CN115226876A - Preparation method of composite essence - Google Patents
Preparation method of composite essence Download PDFInfo
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- CN115226876A CN115226876A CN202210546026.0A CN202210546026A CN115226876A CN 115226876 A CN115226876 A CN 115226876A CN 202210546026 A CN202210546026 A CN 202210546026A CN 115226876 A CN115226876 A CN 115226876A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 239000002131 composite material Substances 0.000 title claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 61
- 238000005192 partition Methods 0.000 claims abstract description 46
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 claims abstract description 24
- 238000001035 drying Methods 0.000 claims abstract description 24
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000000341 volatile oil Substances 0.000 claims abstract description 20
- 238000010438 heat treatment Methods 0.000 claims abstract description 17
- 235000001759 Citrus maxima Nutrition 0.000 claims abstract description 16
- 244000276331 Citrus maxima Species 0.000 claims abstract description 16
- 244000242564 Osmanthus fragrans Species 0.000 claims abstract description 14
- 235000019083 Osmanthus fragrans Nutrition 0.000 claims abstract description 14
- 241000722921 Tulipa gesneriana Species 0.000 claims abstract description 14
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 12
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 claims abstract description 12
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 12
- 241000220317 Rosa Species 0.000 claims abstract description 12
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000000484 citronellol Nutrition 0.000 claims abstract description 12
- 229930008394 dihydromyrcenol Natural products 0.000 claims abstract description 12
- XSNQECSCDATQEL-UHFFFAOYSA-N dihydromyrcenol Chemical compound C=CC(C)CCCC(C)(C)O XSNQECSCDATQEL-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229930007744 linalool Natural products 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 9
- 238000002390 rotary evaporation Methods 0.000 claims description 24
- 239000000243 solution Substances 0.000 claims description 24
- 150000001875 compounds Chemical class 0.000 claims description 20
- 239000000706 filtrate Substances 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 18
- 238000001914 filtration Methods 0.000 claims description 16
- 239000012528 membrane Substances 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 108010059820 Polygalacturonase Proteins 0.000 claims description 8
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 108010093305 exopolygalacturonase Proteins 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 8
- 239000000796 flavoring agent Substances 0.000 claims description 8
- 235000019634 flavors Nutrition 0.000 claims description 8
- 238000000227 grinding Methods 0.000 claims description 8
- 239000011148 porous material Substances 0.000 claims description 8
- 239000002904 solvent Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000005520 cutting process Methods 0.000 claims description 4
- 239000012530 fluid Substances 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 238000001471 micro-filtration Methods 0.000 claims description 4
- 239000011259 mixed solution Substances 0.000 claims description 4
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- 241000913959 Rosa spithamea Species 0.000 claims description 3
- 235000011728 ground rose Nutrition 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 19
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- 230000035943 smell Effects 0.000 description 9
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- 238000004519 manufacturing process Methods 0.000 description 4
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Images
Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/12—Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils
- A23L27/13—Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils from citrus fruits
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/20—Synthetic spices, flavouring agents or condiments
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/20—Synthetic spices, flavouring agents or condiments
- A23L27/202—Aliphatic compounds
- A23L27/2024—Aliphatic compounds having oxygen as the only hetero atom
- A23L27/2026—Hydroxy compounds
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Abstract
The invention relates to the technical field of essence, and discloses a preparation method of a composite essence, which comprises the following steps: s1: preparing raw materials: 15-20 parts of shaddock peel essential oil, 11-15 parts of rose petals, 8-12 parts of tulip petals, 7-14 parts of sweet osmanthus flowers, 2-6 parts of citronellol, 1-4 parts of linalool and 2-3 parts of dihydromyrcenol; the drying equipment comprises a box body, wherein a heating wire is arranged on the inner wall of the bottom of the box body, and a connecting shaft is movably connected to the inner wall of one side of the box body. According to the invention, the essence raw materials can be more fully and uniformly baked by matching the partition plate and the moving plate, the baking effect of the device is improved, meanwhile, the auxiliary arc plate can be used for assisting the essence raw materials to be further dispersed, various natural and harmless raw materials can be adopted, various fragrances and various pure and fresh materials are contained, and the fragrances and the purity of the essence are better preserved by respectively adopting different methods to extract the raw materials.
