CN101954107A - Solid aromatic sleep aid and preparation method thereof - Google Patents
Solid aromatic sleep aid and preparation method thereof Download PDFInfo
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- CN101954107A CN101954107A CN201010501519XA CN201010501519A CN101954107A CN 101954107 A CN101954107 A CN 101954107A CN 201010501519X A CN201010501519X A CN 201010501519XA CN 201010501519 A CN201010501519 A CN 201010501519A CN 101954107 A CN101954107 A CN 101954107A
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Abstract
The invention discloses a solid aromatic sleep aid and a preparation method thereof. The solid aromatic sleep aid comprises the following components in percentage by mass: 0.75-1.50% of sleep aid perfume, 0.50-1.50% of solid air-refreshing gel, 8.00-10.00% of high-efficiency solubilizer, 0.40-0.60% of preservative and the balance distilled water. The preparation method comprises the following four steps: the blending of the sleep aid perfume, the solubilization of the sleep aid perfume, the preparation of the gel, the mixing of the sleep aid perfume and the gel and the like. By using cananga oil and other sleep aid essential oil as main materials, the solid aromatic sleep aid is a pure natural, non-poisonous, harmless safety product. The solid aromatic sleep aid contains rose oil and other components, so that fresh and mild flower/grass fragrance can be sent out, thereby achieving the effects of purifying air, relieving fatigue and the like and being especially suitable for people suffering from poor sleep quality for a long time. Besides, the solid aromatic sleep aid can continuously release pleasant fragrance for 5-10 days and cause no pollution to the environment.
Description
Technical field
The invention belongs to technical field of chemistry, be specifically related to a kind of preparation method of blending technology and solid aromatic sleep aid thereof of solid aromatic sleeping essence.
Background technology
Good sleep is the healthy assurances of people, and along with the development of society, the consciousness of health of people and self-protection is also in continuous increase, and the product that various help people improve sleep quality arises at the historic moment in succession.
At present, the product of sleeping class is a lot of on the domestic market, mainly is to be prepared into medicine (sleeping pill, Anshen Wan etc.), health product etc.The batching majority is to contain synthetic organic chemistry composition (as: Zolpidemtar Trate, alprazolam etc.) in these sleeping products, and people reach the sleeping effect by taking in the body.But can in human body, have side effects.
And solid aromatic sleep aid of the present invention forms by several quintessence oils are composite, can reach better sleeping effect.Wherein effectively the sleeping composition has Cananga odorata oil, eucalyptus quintessence oil, lavandula angustifolia wet goods, people by abnormal smells from the patient better reach releive loosen, the effect of calming soporific.This product belongs to a kind of nontoxic, safety product of pure natural.Show the domestic like product that also do not have.
Summary of the invention
One of purpose of the present invention is to provide a kind of solid aromatic sleep aid in order to address the above problem.
Two of purpose of the present invention provides a kind of preparation method of solid aromatic sleep aid.
Three of purpose of the present invention provides sleeping essence used in a kind of preparation method of solid aromatic sleep aid.
