CN110819458A - Preparation method and application of passion fruit tobacco essence - Google Patents
Preparation method and application of passion fruit tobacco essence Download PDFInfo
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- CN110819458A CN110819458A CN201911088077.8A CN201911088077A CN110819458A CN 110819458 A CN110819458 A CN 110819458A CN 201911088077 A CN201911088077 A CN 201911088077A CN 110819458 A CN110819458 A CN 110819458A
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 241000208125 Nicotiana Species 0.000 claims abstract description 33
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 33
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 26
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 21
- 238000000605 extraction Methods 0.000 claims abstract description 15
- 239000003571 electronic cigarette Substances 0.000 claims abstract description 14
- 238000000199 molecular distillation Methods 0.000 claims abstract description 14
- 238000004821 distillation Methods 0.000 claims abstract description 13
- 238000002791 soaking Methods 0.000 claims abstract description 9
- 239000002904 solvent Substances 0.000 claims abstract description 9
- 238000001914 filtration Methods 0.000 claims abstract description 7
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- 238000004140 cleaning Methods 0.000 claims abstract description 4
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 21
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Botany (AREA)
- Agronomy & Crop Science (AREA)
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Abstract
The invention discloses a preparation method and application of passion fruit tobacco essence. The preparation method comprises the following steps: cleaning passion fruit, selecting, removing peel and shell to obtain pulp juice containing kernel; adding an extraction solvent into the pulp juice, and standing and soaking at normal temperature; performing ultrasonic wall breaking on the soaked passion fruit pulp juice, filtering and concentrating to obtain a passion fruit extract; adding the passion fruit extract into a molecular distillation apparatus for distillation, and reserving distillate flowing out along the wall of a vacuum cavity; and adding the distillate into the ethanol solution, and uniformly stirring to obtain the passion fruit tobacco essence. The preparation method of the invention can retain and enrich natural aroma components of the passion fruit, greatly shortens extraction time, is simple and easy to implement and is easy for industrial production. The essence of the invention has natural, mellow and strong fragrance. When the passion fruit tobacco essence is applied to cigarettes or electronic cigarettes, the smoke quality can be improved, the fragrance of the cigarettes is increased, and the miscellaneous gas in tobacco tar can be effectively covered.
Description
Technical Field
The invention belongs to the technical field of tobacco essence and flavor, and particularly relates to a preparation method and application of passion fruit tobacco essence.
Background
With the increasing social concern on smoking and health, cigarette safety is improved, and the development of low-tar cigarettes has become a main attack direction and development trend in the tobacco industry. At present, cigarette markets at home and abroad require cigarette commodities with the attributes of high fragrance, high concentration and low tar.
Passion fruit is originally produced in south America and is named as passion fruit and eggfruit, and the pulp of passion fruit can emit rich fragrance of more than ten kinds of fruits such as banana, pineapple, strawberry, litchi, lemon, mango, plum and the like. The passion fruit has the magical effects of diminishing inflammation, relieving pain, promoting blood circulation, strengthening the body, reducing blood fat and blood pressure, nourishing yin, tonifying the kidney, refreshing, sobering up, eliminating fatigue, protecting skin, beautifying and the like.
At present, the passion fruit essence perfume on the market has the fragrance of various fruits, most of the passion fruit essence perfumes are artificially synthesized, and the fragrance of the passion fruit essence perfume is different from that of natural passion fruit perfume. The natural passion fruit spice is fragrant and natural, and has mellow and strong fragrance.
Chinese patent 201310386825.7 discloses a preparation method of a special fertilizer for passion fruit, which takes passion fruit fallen leaves and kitchen garbage as main raw materials, can change waste into valuable, reduces the environmental pollution of waste, and has good fertilizer effect by adding enzyme bacteria for fermentation.
Chinese patent 201510733794.7 discloses a method for extracting passion fruit extract, comprising the steps of: the method comprises the following steps of cleaning passion fruits, crushing, soaking, wall breaking, warm water soaking, centrifuging, filtering to obtain a supernatant, and concentrating the obtained supernatant to obtain a target product, wherein the target product is applied to hair care products.
Chinese patent 201610557454.8 discloses a preparation method of passion fruit extract and application of the prepared product. By utilizing a cold soaking technology and a falling film concentration technology, effective aroma components of the passion fruit can be effectively improved, head aroma components are effectively reserved, the aroma is more vivid, the mouthfeel is better, and the aroma components of the passion fruit are damaged to a certain extent by crushing pulp and nutlets by using a juice extractor.