Description
The invention relates to the technical field of essence, in particular to a preparation method of a composite essence.
Background
The essence is widely applied in daily life as an additive, such as industries of food, daily chemicals, tobacco and the like, and meanwhile, along with the improvement of living standard, the quality requirement of people on the essence is gradually improved, firstly, the requirement on the raw materials of the essence is improved, more pure natural and safe raw materials are pursued, secondly, the requirement on the fragrance of the essence is improved, and in order to comply with the market demand, pure natural plants are selected to extract the essence.
The processing procedures of the essence are various, one procedure is to dry the essence raw materials, however, the essence manufacturing raw materials in the current market are various, the components are unsafe, the additives are more, the discomfort of people is easily caused after long-time use, and the requirements of people cannot be met, so that the preparation method of the compound essence is very necessary.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a preparation method of a compound essence, and solves the problems that in the current market, the raw materials for refining the essence are various, the components are unsafe, the additives are more, the discomfort of people is easily caused after long-time use, and the requirements of people cannot be met.
(II) technical scheme
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of a compound essence comprises the following steps:
s1: preparing raw materials: 15-20 parts of shaddock peel essential oil, 11-15 parts of rose petals, 8-12 parts of tulip petals, 7-14 parts of sweet osmanthus flowers, 2-6 parts of citronellol, 1-4 parts of linalool, 2-3 parts of dihydromyrcenol, 3-6 parts of pectinase, 4-8 parts of a composite solvent and 10-16 parts of deionized water;
s2: preparing pericarpium Citri Grandis essential oil, cutting pericarpium Citri Grandis to 2-9mm particle diameter, performing supercritical C02 fluid extraction, and separating to obtain pericarpium Citri Grandis essential oil;
s3: preparing mixed flavor powder, drying rose petals, tulip petals and sweet osmanthus flowers in a drying device, grinding the dried rose petals, tulip petals and sweet osmanthus flowers in a ball mill for 30-50 minutes, screening the ground rose petals, tulip petals and sweet osmanthus flowers to remove impurities, adding a composite solvent and deionized water, stirring, mixing, heating for 30-50 minutes, adding pectinase for enzymolysis, filtering the obtained enzymolysis liquid to obtain filtrate, homogenizing the filtrate, concentrating and drying the filtrate in vacuum for 1-3 hours, and grinding the filtrate to obtain the mixed flavor powder;
s4: stirring and mixing, adding pericarpium Citri Grandis essential oil, citronellol, mixed essence powder, linalool, and dihydromyrcenol into a mixing tank, stirring and premixing at the speed of 95-160r/min for 40-65min;
s5: performing rotary evaporation, performing coarse filtration on the mixed solution at room temperature by using medium-speed filter paper, then putting the filtrate into a rotary evaporation device for rotary evaporation, controlling the temperature to be 45-65 ℃ and the negative pressure to be 0.06-0.09Mpa, and stopping the rotary evaporation when 78-92% of the total volume of the solution is subjected to rotary evaporation;
s6: and (3) performing multiple filtration, namely placing the residual solution after rotary evaporation to room temperature, filtering the solution again by using medium-speed filter paper, then sequentially entering membrane separation equipment twice, performing microfiltration on the solution by using a membrane with the pore size of 10-50 mu m, and passing the obtained solution through an ultrafiltration membrane with the pore size of 15-20nm to obtain the final solution, namely the compound essence.
As a further scheme of the invention, the extraction pressure in the S2 is 20-23MPa, the temperature is 40-49 ℃, and the time is 0.5-1h.
Further, a 200-500 mesh sieve is used for sieving in the S3, the mixing and heating time is 30-50min, and the constant temperature is kept at 40-60 ℃.
On the basis of the scheme, drying equipment includes the box, and the bottom inner wall of box is equipped with the heater strip, one side inner wall swing joint of box has the connecting axle, the outside fixedly connected with baffle of connecting axle, the first fluted disc of box and fixedly connected with is passed to the one end of connecting axle, one side outer wall swing joint of box has the second fluted disc, and the second fluted disc meshes with first fluted disc mutually, one side fixedly connected with pointer of connecting axle, one side outer wall of box is equipped with the identification, and the pointer can contact with the identification, one side outer wall fixedly connected with fixing base of box, the slide has been seted up at the top of fixing base, and swing joint has the toothholder in the slide, and the second fluted disc meshes with the toothholder mutually, the first electric telescopic handle of one side outer wall fixedly connected with of fixing base, and first electric telescopic handle is fixed mutually with the toothholder, the shifting chute has all been seted up to the both sides of baffle, and the shifting chute swing joint has the movable plate, and the movable plate can contact with the box, one side fixedly connected with two springs of movable plate, and the shifting chute is fixed mutually.