Technical scheme of the present invention
A kind of solid aromatic sleep aid, the mass percent of its contained each composition is composed as follows:
Sleeping essence 0.75～1.50%
Solid air freshening glue 0.50～1.50%
Efficient solubilizing agents 8.00～10.00%
Antiseptic 0.40～0.60%
Surplus is a distilled water;
Efficient solubilizing agents wherein is based on nonionic, amphoteric ionic surfactant, mainly is the organic compound of alcohol, ether structure: polyoxypropylene fatty alcohol ether, polyoxyethylene aliphatic alcohol ether (12-13 alkanol polyxyethylated alcohol) etc.; Be preferably 12-13 alkanol polyxyethylated alcohol;
Solid air freshening glue wherein is macromolecular materials such as polyvinyl alcohol, hydroxypropyl emthylcellulose or modified cellulose; Be preferably modified cellulose;
Antiseptic wherein is a DMDMH(dihydroxymethyl dimethyl hydantoin) and IPBC(3-iodo-2-propynyl butyl carbamate) mixture; Be preferably that model is the product of G.P.L in the Chinese daily use chemicals industry;
Wherein said sleeping essence comprises components such as Cananga odorata oil, eucalyptus quintessence oil, jasmin quintessence oil, Anthemis nobilis quintessence oil, coriander seed oil, Radix Et Rhizoma Nardostachyos quintessence oil, Oleum lavandula angustifolia, rose oil, Oleum Caryophylli, Herba Pogostemonis oil, sage oil, cade oil, antioxidant;
And the mass percent of each component described in the sleeping essence sees Table 1:
The quality percentage composition of each component in the used sleeping essence of table 1
| Sequence number | The raw material name | Quality percentage composition (%) |
| 1 | Cananga odorata oil | 25.00～35.00 |
| 2 | Eucalyptus quintessence oil | 8.00～15.00 |
| 3 | Jasmin quintessence oil | 1.00～5.00 |
| 4 | The Anthemis nobilis quintessence oil | 0.50～5.00 |
| 5 | Coriander seed oil | 1.00～7.00? |
| 6 | The Radix Et Rhizoma Nardostachyos quintessence oil | 1.00～7.00? |
| 7 | Oleum lavandula angustifolia | 25.00～35.00 |
| 8 | Rose oil | 0.50～5.00? |
| 9 | Oleum Caryophylli | 1.00～5.00? |
| 10 | Herba Pogostemonis oil | 1.00～5.00? |
| 11 | Sage oil | 3.00～10.00? |
| 12 | Cade oil | 3.00～10.00? |
| 13 | Antioxidant | 1.00～2.00? |
| Solvent | Dipropylene glycol | Surplus |
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
The mass percent of each component described in the sleeping essence preferably sees Table 2:
The quality percentage composition of each component in the used sleeping essence of table 2
| Sequence number | The raw material name | Quality percentage composition (%) |
| 1 | Cananga odorata oil | 25.00～32.00 |
| 2 | Eucalyptus quintessence oil | 8.00～10.00 |
| 3 | Jasmin quintessence oil | 3.00～4.00 |
| 4 | The Anthemis nobilis quintessence oil | 1.00 |
| 5 | Coriander seed oil | 2.00 |
| 6 | The Radix Et Rhizoma Nardostachyos quintessence oil | 4.00～5.00 |
| 7 | Oleum lavandula angustifolia | 32.00～35.00 |
| 8 | Rose oil | 1.00 |
| 9 | Oleum Caryophylli | 2.00～3.00 |
| 10 | Herba Pogostemonis oil | 1.00～4.00 |
| 11 | Sage oil | 4.00～6.00 |
| 12 | Cade oil | 4.00～6.00 |
| 13 | Antioxidant | 1.00 |
| Solvent | Dipropylene glycol | Surplus |
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
A kind of preparation method of solid aromatic sleep aid comprises being prepared as follows step:
(1), the allotment of sleeping essence
Each component in the sleeping essence is added in the anticorrosion container (1) successively by sequence number, be stirred to 15 minutes and promptly reach even later on;
(2), the solubilising of sleeping essence
The sleeping essence that step (1) is deployed carries out solubilising:
At first in anticorrosion container (2), add account for solid aromatic sleep aid product gross mass (hereinafter to be referred as: product population) be 8.00～10.00% efficient solubilizing agents, be heated to 55～60 ℃, after 15 minutes, to clear;
To account for product population be 0.75～1.50% the deployed sleeping essence of step (1) to wherein adding then, after stirring 5～10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets solubilising sleeping essence;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 86.40～90.50% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 10.00～15.00% distilled water, heat, progressively being sprinkled into while stirring and accounting for product population is 0.50～1.50% solid air freshening glue, and heated and stirred to 85～90 ℃, after 20～30 minutes, after making powder dissolution, stop heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sleeping essence and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.40%～0.60% the antiseptic, when naturally cooling to 40～50 ℃, slowly in the gel colloid, pour the solubilising sleeping essence of step (2) gained into, after continuing stirred for several minute, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly and be combined into the solid aromatic sleep aid;
It is poured in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic sleep aid product of the present invention.
