.On the other hand second is added
Alcohol is by species precipitates such as the macro-molecular proteins and pectin of non-complete hydrolysis and leaches that these materials are in tobacco aromatics using
The too high aesthetic quality that can affect Medicated cigarette of content.
The cigarette additives of filter tip principal character of the present invention is reduction of harmful constituents in cigarette flue gas such as tar, cyaniding
The burst size of the compositions such as hydrogen, ammonia and phenol and Medicated cigarette harm sex index, effectively reduce flue gas to smoker's respiratory system
Pungent stimulation, reduces respiratory tract disease, mitigates harm of smoking.
Specific embodiment
The present invention will be further described as follows with embodiment, and as a result such as table 1, but the scope of the invention is certainly not limited to
These embodiments.
Embodiment 1
With constant flow pump just 10 weight portion polyethylene glycol 200s：Passifolra edulis extractum (20:1 weight ratio) mixed solution is sprayed at
On 100 parts by weight acetic acid fibre bundles of shredding, by cigarette filter production and processing technology requirement, it is coated with filter forming machine
The acetate silk of polyethylene glycol 200 and Passifolra edulis extractum mixed solution rolls into cigarette filter plug, and rolls into cigarette.It is close
Envelope is preserved 24 hours, and by country or industry standard methods coal-tar middle oil cigarette smoke, carbon monoxide, nicotine, hydrocyanic acid, nitrous are determined
Amine (NNK), ammonia, benzo [α] pyrene, phenol, the content of crotonic aldehyde.As a result show：Compared with control Medicated cigarette, cigarette smoke is tested
Middle carbon monoxide release amount reduction rate -2.3%, Blausure (German) (HCN) burst size reduction rate 8.3%, nitrosamine (NNK) burst size drop
Low rate -6.8%, ammonia (NH3) burst size reduction rate -2.9%, benzopyrene (B [a] P) burst size reduction rate 5.6%, phenol is released
High-volume reduction rate 9.0%；Crotonaldehyde release amount reduction rate 4.6%, the burst size reduction rate of seven harmful components adds up to 15%,
Overall harm sex index reduces by 0.2, while cigarette smoke is coal-tar middle oil to reduce 1.3mg/ cigarette.
Embodiment 2
With constant flow pump just 10 weight portion polyethylene glycol 200s：Passifolra edulis extractum (15:1 weight ratio) mixed solution is sprayed at
On 100 parts by weight acetic acid fibre bundles of shredding, by cigarette filter production and processing technology requirement, it is coated with filter forming machine
The acetate silk of polyethylene glycol 200 and Passifolra edulis extractum mixed solution rolls into cigarette filter plug, and rolls into cigarette.It is close
Envelope is preserved 24 hours, and by country or industry standard methods coal-tar middle oil cigarette smoke, carbon monoxide, nicotine, hydrocyanic acid, nitrous are determined
Amine (NNK), ammonia, benzo [α] pyrene, phenol, the content of crotonic aldehyde.As a result show：Compared with control Medicated cigarette, cigarette smoke is tested
Middle carbon monoxide release amount reduction rate -3.8%, Blausure (German) (HCN) burst size reduction rate 2.7%, nitrosamine (NNK) burst size drop
Low rate 0%, ammonia (NH3) burst size reduction rate -8.7%, benzopyrene (B [a] P) burst size reduction rate 7.8%, phenol release amount
Reduction rate 17.3%；Crotonaldehyde release amount reduction rate 5.1%, the burst size reduction rate of seven harmful components adds up to 21%, always
Body harm sex index reduces by 0.3, while cigarette smoke is coal-tar middle oil to reduce 0.6mg/ cigarette.