Furthermore, a sliding groove is formed in the box body, a baffle is movably connected in the sliding groove, a second electric telescopic rod is fixedly connected to the outer wall of one side of the box body, and the second electric telescopic rod is fixed to the baffle.
On the basis of the scheme, a discharge hole is formed in one side of the box body, the baffle is connected with the discharge hole in a sliding mode, and an inclined hopper is fixedly connected into the discharge hole.
Furthermore, both sides of the connecting shaft are fixedly connected with supporting plates, the supporting plates are fixed with the partition plates, and the upper surfaces of the partition plates are fixedly connected with a plurality of auxiliary arc plates.
On the basis of the scheme, the outer wall of the bottom of the box body is fixedly connected with a plurality of supporting columns, and the supporting columns are symmetrically distributed.
(III) advantageous effects
Compared with the prior art, the invention provides a preparation method of the compound essence, which has the following beneficial effects:
1. according to the invention, through the arrangement of the movable plate arranged on the partition plate, the first electric telescopic rod extends to enable the tooth holder to drive the second gear disc to rotate, so that the first gear disc drives the connecting shaft to rotate, the partition plate swings left and right, when the partition plate rotates to a proper angle, a gap is generated between the partition plate and the box body, and at the moment, the spring rebounds and extends, so that the movable plate moves to a proper position along the moving groove to be contacted with the box body, and meanwhile, the partition plate swings to enable essence raw materials to be dispersed and turned over, so that the essence raw materials are more fully and uniformly baked, the phenomenon that the essence raw materials are not uniformly baked due to the fact that a common drying device in the market usually adopts a single heating wire to bake is avoided, and the baking effect of the device is improved.
2. According to the invention, the auxiliary arc plate is arranged on the partition plate, so that when the essence raw materials move on the partition plate, the auxiliary arc plate can assist the essence raw materials to be further dispersed, the essence raw materials are more efficiently baked, and the using effect of the device is improved.
3. According to the invention, the baffle is arranged in the box body, the second electric telescopic rod extends to enable the baffle to move upwards along the sliding groove and leave the discharge hole, and at the moment, raw materials on the baffle flow out of the discharge hole through the moving plate, so that the device can automatically discharge materials, and the discharging effect of the device is improved.
4. The composite essence provided by the invention adopts various natural and harmless raw materials, contains various fragrances, is fresh and pure, and extracts the raw materials by different methods respectively, so that the fragrance and the purity of the essence are better preserved, and the fragrance is pleasant and lasting.
5. The citronellol disclosed by the invention not only has good flower fragrance, but also has good antibacterial and insect-repelling effects, and can play roles in improving the lung ventilation function and reducing the airway resistance, so that the overall application effect of the essence is greatly improved, the shaddock peel essential oil can remove peculiar smell, can exert good and stable deodorization effect, can refresh the brain, inhibit bacteria and sterilize, and the production raw materials are low in cost, so that the overall application effect of the essence can be improved.
6. The linalool and the dihydromyrcenol have the fragrance of the Convallaria majalis, can mutually play a good role in compounding and synergism, show strong capability of covering bad smell, and can be combined with substances with smells in the air, thereby playing a good deodorizing effect.
Drawings
Fig. 1 is a schematic view of a three-dimensional structure of a drying device of a preparation method of a compound essence provided by the invention;
fig. 2 is a schematic sectional structure view of a drying device of the preparation method of the compound essence provided by the invention;
fig. 3 is a schematic diagram of a partially enlarged structure of a drying device of the preparation method of the compound essence provided by the invention;
fig. 4 is a schematic flow structure diagram of a preparation method of the compound essence provided by the invention.