Although the purpose of the above patents is to comprehensively utilize passion fruit, the extraction of the passion fruit for tobacco flavor is not utilized, and no report is found about the extraction technology of the passion fruit for tobacco flavor. Therefore, the invention develops a preparation method and application of the passion fruit tobacco essence.
Disclosure of Invention
In order to solve the technical problems, the invention provides a preparation method and application of an essence for passion fruit cigarettes. The passion fruit cigarette essence has natural, mellow and strong fragrance. The passion fruit cigarette flavor is sprayed into cigarette tobacco shreds, so that the smoke quality can be improved, the cigarette aroma can be increased, the cigarette smoke is rich, sweet and mellow, the thorns and impurities are inhibited and reduced, and the characteristics of enriching the smoke aroma, enhancing the sweet feeling of the smoke and the like are achieved; when the electronic cigarette liquid is added into the electronic cigarette liquid, the electronic cigarette can be endowed with elegant and natural passion fruit fragrance, the fragrance is fresh and elegant, the fragrance quality of the electronic cigarette is improved, and miscellaneous gas in tobacco tar is effectively covered.
In order to achieve the purpose, the invention adopts the following technical scheme:
a preparation method of an essence for passion fruit cigarettes comprises the following steps:
(1) cleaning the passion fruit, selecting the well-cooked passion fruit, removing peel and shell of the passion fruit to obtain pulp juice containing fruit pits;
(2) adding an extraction solvent into the fruit pulp juice, and standing and soaking for 24-48 h at normal temperature;
(3) carrying out ultrasonic wall breaking on the passion fruit pulp juice soaked in the step (2), filtering and concentrating to obtain a passion fruit extract;
(4) adding the obtained passion fruit extract into a molecular distillation apparatus for distillation, setting the distillation temperature of molecular distillation equipment to be 40-50 ℃, the material flow rate to be 1-2 ml/min, the film scraping rotation speed to be 40-60 r/min, and the vacuum degree to be 20-30 Pa, and keeping distillate flowing out along the wall of a vacuum cavity;
(5) and adding the distillate into a 75% ethanol solution, and uniformly stirring to obtain the passion fruit tobacco essence.
Further, the extraction solvent in the step (2) is a mixed solvent of 95% ethanol and propylene glycol, and the weight ratio of the extraction solvent to the propylene glycol is 1: 1-3: 1.
Further, the weight ratio of the extraction solvent to the passion fruit pulp juice in the step (2) is 3: 1-6: 1.
Further, the ultrasonic power in the step (3) is 500-800W, and the ultrasonic time is 1-2 h.
Further, the concentration treatment in the step (3) is carried out by adopting a rotary evaporator under the conditions that the vacuum degree is 0.090-0.095 Mpa and the temperature is 40-45 ℃.
Further, the distillation temperature of the molecular distillation in the step (4) is 45 ℃, the material flow rate is 2ml/min, the film scraping rotation speed is 50r/min, and the vacuum degree is 25 Pa.
Further, the weight ratio of the distillate obtained in the step (5) to 75% ethanol is 6: 4-7: 3.
According to the invention, the effective components of the passion fruit are more fully extracted through the unique physical properties of ultrasonic waves, the aroma components are more greatly reserved, the extraction time is greatly shortened, and the method is simple and easy to operate; the passion fruit extract is treated by molecular distillation, so that the aroma components of the passion fruit extract are enriched greatly, and the obtained passion fruit cigarette essence has natural, mellow and strong aroma.
The invention also provides the essence prepared by the preparation method of the passion fruit cigarette essence.
The invention also provides application of the essence in cigarettes or electronic cigarettes.
The invention has the beneficial effects that:
(1) compared with the traditional extraction method, the preparation method of the passion fruit tobacco essence provided by the invention can better retain and enrich the natural aroma components of the passion fruit, the extraction time is greatly shortened, and the method is simple and easy to operate.
(2) The passion fruit tobacco essence obtained by the preparation method provided by the invention is sprayed into cigarette tobacco shreds, so that the smoke quality can be improved, the cigarette fragrance is increased, the cigarette smoke is rich, sweet and mellow, and the characteristics of enriching the smoke fragrance, enhancing the sweet feeling of the smoke and the like are achieved. The passion fruit tobacco essence prepared in the embodiment is added into the electronic cigarette liquid, so that the electronic cigarette can be endowed with elegant and natural passion fruit fragrance, the fragrance is fresh and elegant, the fragrance quality of the electronic cigarette is improved, and the miscellaneous gas in tobacco tar is effectively covered.
(3) The method has mild reaction conditions, low cost and easy industrial production; and the method provided by the invention has no harmful substance addition and generation, and has no harm to the environment.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions of the embodiments of the present invention will be clearly and completely described below. It is to be understood that the embodiments described are only a few embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the described embodiments of the invention without any inventive step, are within the scope of protection of the invention.