Key character of the present invention is the blending technology of sleeping essence in the solid aromatic sleep aid.
Beneficial effect of the present invention
The present invention is the primary raw material of sleeping perfume ingredient with Cananga odorata oil, eucalyptus quintessence oil, Oleum lavandula angustifolia, and the solid aromatic sleep aid product of gained belongs to a kind of pure natural, nontoxic, safety product.Make solid aromatic sleep aid of the present invention give out the fragrant fragrance of pure and fresh soft flowers and plants owing to also contain one-tenth branches such as rose oil, Anthemis nobilis quintessence oil, jasminun sambae aif in the solid aromatic sleep aid again, not only can purify air, and the effect of driving away tired, anti-melancholy, peace show tender affection for emotion arranged, when bringing the fragrant fragrance of a flower gas of pure and fresh, silk silk to air, can also alleviate operating pressure, bring joyful and light, stable to mood.
Solid aromatic sleep aid of the present invention is compared with other type products on the market, safety, to human body have no side effect, easy to carry, and be not subject to influences such as temperature, humidity, the crowd who especially is fit to be in for a long time poor sleeping quality uses.Under conventional environment, can continue to discharge 5～10 days pleasant fragrance, the people there is not any injury, and abnormal smells from the patient fragrance nature, also pollution-free to environment.
The specific embodiment
Below by embodiment, the present invention is further described, but do not limit the present invention.
The model of now using Shanghai Fine Chemical Co., Ltd of Supreme Being section to produce to provide as the product of Cosmacd N II-9 as the efficient solubilizing agents in the solid aromatic sleep aid;
Now use Shanghai tie up U.S. biotechnology Development Co., Ltd produce the model that provides as the product of LA01 as the solid air freshening glue in the solid aromatic sleep aid;
The model of now using Shanghai Fine Chemical Co., Ltd of Supreme Being section to produce to provide as the product of G.P.L as the antiseptic in the solid aromatic sleep aid;
The product B HT(2.6-ditertbutylparacresol that now uses Shanghai traditional Chinese medicines group company to produce to provide) as the antioxidant of solid aromatic sleep aid.
Embodiment 1
A kind of solid aromatic sleep aid, the mass percent of its contained each composition is composed as follows:
Sleeping essence A 0.75%
Solid air freshening glue 0.50%
Efficient solubilizing agents 8.00%
Antiseptic 0.40%
Surplus is a distilled water 90.35%
The preparation method of above-mentioned a kind of solid aromatic sleep aid comprises being prepared as follows step:
(1), the allotment of sleeping essence A
The mass percent of each raw material sees Table 3 in the sleeping essence A example:
The quality percentage composition of each component in the used sleeping essence of the table 3 A example
| Sequence number | The raw material name | Quality percentage composition (%) A |
| 1 | Cananga odorata oil | 32.00 |
| 2 | Eucalyptus quintessence oil | 8.00 |
| 3 | Jasmin quintessence oil | 3.00 |
| 4 | The Anthemis nobilis quintessence oil | 1.00 |
| 5 | The coriander quintessence oil | 2?.00 |
| 6 | The Radix Et Rhizoma Nardostachyos quintessence oil | 4?.00 |
| 7 | Oleum lavandula angustifolia | 32.00 |
| 8 | Rose oil | 1?.00 |
| 9 | Oleum Caryophylli | 3?.00 |
| 10 | Herba Pogostemonis oil | 1?.00 |
| 11 | Sage oil | 6?.00 |
| 12 | Cade oil | 6?.00 |
| 13 | Antioxidant | 1?.00 |
| Solvent | Dipropylene glycol | 0.00 |
According to the quality percentage composition of each component in the table 3, each component is added in the anticorrosion container (1) successively by sequence number in the table 3, be stirred to 15 minutes and promptly reach even later on;
(2), the solubilising of sleeping essence A