In the figure: 1. a partition plate; 2. a pointer; 3. a first fluted disc; 4. a connecting shaft; 5. a second fluted disc; 6. a tooth holder; 7. a fixed seat; 8. a first electric telescopic rod; 9. a support pillar; 10. a box body; 11. an inclined hopper; 12. A second electric telescopic rod; 13. a baffle plate; 14. a discharge port; 15. heating wires; 16. a support plate; 17. a spring; 18. an auxiliary arc plate; 19. and (5) moving the plate.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
Example 1
Referring to fig. 1-4, a preparation method of a compound essence comprises the following steps:
s1: preparing raw materials: 16 parts of shaddock peel essential oil, 12 parts of rose petals, 9 parts of tulip petals, 9 parts of sweet osmanthus flowers, 4 parts of citronellol, 2 parts of linalool, 2 parts of dihydromyrcenol, 4 parts of pectinase, 5 parts of a composite solvent and 12 parts of deionized water, wherein the citronellol not only has good flowery fragrance, but also has good antibacterial and insect-repellent effects, and can also improve the lung ventilation function and reduce the airway resistance, so that the overall application effect of the essence is greatly improved;
s2: preparing the shaddock peel essential oil, cutting shaddock peel into 4mm particle sizes, performing supercritical C02 fluid extraction, and separating to obtain the shaddock peel essential oil, wherein the shaddock peel essential oil can remove peculiar smell, can exert good and stable deodorization effect, can refresh brain, inhibit bacteria and disinfect, has low production raw material cost, and further can improve the overall application effect of the essence;
s3: preparing mixed flavor powder, drying rose petals, tulip petals and sweet osmanthus flowers in a drying device, grinding the dried rose petals, tulip petals and sweet osmanthus flowers in a ball mill for 32 minutes, screening the ground rose petals, removing impurities, adding a composite solvent and deionized water, stirring, mixing, heating for 35 minutes, adding pectinase for enzymolysis, filtering the obtained enzymolysis liquid to obtain filtrate, homogenizing the filtrate, concentrating and drying the filtrate in vacuum for 1.8 hours, and grinding the filtrate to obtain the mixed flavor powder;
s4: stirring and mixing, namely adding the shaddock peel essential oil, the citronellol, the mixed essence powder, the linalool and the dihydromyrcenol into a mixing tank for stirring and premixing, wherein the speed is 120r/min, the mixing time is 45min, the linalool and the dihydromyrcenol have the fragrance of convallaria majalis, can mutually play a good role in compounding and synergism, and show strong capability of covering bad smell, and can be combined with substances with smell in the air, so that a good deodorization effect is achieved;
s5: performing rotary evaporation, performing rough filtration on the mixed solution at room temperature by adopting medium-speed filter paper, then putting the filtrate into a rotary evaporation device for rotary evaporation, controlling the temperature to be 50 ℃ and the negative pressure to be 0.07Mpa, and stopping the rotary evaporation when 82% of the total volume of the solution is subjected to rotary evaporation;
s6: and (2) performing multiple filtration, namely placing the residual solution after rotary evaporation to room temperature, filtering the solution again by using medium-speed filter paper, then sequentially entering membrane separation equipment twice, performing microfiltration on the solution by using a membrane with the pore size of 20 mu m, and passing the obtained solution through an ultrafiltration membrane with the pore size of 16nm to obtain the final solution, namely the composite essence.
In the invention, the extraction pressure in S2 is 21MPa, the temperature is 43 ℃, the time is 0.6h, a 220-mesh sieve is used for sieving in S3, the mixing and heating time is 35min, and the constant temperature is kept at 44 ℃.