Unless defined otherwise, technical or scientific terms used herein shall have the ordinary meaning as understood by one of ordinary skill in the art to which this invention belongs.
Embodiment 1 a method for preparing an essence for passion fruit cigarettes comprises the following steps:
a. selecting 20kg of ripe passion fruit, removing peel and shell to obtain 4.5kg of pulp juice containing kernels;
b. adding 6.75kg of 95% ethanol and 6.75kg of propylene glycol into the pulp juice, mixing, standing at room temperature, and soaking for 24 hr
c. Performing ultrasonic wall breaking on the soaked passion fruit pulp juice, wherein the ultrasonic power is 600W, the ultrasonic time is 1h, filtering an ultrasonic extracting solution, taking out a filtrate, and concentrating the filtrate at 45 ℃ under the condition that the vacuum degree is 0.090 Mpa to obtain a passion fruit extract, wherein the relative water density of the passion fruit extract is 1.041;
d. c, adding the passion fruit extract obtained in the step c into a molecular distillation apparatus for distillation, setting the distillation temperature of molecular distillation equipment to be 45 ℃, the material flow rate to be 2ml/min, the film scraping rotation speed to be 50r/min, the vacuum degree to be 25Pa, and keeping the passion fruit distilled light component flowing out along the wall of the vacuum cavity, wherein the relative water density of the passion fruit distilled light component is 1.038;
e. adding 70g of the passion fruit distilled and distilled light component into 30g of 75% ethanol, and uniformly stirring to obtain the passion fruit tobacco essence 1.
Embodiment 2 a method for preparing an essence for passion fruit cigarettes comprises the following steps:
a. selecting 20kg of ripe passion fruit, removing peel and shell to obtain 4.5kg of pulp juice containing kernels;
b. adding 11.25kg of 95% ethanol and 11.25kg of propylene glycol into the pulp juice, mixing, standing at room temperature, and soaking for 36 hr
c. Performing ultrasonic wall breaking on the soaked passion fruit pulp juice, wherein the ultrasonic power is 700W, the ultrasonic time is 1.5h, filtering the ultrasonic extracting solution, taking out the filtrate, and concentrating the filtrate at 40 ℃ under the condition that the vacuum degree is 0.090 Mpa to obtain a passion fruit extract, wherein the relative water density of the passion fruit extract is 1.042;
d. c, adding the passion fruit extract obtained in the step c into a molecular distillation apparatus for distillation, setting the distillation temperature of molecular distillation equipment to be 40 ℃, the material flow rate to be 2ml/min, the film scraping rotation speed to be 40r/min, the vacuum degree to be 20Pa, and keeping the passion fruit distilled light component flowing out along the wall of the vacuum cavity, wherein the relative water density of the passion fruit distilled light component is 1.039;
e. adding 60g of the passion fruit distilled and distilled light component into 40g of 75% ethanol, and uniformly stirring to obtain the passion fruit tobacco essence 2.
Embodiment 3, a preparation method of an essence for passion fruit cigarettes comprises the following steps:
a. selecting 20kg of ripe passion fruit, removing peel and shell to obtain 4.5kg of pulp juice containing kernels;
b. adding 18kg of 95% ethanol and 9kg of propylene glycol into the pulp juice, mixing, standing at room temperature, and soaking for 48 hr
c. Performing ultrasonic wall breaking on the soaked passion fruit pulp juice, wherein the ultrasonic power is 800W, the ultrasonic time is 5h, filtering an ultrasonic extracting solution, taking out a filtrate, and concentrating the filtrate at 50 ℃ under the condition that the vacuum degree is 0.090 Mpa to obtain a passion fruit extract, wherein the relative water density of the passion fruit extract is 1.042;
d. c, adding the passion fruit extract obtained in the step c into a molecular distillation apparatus for distillation, setting the distillation temperature of molecular distillation equipment to be 45 ℃, the material flow rate to be 2ml/min, the film scraping rotation speed to be 50r/min, the vacuum degree to be 30Pa, and keeping the passion fruit distilled light component flowing out along the wall of the vacuum cavity, wherein the relative water density of the passion fruit distilled light component is 1.039;
e. 65g of the passion fruit distilled and distilled light component is added into 35g of 75% ethanol, and the mixture is uniformly stirred to obtain the passion fruit tobacco essence 3.