The sleeping essence A that step (1) is deployed carries out solubilising: add in anticorrosion container (2) at first that to account for product population be 8.00% efficient solubilizing agents, be heated to 55 ℃～60 ℃, after 15 minutes, to clear; To account for product population be 0.75% the deployed sleeping essence A of step (1) to wherein adding then, after stirring 10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets solubilising sleeping essence A;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 90.35% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 15.00% distilled water, heats, and progressively being sprinkled into while stirring and accounting for product population is 0.50% solid air freshening glue, and heated and stirred to 85～90 ℃, after 30 minutes, make powder dissolution after, stop the heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sleeping essence A and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.40% the antiseptic, when naturally cooling to 40～50 ℃, slowly in the gel colloid, pour the solubilising sleeping essence A of step (2) gained into, continue to stir, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly and be combined into the solid aromatic sleep aid.It is poured in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic sleep aid product of the present invention.
The solid aromatic sleep aid of above-mentioned gained has obvious fragrant cananga fragrance of a flower fragrance, but the turbid fragrance of the fragrance of a flower is heavier, fragrance the nature, fragrance is too single, fragrance inadequately the circle and, abundant, do not send out thoroughly, outward appearance is transparent gel-form.After a period of time, fragrance weakens gradually, loses fragrance, and the colloid evaporation rate is fast.Can continue to discharge 4～6 days fragrance, the sleeping effect is more not obvious.
Embodiment 2
A kind of solid aromatic sleep aid, the mass percent of its contained each composition is composed as follows:
Sleeping essence B 1.50%
Solid air freshening glue 1.50%
Efficient solubilizing agents 10.00%
Antiseptic 0.60%
Surplus is a distilled water.
The preparation method of above-mentioned a kind of solid aromatic sleep aid comprises being prepared as follows step:
(1), the allotment of sleeping essence B
The mass percent of each raw material sees Table 4 in the sleeping essence B example:
The quality percentage composition of each component in the used sleeping essence of the table 4 B example
| Sequence number | The raw material name | Quality percentage composition (%) B |
| 1 | Cananga odorata oil | 30.00 |
| 2 | Eucalyptus quintessence oil | 10.00 |
| 3 | Jasmin quintessence oil | 4.00 |
| 4 | The Anthemis nobilis quintessence oil | 1.00 |
| 5 | The coriander quintessence oil | 2.00 |
| 6 | The Radix Et Rhizoma Nardostachyos quintessence oil | 4?.00 |
| 7 | Oleum lavandula angustifolia | 35.00 |
| 8 | Rose oil | 1?.00 |
| 9 | Oleum Caryophylli | 2?.00 |
| 10 | Herba Pogostemonis oil | 2?.00 |
| 11 | Sage oil | 4?.00 |
| 12 | Cade oil | 4?.00 |
| 13 | Antioxidant | 1?.00 |
| Solvent | Dipropylene glycol | 0.00 |
According to the quality percentage composition of each component in the table 4, each component is added in the anticorrosion container (1) successively by sequence number in the table 4, be stirred to 15 minutes and promptly reach even later on;
(2), the solubilising of sleeping essence B
The sleeping essence B that step (1) is deployed carries out solubilising: add in anticorrosion container (2) at first that to account for product population be 10.00% efficient solubilizing agents, be heated to 55～60 ℃, after 15 minutes, to clear; To account for product population be 1.50% the deployed sleeping essence B of step (1) to wherein adding then, after stirring 10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets solubilising sleeping essence B;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 86.40% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 15.00% distilled water, heats, and progressively being sprinkled into while stirring and accounting for product population is 1.50% solid air freshening glue, and heated and stirred to 85～90 ℃, after 30 minutes, make powder dissolution after, stop the heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sleeping essence B and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.60% the antiseptic, when naturally cooling to 40～50 ℃, slowly in the gel colloid, pour the solubilising sleeping essence B of step (2) gained into, continue to stir, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly and be combined into the solid aromatic sleep aid;
It is poured in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic sleep aid product of the present invention.