It should be particularly noted that the drying device includes a box 10, a heating wire 15 is disposed on an inner wall of a bottom of the box 10, the heating wire 15 can generate heat, thereby baking the raw material, a connecting shaft 4 is rotatably connected to an inner wall of one side of the box 10, a partition plate 1 is fixed to an outer side of the connecting shaft 4 through a bolt, one end of the connecting shaft 4 penetrates through the box 10 and is connected to a first fluted disc 3 in a key manner, a second fluted disc 5 is rotatably connected to an outer wall of one side of the box 10, and the second fluted disc 5 is meshed with the first fluted disc 3, a pointer 2 is fixed to one side of the connecting shaft 4 through a bolt, an indication mark is disposed on an outer wall of one side of the box 10, a fixing seat 7 is fixed to an outer wall of one side of the box 10 through a bolt, a slide is disposed at a top of the fixing seat 7, a toothholder 6 is slidably connected to the slide, and the second fluted disc 5 is meshed with the toothholder 6, the outer wall of one side of the fixed seat 7 is fixed with a first electric telescopic rod 8 through bolts, the first electric telescopic rod 8 is fixed with a tooth holder 6, two sides of the partition board 1 are respectively provided with a moving groove, a moving board 19 is connected in the moving groove in a sliding way, the moving board 19 can be contacted with the box body 10, one side of the moving board 19 is welded with two springs 17, the springs 17 are fixed with the moving grooves, the first electric telescopic rod 8 extends to enable the tooth holder 6 to drive the second gear disc 5 to rotate, so that the first gear disc 3 drives the connecting shaft 4 to rotate, further the partition board 1 swings left and right, when the partition board 1 rotates to a proper angle, a gap is generated between the partition board 1 and the box body 10, at the moment, the springs 17 rebound and extend, so that the moving board 19 moves to a proper position along the moving groove to be contacted with the box body 10, and meanwhile, the partition board 1 swings to enable essence raw materials to be dispersed and overturned, so that the essence raw materials are baked more fully and uniformly, avoid drying equipment commonly used in the existing market to adopt single heater strip 15 to toast usually and lead to essence raw materials stoving inhomogeneous.
It needs to be particularly noted that, a chute is provided in the box 10, a baffle 13 is slidably connected in the chute, a second electric telescopic rod 12 is fixed on an outer wall of one side of the box 10 through a bolt, the second electric telescopic rod 12 is fixed with the baffle 13, a discharge port 14 is provided on one side of the box 10, the baffle 13 is slidably connected with the discharge port 14, the baffle 13 moves upwards along the chute when the second electric telescopic rod 12 extends, and the baffle is separated from the discharge port 14, at this time, the raw material on the partition plate 1 flows out of the discharge port 14 through a movable plate 19, so that the device can automatically discharge material, a tilted hopper 11 is fixed in the discharge port 14 through a bolt, the tilted hopper 11 can guide the roasted essence raw material, support plates 16 are fixed on two sides of the connecting shaft 4 through bolts, the support plates 16 are fixed with the partition plate 1, a plurality of auxiliary arc plates 18 are fixed on the upper surface of the partition plate 1 through bolts, when the essence raw material moves on the partition plate 1, the auxiliary arc plates 18 can assist the essence raw material to further disperse, so that the essence raw material is roasted more efficiently, the essence raw material is roasted material, a plurality of the outer wall of the box 10 is fixed with a plurality of support columns 9 symmetrically distributed through bolts.
The working principle is as follows: when essence raw materials need to be baked, first electric telescopic rod 8 is started, first electric telescopic rod 8 extends to enable tooth holder 6 to drive second tooth disc 5 to rotate, so that first tooth disc 3 drives connecting shaft 4 to rotate, and partition plate 1 swings left and right, when partition plate 1 rotates to a proper angle, a gap is formed between partition plate 1 and box 10, spring 17 rebounds and extends, so that moving plate 19 moves to a proper position along a moving groove to be in contact with box 10, meanwhile, partition plate 1 swings to enable the essence raw materials to be dispersed and turned over, heating wire 15 bakes the essence raw materials on partition plate 1, so that the essence raw materials are baked more fully and uniformly, and when the essence raw materials move on partition plate 1, auxiliary arc plate 18 further disperses the auxiliary essence raw materials, so that the essence raw materials are baked more efficiently, after baking is finished, when pointer 2 rotates to a proper position to be in contact with an indicating mark, moving plate 19 moves to one side of discharge hole 14, second electric telescopic rod 12 is started, baffle 13 extends to enable baffle plate 13 to move upwards along the sliding groove, and leaves discharge hole 14, at the baffle plate 1 flows out of raw materials, and then, and discharging materials flow out of the automatic discharging device 14.