Embodiment 3
With constant flow pump just 10 weight portion polyethylene glycol 200s：Passifolra edulis extractum (10:1 weight ratio) it is sprayed at the 100 of shredding
On parts by weight acetic acid fibre bundle, by cigarette filter production and processing technology requirement, with filter forming machine Polyethylene Glycol is coated with
200 and the acetate silk of Passifolra edulis extractum mixed solution roll into cigarette filter plug, and roll into cigarette.Sealing preserve 24
Hour, determine that cigarette smoke is coal-tar middle oil by country or industry standard methods, carbon monoxide, nicotine, hydrocyanic acid, nitrosamine (NNK),
Ammonia, benzo [α] pyrene, phenol, the content of crotonic aldehyde.As a result show：Compared with control Medicated cigarette, an oxidation in test cigarette smoke
Carbon emissions amount reduction rate -3.0%, Blausure (German) (HCN) burst size reduction rate 5.0%, nitrosamine (NNK) burst size reduction rate 0%,
Ammonia (NH3) burst size reduction rate 11.6%, benzopyrene (B [a] P) burst size reduction rate 4.5%, phenol release amount reduction rate
18.8%；Crotonaldehyde release amount reduction rate -0.5%, the burst size reduction rate of seven harmful components adds up to 36.4%, overall danger
Evil sex index reduces by 0.4, while cigarette smoke is coal-tar middle oil to reduce 1.0mg/ cigarette.
Table 1 cigarette mainstream flue gas, three indexs
Harm sex index=(CO/14.2+HCN/146.3+NNK/5.5+NH3/8.1+B [a] P/10.9+ phenol/17.4+
Crotonic aldehyde/18.6) * 10/7.
Claims (3)
1. a kind of harm reduction type cigarette additives of filter tip and cigarette filter tip, it is characterised in that primary raw material used includes：1～20 weight
Amount part polyethylene glycol 200,1～10 weight portion Passifolra edulis extractum and 100 parts by weight acetic acid fibre bundles；Wherein polyethylene glycol 200
Purity more than 99.5%.
2. the preparation method of harm reduction type cigarette additives of filter tip as claimed in claim 1 and cigarette filter tip, is characterized in that：First
By the polyethylene glycol 200 of different proportion and Passifolra edulis extractum mix homogeneously；Secondly opener looses off acetate silk；
Then polyethylene glycol 200 and Passifolra edulis extractum mixed solution are sprayed on acetate silk with constant flow pump；Finally use filter tip
Forming machine is coated with the acetate silk of Polyethylene Glycol and Passifolra edulis extractum mixed solution and rolls into cigarette filter plug.
3. the Medicated cigarette of addition harm reduction type cigarette additives of filter tip as claimed in claim 1 or 2 and cigarette filter tip, is characterized in that：
Reduce the harmful constituents in cigarette flue gas such as burst size of the composition such as tar, cigarette Blausure (German), ammonia and phenol and Medicated cigarette harm
Sex index, effectively reduces pungent stimulation of the flue gas to smoker's respiratory system, reduces respiratory tract disease, mitigates harm of smoking
Property.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710079036.7A CN106617289A (en) | 2017-02-14 | 2017-02-14 | Harm-reducing cigarette filter additive and filter preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710079036.7A CN106617289A (en) | 2017-02-14 | 2017-02-14 | Harm-reducing cigarette filter additive and filter preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106617289A true CN106617289A (en) | 2017-05-10 |
Family
ID=58845201
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710079036.7A Pending CN106617289A (en) | 2017-02-14 | 2017-02-14 | Harm-reducing cigarette filter additive and filter preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106617289A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN101433620A (en) * | 2008-12-10 | 2009-05-20 | 广东省农业科学院农业生物技术研究所 | Longan water-soluble active substance as well as extraction method and use thereof |