The solid aromatic sleep aid of above-mentioned gained has obviously compound with faint fragrance of a flower fragrance, slightly cool, delicate fragrance.Fragrance is sent out thoroughly, coordination, pure and mild, mellow and full, be transparent outward appearance, and have certain gel.With the passing of time, fragrance can slowly volatilize, and still can keep fragrance preferably, and bottom note still has the compound flower note of the band Radix Aucklandiae, and colloidal outward appearance also can diminish over time gradually, but the state of its gel can't change.7～10 days pleasant fragrance can be continued to discharge, and function for assisting sleep can be effectively reached.
Embodiment 3
A kind of solid aromatic sleep aid, the mass percent of its contained each composition is composed as follows:
Sleeping essence C 1.13%
Solid air freshening glue 1.00%
Efficient solubilizing agents 9.00%
Antiseptic 0.50%
Surplus is a distilled water.
The preparation method of above-mentioned a kind of solid aromatic sleep aid comprises being prepared as follows step:
(1), the allotment of sleeping essence C
The mass percent of each raw material sees Table 5 in the sleeping essence C example:
The quality percentage composition of each component in the used sleeping essence of the table 5 C example
| Sequence number | The raw material name | Quality percentage composition (%) C |
| 1 | Cananga odorata oil | 25.00 |
| 2 | Eucalyptus quintessence oil | 10.00 |
| 3 | Jasmin quintessence oil | 4.00 |
| 4 | The Anthemis nobilis quintessence oil | 1.00 |
| 5 | The coriander quintessence oil | 2.00 |
| 6 | The Radix Et Rhizoma Nardostachyos quintessence oil | 5?.00 |
| 7 | Oleum lavandula angustifolia | 35.00 |
| 8 | Rose oil | 1?.00 |
| 9 | Oleum Caryophylli | 2?.00 |
| 10 | Herba Pogostemonis oil | 4?.00 |
| 11 | Sage oil | 6.00 |
| 12 | Cade oil | 4?.00 |
| 13 | Antioxidant | 1?.00 |
| Solvent | Dipropylene glycol | 0.00 |
According to the quality percentage composition of each component in the table 5, each component is added in the anticorrosion container (1) successively by sequence number in the table 5, be stirred to 15 minutes and promptly reach even later on;
(2), the solubilising of sleeping essence C
The sleeping essence C that step (1) is deployed carries out solubilising: add in anticorrosion container (2) at first that to account for product population be 9.00% efficient solubilizing agents, be heated to 55～60 ℃, after 15 minutes, to clear; To account for product population be the deployed sleeping essence C of 1.13% step (1) to wherein adding then, after stirring 10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets solubilising sleeping essence C;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 88.37% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 15.00% distilled water, heats, and progressively being sprinkled into while stirring and accounting for product population is 1.00% solid air freshening glue, and heated and stirred to 85～90 ℃, after 30 minutes, make powder dissolution after, stop the heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sleeping essence C and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.50% the antiseptic, when naturally cooling to 40～50 ℃, slowly in the gel colloid, pour the solubilising sleeping essence C of step (2) gained into, continue to stir, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly and be combined into the solid aromatic sleep aid;
It is poured in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic sleep aid product of the present invention.