Example 2
Referring to fig. 1-4, a preparation method of a compound essence comprises the following steps:
s1: preparing raw materials: the essence comprises 18 parts of shaddock peel essential oil, 14 parts of rose petals, 11 parts of tulip petals, 13 parts of sweet osmanthus flowers, 4 parts of citronellol, 3 parts of linalool, 3 parts of dihydromyrcenol, 5 parts of pectinase, 7 parts of a composite solvent and 15 parts of deionized water, wherein the citronellol not only has good flower fragrance, but also has good antibacterial and insect-repellent effects, and can also play a role in improving the lung ventilation function and reducing the airway resistance, so that the overall application effect of the essence is greatly improved;
s2: preparing the shaddock peel essential oil, cutting the shaddock peel into pieces with the particle size of 8mm, performing supercritical C02 fluid extraction, and separating to obtain the shaddock peel essential oil, wherein the shaddock peel essential oil can remove peculiar smell, can exert good and stable deodorization effect, can refresh brain, inhibit bacteria and sterilize, is low in production raw material cost, and further can improve the overall application effect of the essence;
s3: preparing mixed flavor powder, drying rose petals, tulip petals and sweet osmanthus flowers in a drying device, grinding in a ball mill for 45 minutes after drying, screening to remove impurities, adding a composite solvent and deionized water, stirring, mixing, heating for 46 minutes, adding pectinase for enzymolysis, filtering the obtained enzymatic hydrolysate to obtain filtrate, homogenizing the filtrate, concentrating and drying in vacuum for 2.6 hours, and grinding to obtain the mixed flavor powder;
s4: stirring and mixing, namely adding the shaddock peel essential oil, the citronellol, the mixed essence powder, the linalool and the dihydromyrcenol into a mixing tank for stirring and premixing, wherein the speed is 150r/min, the mixing time is 60min, the linalool and the dihydromyrcenol have the fragrance of convallaria majalis, can mutually play a good role in compounding and synergism, and show strong capability of covering bad smell, and can be combined with substances with smell in the air, so that a good deodorization effect is achieved;
s5: performing rotary evaporation, namely performing rough filtration on the mixed solution at room temperature by adopting medium-speed filter paper, then putting the filtrate into a rotary evaporation device for rotary evaporation, controlling the temperature to be 60 ℃ and the negative pressure to be 0.08Mpa, and stopping the rotary evaporation when 89 percent of the total volume of the solution is subjected to rotary evaporation;
s6: and (2) performing multiple filtration, namely placing the residual solution after rotary evaporation to room temperature, filtering the solution again by using medium-speed filter paper, then sequentially entering membrane separation equipment twice, performing microfiltration on the solution by using a membrane with the pore size of 40 mu m, passing the obtained solution through an ultrafiltration membrane with the pore size of 18nm, and finally obtaining the solution, namely the composite essence.
In the invention, the extraction pressure in S2 is 23MPa, the temperature is 47 ℃, the time is 0.9h, a 460-mesh sieve is used for sieving in S3, the mixing and heating time is 47min, and the constant temperature is kept at 58 ℃.
It should be particularly noted that the drying device includes a box 10, a heating wire 15 is disposed on an inner wall of a bottom of the box 10, the heating wire 15 can generate heat, thereby baking the raw material, a connecting shaft 4 is rotatably connected to an inner wall of one side of the box 10, a partition plate 1 is fixed to an outer side of the connecting shaft 4 through a bolt, one end of the connecting shaft 4 penetrates through the box 10 and is connected to a first fluted disc 3 in a key manner, a second fluted disc 5 is rotatably connected to an outer wall of one side of the box 10, and the second fluted disc 5 is meshed with the first fluted disc 3, a pointer 2 is fixed to one side of the connecting shaft 4 through a bolt, an indication mark is disposed on an outer wall of one side of the box 10, a fixing seat 7 is fixed to an outer wall of one side of the box 10 through a bolt, a slide is disposed at a top of the fixing seat 7, a toothholder 6 is slidably connected to the slide, and the second fluted disc 5 is meshed with the toothholder 6, a first electric telescopic rod 8 is fixed on the outer wall of one side of the fixed seat 7 through bolts, the first electric telescopic rod 8 is fixed with a tooth holder 6, moving grooves are formed in two sides of the partition plate 1, a moving plate 19 is connected in the moving grooves in a sliding mode, the moving plate 19 can be in contact with the box body 10, two springs 17 are welded on one side of the moving plate 19, the springs 17 are fixed with the moving grooves, the tooth holder 6 drives the second gear plate 5 to rotate through extension of the first electric telescopic rod 8, the first gear plate 3 drives the connecting shaft 4 to rotate, the partition plate 1 can swing left and right, when the partition plate 1 rotates to a proper angle, a gap is formed between the partition plate 1 and the box body 10, the springs 17 rebound and extend, the moving plate 19 moves to a proper position along the moving grooves to be in contact with the box body 10, meanwhile, the partition plate 1 swings to enable essence raw materials to be dispersed and turned over, and more sufficiently and uniformly baked, avoid drying equipment commonly used in the existing market to adopt single heater strip 15 to toast usually and lead to essence raw materials stoving inhomogeneous.