| CN202035470U (en) * | 2010-06-13 | 2011-11-16 | 湖南中烟工业有限责任公司 | Function forming paper filtering rod |
| CN102811632A (en) * | 2009-12-21 | 2012-12-05 | 英美烟草(投资)有限公司 | Sheet Filter Materials With Additives |
| CN104351946A (en) * | 2014-10-22 | 2015-02-18 | 浙江中烟工业有限责任公司 | Cigarette filter rod for selectively reducing phenol content in smoke gas of cigarettes as well as preparation method and application of cigarette filter rod |
| CN104611136A (en) * | 2014-12-24 | 2015-05-13 | 杨秋慧 | Cigarette essence prepared by utilization of passion fruit and preparing method thereof |
-
2017
- 2017-02-14 CN CN201710079036.7A patent/CN106617289A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN101433620A (en) * | 2008-12-10 | 2009-05-20 | 广东省农业科学院农业生物技术研究所 | Longan water-soluble active substance as well as extraction method and use thereof |
| CN102811632A (en) * | 2009-12-21 | 2012-12-05 | 英美烟草(投资)有限公司 | Sheet Filter Materials With Additives |
| CN105661639A (en) * | 2009-12-21 | 2016-06-15 | 英美烟草(投资)有限公司 | Sheet filter materials with additives |
| CN202035470U (en) * | 2010-06-13 | 2011-11-16 | 湖南中烟工业有限责任公司 | Function forming paper filtering rod |
| CN104351946A (en) * | 2014-10-22 | 2015-02-18 | 浙江中烟工业有限责任公司 | Cigarette filter rod for selectively reducing phenol content in smoke gas of cigarettes as well as preparation method and application of cigarette filter rod |
| CN104611136A (en) * | 2014-12-24 | 2015-05-13 | 杨秋慧 | Cigarette essence prepared by utilization of passion fruit and preparing method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 许春平 张峻松 主编: "《烟草专业英语》", 30 November 2012 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101411543B (en) | Method for preparing flavoring for cigarette and use | |
| CN105595417B (en) | Linear composite gel fragrance controlled-release filter stick and preparation method and application thereof | |
| CN105062674A (en) | Preparation method of tobacco microcapsule spearmint oil | |
| CN107136555B (en) | The method that proline solid phase Maillard reaction improves stem organoleptic quality | |
| CN105558115A (en) | Preparation method of red tea | |
| CN110283661A (en) | A kind of quick-fried pearl of cigarette gel and preparation method thereof | |
| CN103462212B (en) | Method for improving quality of tobacco leaves by adding enzyme preparation, glucose and citric acid | |
| CN101768514A (en) | Alhagi sparsifolia extract and preparation method and application thereof | |
| CN101856144B (en) | Method for improving quality of cigarette tobacco shreds | |
| CN108634362B (en) | Preparation method and application of composite type tobacco flavor enhancer | |
| RU2313999C1 (en) | Smoking mixture | |
| CN107495462B (en) | Method for improving tobacco quality and reducing harmful substances | |
| CN104188090A (en) | Method for reducing carbonic oxide emission of paper-making reconstituted tobacco | |
| CN108354848A (en) | A kind of dregs of grape wine clay mask and preparation method thereof | |
| CN102757864B (en) | Method for preparing essence fragrance used in rue cigarette | |
| CN106617289A (en) | Harm-reducing cigarette filter additive and filter preparation method | |
| CN103126058B (en) | Non-toxic cigarette produced by Moringa tree (Cinnamomum kotoense) trunks | |
| CN207544325U (en) | A kind of harm reduction type cigarette filter tip rod | |
| CN115281363A (en) | Fragrance base module with effects of softening and reducing thorn, preparation method thereof and application of fragrance base module in cigarettes | |
| CN104138027B (en) | tobacco humectant | |
| KR930000313B1 (en) | Process for preparing tobacco | |
| CN113057369A (en) | Paper filter stick and preparation method thereof | |
| CN113749277A (en) | Atomized liquid with ambergris fragrance and preparation method thereof | |
| CN107384838B (en) | Microbial preparation for improving tobacco quality | |
| CN101342008B (en) | Low-harm cigarette |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170510 |