The solid aromatic sleep aid of above-mentioned gained has obvious fragrance of a flower fragrance, but fragrance is blue or green and dull partially, fragrance of a flower breath and Radix Aucklandiae breath with tangible lavandula angustifolia, fragrance inadequately the circle and, pure and mild, though outward appearance is transparent gel-form, gel effect is not good, after a period of time, not only fragrance weakens, and lose single fragrance of a flower fragrance, and the colloid evaporation rate is fast.Can continue to discharge 5～7 days fragrance, the sleeping effect is more not obvious.
Above said content only is the basic explanation of the present invention under conceiving, and according to any equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.
Claims (12)
1. solid aromatic sleep aid is characterized in that the mass percent of its contained each composition is composed as follows:
Sleeping essence 0.75～1.50%
Solid air freshening glue 0.50～1.50%
Efficient solubilizing agents 8.00～10.00%
Antiseptic 0.40～0.60%
Surplus is a distilled water;
Efficient solubilizing agents wherein is polyoxypropylene fatty alcohol ether, polyoxyethylene aliphatic alcohol ether (12-13 alkanol polyxyethylated alcohol) etc.;
Solid air freshening glue wherein is macromolecular materials such as polyvinyl alcohol, hydroxypropyl emthylcellulose or modified cellulose;
Antiseptic wherein is a DMDMH(dihydroxymethyl dimethyl hydantoin) and IPBC(3-iodo-2-propynyl butyl carbamate) mixture;
Wherein said sleeping essence comprises components such as Cananga odorata oil, eucalyptus quintessence oil, jasmin quintessence oil, Anthemis nobilis quintessence oil, coriander seed oil, Radix Et Rhizoma Nardostachyos quintessence oil, Oleum lavandula angustifolia, rose oil, Oleum Caryophylli, Herba Pogostemonis oil, sage oil, cade oil, antioxidant;
And the mass percent of each component described in the sleeping essence sees Table 1:
The quality percentage composition of each component in the used sleeping essence of table 1
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
2. a kind of solid aromatic sleep aid as claimed in claim 1 is characterized in that:
Efficient solubilizing agents wherein is preferably 12-13 alkanol polyxyethylated alcohol;
Solid air freshening glue wherein is preferably modified cellulose.
3. a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that the mass percent of its contained each composition is composed as follows:
Sleeping essence 0.75～1.50%
Solid air freshening glue 0.50～1.50%
Efficient solubilizing agents 8.00～10.00%
Antiseptic 0.40～0.60%
Surplus is a distilled water;
The mass percent of each component described in the wherein said sleeping essence sees Table 2:
The quality percentage composition of each component in the used sleeping essence of table 2
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
4. a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that the mass percent composition of its contained each composition is preferably as follows:
Sleeping essence 0.75%
Solid air freshening glue 0.50%
Efficient solubilizing agents 8.00%
Antiseptic 0.40%
Surplus is a distilled water;
The mass percent of each component described in the wherein said sleeping essence sees Table 3:
The quality percentage composition of each component in the used sleeping essence of table 3
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
5. a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that its contained each composition
The mass percent composition is preferably as follows:
Sleeping essence 1.50%
Solid air freshening glue 1.50%
Efficient solubilizing agents 10.00%
Antiseptic 0.60%
Surplus is a distilled water;
The mass percent of each component described in the wherein said sleeping essence sees Table 4:
The quality percentage composition of each component in the used sleeping essence of table 4
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
6. a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that the mass percent composition of its contained each composition is preferably as follows:
Sleeping essence 1.13%
Solid air freshening glue 1.00%
Efficient solubilizing agents 9.00%
Antiseptic 0.50%
Surplus is a distilled water;
The mass percent of each raw material sees Table 5 in the wherein said sleeping essence:
The quality percentage composition of each component in the used sleeping essence of table 5
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
7. the preparation method of an a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that comprising being prepared as follows step:
(1), the allotment of sleeping essence
Each component in the sleeping essence is added in the anticorrosion container (1) successively by sequence number, be stirred to 15
Minute promptly reach even later on;
(2), the solubilising of sleeping essence
The sleeping essence that step (1) is deployed carries out solubilising:
At first in anticorrosion container (2), add account for solid aromatic sleep aid product gross mass (hereinafter to be referred as: product population) be 8.00～10.00% efficient solubilizing agents, be heated to 55～60 ℃, after 15 minutes, to clear;
To account for product population be 0.75～1.50% the deployed sleeping essence of step (1) to wherein adding then, after stirring 5～10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets solubilising sleeping essence;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 86.40～90.50% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 10.00～15.00% distilled water, heat, progressively being sprinkled into while stirring and accounting for product population is 0.50～1.50% solid air freshening glue, and heated and stirred to 85～90 ℃, after 20～30 minutes, after making powder dissolution, stop heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sleeping essence and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.40～0.60% the antiseptic, when naturally cooling to 40～50 ℃, slowly in the gel colloid, pour the solubilising sleeping essence of step (2) gained into, after continuing stirred for several minute, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly and be combined into the solid aromatic sleep aid;
It is poured in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic sleep aid product of the present invention.