It needs to be particularly noted that, a chute is provided in the box 10, a baffle 13 is slidably connected in the chute, a second electric telescopic rod 12 is fixed on an outer wall of one side of the box 10 through a bolt, the second electric telescopic rod 12 is fixed with the baffle 13, a discharge port 14 is provided on one side of the box 10, the baffle 13 is slidably connected with the discharge port 14, the baffle 13 moves upwards along the chute when the second electric telescopic rod 12 extends, and the baffle is separated from the discharge port 14, at this time, the raw material on the partition plate 1 flows out of the discharge port 14 through a movable plate 19, so that the device can automatically discharge material, a tilted hopper 11 is fixed in the discharge port 14 through a bolt, the tilted hopper 11 can guide the roasted essence raw material, support plates 16 are fixed on two sides of the connecting shaft 4 through bolts, the support plates 16 are fixed with the partition plate 1, a plurality of auxiliary arc plates 18 are fixed on the upper surface of the partition plate 1 through bolts, when the essence raw material moves on the partition plate 1, the auxiliary arc plates 18 can assist the essence raw material to further disperse, so that the essence raw material is roasted more efficiently, the essence raw material is roasted material, a plurality of the outer wall of the box 10 is fixed with a plurality of support columns 9 symmetrically distributed through bolts.
The working principle is as follows: when essence raw materials need to be baked, first electric telescopic handle 8 is started at first, first electric telescopic handle 8 extends to enable toothholder 6 to drive second fluted disc 5 to rotate, thereby enabling first fluted disc 3 to drive connecting shaft 4 to rotate, and further enabling partition plate 1 to swing left and right, when partition plate 1 rotates to a proper angle, a gap is generated between partition plate 1 and box 10, spring 17 rebounds and extends at the moment, thereby enabling movable plate 19 to move to a proper position along a moving groove to be in contact with box 10, meanwhile, partition plate 1 swings to enable essence raw materials to be dispersed and overturned, heater strip 15 bakes the essence raw materials on partition plate 1, thereby enabling the essence raw materials to be baked more fully and uniformly, and when the essence raw materials move on partition plate 1, auxiliary arc plate 18 assists essence raw materials to be further dispersed, so that the essence raw materials are baked more efficiently, after baking is finished, when pointer 2 rotates to a proper position to be in contact with an indication mark, at the moment, 19 moves to one side of discharge hole 14, second electric telescopic handle 12 is started, baffle 13 extends to enable baffle plate 13 to move upwards along sliding groove 14, and when pointer 1 moves out of raw materials, at the discharge hole 14, at the moment, and discharging materials flows out through automatic discharging device.