Example 4
The passion fruit essence 1 for cigarette, the passion fruit essence 2 for cigarette and the passion fruit essence 3 for cigarette prepared in the above examples 1-3 are flavored, the same application proportion is carried out under the same condition, the applied samples are subjected to sensory comparison smoking evaluation, 9 members of a sensory smoking evaluation group adopt GB5606.4-2005, the smoking evaluation standard adopts GB5606.4-2005, the average value of smoking evaluation results is shown in tables 1, 2 and 3. The application proportion is the weight percentage of the tobacco shreds.
Table 1: sensory evaluation result at an application rate of 0.05%
Table 2: sensory evaluation result at an application rate of 0.10%
Table 3: sensory evaluation result at an application rate of 0.15%
As can be seen from the sensory evaluation results in tables 1-3, the essence for passion fruit cigarettes provided by the invention can be sprayed into the cut tobacco of the cigarettes, so that the smoke quality can be improved, the fragrance of the cigarettes is increased, the smoke of the cigarettes is rich, sweet and mellow, and the effects of enriching the smoke fragrance and enhancing the sweet feeling of the smoke are achieved.
Example 5
The essence for the passion fruit cigarette prepared in the examples 1-3 is added into the electronic cigarette liquid, the adding amount is 20-30% of the total weight of the electronic cigarette liquid, the elegant and natural passion fruit fragrance can be given to the electronic cigarette, the fragrance is fresh and elegant, the fragrance quality of the electronic cigarette is improved, and the miscellaneous gas in the tobacco tar is effectively covered.
The above description of the embodiments is only intended to facilitate the understanding of the method of the invention and its core ideas. It should be noted that, for those skilled in the art, it is possible to make various improvements and modifications to the present invention without departing from the principle of the present invention, and those improvements and modifications also fall within the scope of the claims of the present invention.
Claims (9)
1. A preparation method of essence for passion fruit cigarettes is characterized by comprising the following steps:
(1) cleaning the passion fruit, selecting the well-cooked passion fruit, removing peel and shell of the passion fruit to obtain pulp juice containing fruit pits;
(2) adding an extraction solvent into the fruit pulp juice, and standing and soaking for 24-48 h at normal temperature;
(3) carrying out ultrasonic wall breaking on the passion fruit pulp juice soaked in the step (2), filtering and concentrating to obtain a passion fruit extract;
(4) adding the obtained passion fruit extract into a molecular distillation apparatus for distillation, setting the distillation temperature of molecular distillation equipment to be 40-50 ℃, the material flow rate to be 1-2 ml/min, the film scraping rotation speed to be 40-60 r/min, and the vacuum degree to be 20-30 Pa, and keeping distillate flowing out along the wall of a vacuum cavity;
(5) and adding the distillate into a 75% ethanol solution, and uniformly stirring to obtain the passion fruit tobacco essence.
2. The preparation method of the passion fruit tobacco flavor according to claim 1, wherein the extraction solvent in the step (2) is a mixed solvent of 95% ethanol and propylene glycol, and the weight ratio of the extraction solvent to the propylene glycol is 1: 1-3: 1.
3. The preparation method of the passion fruit tobacco flavor according to claim 1, wherein the weight ratio of the extraction solvent to the passion fruit pulp juice in the step (2) is 3: 1-6: 1.
4. The preparation method of the passion fruit tobacco flavor according to claim 1, wherein the ultrasonic power in the step (3) is 500-800W, and the ultrasonic time is 1-2 h.
5. The preparation method of the passion fruit tobacco flavor according to claim 1, wherein the concentration treatment in the step (3) is performed by adopting a rotary evaporator under the conditions that the vacuum degree is 0.090-0.095 Mpa and the temperature is 40-45 ℃.
6. The preparation method of the passion fruit tobacco flavor according to claim 1, wherein the distillation temperature of molecular distillation in the step (4) is 45 ℃, the material flow rate is 2ml/min, the film scraping rotation speed is 50r/min, and the vacuum degree is 25 Pa.
7. The preparation method of the passion fruit tobacco essence according to claim 1, wherein the weight ratio of the distillate obtained in the step (5) to 75% ethanol is 6: 4-7: 3.
8. An essence prepared by the preparation method of the passion fruit cigarette essence of any one of claims 1-7.
9. Use of the passion fruit tobacco flavor of any one of claims 1-8 in cigarettes or electronic cigarettes.
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| CN201911088077.8A CN110819458A (en) | 2019-11-08 | 2019-11-08 | Preparation method and application of passion fruit tobacco essence |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112262938A (en) * | 2020-11-12 | 2021-01-26 | 福建农林大学 | Method for preparing strong-fragrance passion fruit juice |
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| CN109777618A (en) * | 2017-11-11 | 2019-05-21 | 苏洁萌 | A kind of extracting method of cream jasmin france |
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