In the description herein, it is noted that relational terms such as first and second, and the like, are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. The preparation method of the compound essence is characterized by comprising the following steps:
s1: preparing raw materials: 15-20 parts of shaddock peel essential oil, 11-15 parts of rose petals, 8-12 parts of tulip petals, 7-14 parts of sweet osmanthus flowers, 2-6 parts of citronellol, 1-4 parts of linalool, 2-3 parts of dihydromyrcenol, 3-6 parts of pectinase, 4-8 parts of a composite solvent and 10-16 parts of deionized water;
s2: preparing pericarpium Citri Grandis essential oil, cutting pericarpium Citri Grandis to 2-9mm particle diameter, performing supercritical C02 fluid extraction, and separating to obtain pericarpium Citri Grandis essential oil;
s3: preparing mixed flavor powder, drying rose petals, tulip petals and sweet osmanthus flowers in a drying device, grinding the dried rose petals, tulip petals and sweet osmanthus flowers in a ball mill for 30-50 minutes, screening the ground rose petals, tulip petals and sweet osmanthus flowers to remove impurities, adding a composite solvent and deionized water, stirring, mixing, heating for 30-50 minutes, adding pectinase for enzymolysis, filtering the obtained enzymolysis liquid to obtain filtrate, homogenizing the filtrate, concentrating and drying the filtrate in vacuum for 1-3 hours, and grinding the filtrate to obtain the mixed flavor powder;
s4: stirring and mixing, adding pericarpium Citri Grandis essential oil, citronellol, mixed essence powder, linalool, and dihydromyrcenol into a mixing tank, stirring and premixing at the speed of 95-160r/min for 40-65min;
s5: performing rotary evaporation, performing coarse filtration on the mixed solution at room temperature by using medium-speed filter paper, then putting the filtrate into a rotary evaporation device for rotary evaporation, controlling the temperature to be 45-65 ℃ and the negative pressure to be 0.06-0.09Mpa, and stopping the rotary evaporation when 78-92% of the total volume of the solution is subjected to rotary evaporation;
s6: and (3) performing multiple filtration, namely standing the residual solution after the rotary evaporation to room temperature, filtering the solution by using medium-speed filter paper again, then sequentially entering membrane separation equipment twice, performing microfiltration on the solution by using a membrane with the pore size of 10-50 mu m, and passing the obtained solution through an ultrafiltration membrane with the pore size of 15-20nm to obtain the compound essence.
2. The preparation method of the compound essence according to claim 1, wherein the extraction pressure in the S2 is 20-23MPa, the temperature is 40-49 ℃, and the time is 0.5-1h.
3. The method for preparing the compound essence according to claim 1, wherein a 200-500 mesh sieve is used for sieving in S3, the mixing and heating time is 30-50min, and the constant temperature is kept at 40-60 ℃.
4. The preparation method of the compound essence according to claim 1, wherein the drying equipment comprises a box body (10), a heating wire (15) is arranged on the inner wall of the bottom of the box body (10), a connecting shaft (4) is movably connected to the inner wall of one side of the box body (10), a partition plate (1) is fixedly connected to the outer side of the connecting shaft (4), one end of the connecting shaft (4) penetrates through the box body (10) and is fixedly connected with a first fluted disc (3), a second fluted disc (5) is movably connected to the outer wall of one side of the box body (10), the second fluted disc (5) is meshed with the first fluted disc (3), a pointer (2) is fixedly connected to one side of the connecting shaft (4), an indicating mark is arranged on the outer wall of one side of the box body (10), the pointer (2) can be contacted with the indicating mark, a fixing seat (7) is fixedly connected to the outer wall of one side of the box body (10), the top of the fixing seat (7) is provided with a sliding way, a tooth seat (6) is movably connected to the sliding way, the second fluted disc (5) is meshed with the tooth seat (6), a first electric telescopic rod (8) is fixedly connected to the sliding way, and a movable plate (19) is arranged on two sides of the sliding way, and the moving plate (19) can be contacted with the box body (10), one side of the moving plate (19) is fixedly connected with two springs (17), and the springs (17) are fixed with the moving groove.
5. A preparation method of a compound essence according to claim 4, characterized in that a chute is opened in the box body (10), a baffle (13) is movably connected in the chute, a second electric telescopic rod (12) is fixedly connected to the outer wall of one side of the box body (10), and the second electric telescopic rod (12) is fixed with the baffle (13).
6. A preparation method of a compound essence according to claim 5, wherein a discharge port (14) is opened at one side of the box body (10), the baffle (13) is connected with the discharge port (14) in a sliding manner, and an inclined hopper (11) is fixedly connected in the discharge port (14).
7. The preparation method of the compound type essence according to claim 6, wherein the two sides of the connecting shaft (4) are fixedly connected with supporting plates (16), the supporting plates (16) are fixed with the partition board (1), and the upper surface of the partition board (1) is fixedly connected with a plurality of auxiliary arc plates (18).
8. A preparation method of a compound essence according to claim 7, characterized in that the outer wall of the bottom of the box body (10) is fixedly connected with a plurality of support columns (9), and the support columns (9) are symmetrically distributed.
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| CN104531354A (en) * | 2014-12-25 | 2015-04-22 | 鹰潭华宝香精香料有限公司 | Fig type compound essence and extraction method thereof |
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