8. used sleeping essence in a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that the mass percent of its contained each composition is composed as follows:
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
9. sleeping essence as claimed in claim 8 is characterized in that the mass percent composition of its contained each composition is preferably as follows:
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
10. sleeping essence as claimed in claim 8 is characterized in that the mass percent composition of its contained each composition is preferably as follows:
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
11. sleeping essence as claimed in claim 8 is characterized in that the mass percent composition of its contained each composition is preferably as follows:
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
12. sleeping essence as claimed in claim 8 is characterized in that the mass percent composition of its contained each composition is preferably as follows:
Wherein said antioxidant is the BHT(2.6-ditertbutylparacresol).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010501519 CN101954107B (en) | 2010-10-11 | 2010-10-11 | Solid aromatic sleep aid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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Cited By (7)
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| CN104958773A (en) * | 2015-06-11 | 2015-10-07 | 北京清科慧谷科技发展有限公司 | Odor removing and air refreshing composition and preparation method thereof |
| CN106729863A (en) * | 2017-03-07 | 2017-05-31 | 东华理工大学 | High-elastic moisturizing solid scent and preparation method thereof |
| CN104399103B (en) * | 2014-11-28 | 2017-05-31 | 华南理工大学 | A kind of natural air freshener and preparation method thereof |
| CN108926618A (en) * | 2018-08-16 | 2018-12-04 | 云南现代民族药工程技术研究中心 | A kind of plant aromatherapy essential oil of assisting sleep |
| CN110613805A (en) * | 2019-10-18 | 2019-12-27 | 成都瑞事吉事商贸有限公司 | Compound essential oil with calming and sleep-aiding effects and preparation method thereof |
| CN115572640A (en) * | 2022-10-22 | 2023-01-06 | 广州芬豪香精有限公司 | Sleep-aiding and nerve-calming essence and preparation method thereof |
| CN116407591A (en) * | 2023-03-28 | 2023-07-11 | 科丽思化妆品（上海）有限公司 | Sleep-aiding compound essential oil composition, essential oil microcapsule and preparation method of essential oil microcapsule |
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| CN104399103B (en) * | 2014-11-28 | 2017-05-31 | 华南理工大学 | A kind of natural air freshener and preparation method thereof |
| CN104958773A (en) * | 2015-06-11 | 2015-10-07 | 北京清科慧谷科技发展有限公司 | Odor removing and air refreshing composition and preparation method thereof |
| CN104958773B (en) * | 2015-06-11 | 2018-11-27 | 北京蓝盾慧谷生物科技有限公司 | A kind of removing peculiar smell, composition of fresh air and preparation method thereof |
| CN106729863A (en) * | 2017-03-07 | 2017-05-31 | 东华理工大学 | High-elastic moisturizing solid scent and preparation method thereof |
| CN106729863B (en) * | 2017-03-07 | 2019-09-17 | 东华理工大学 | High-elastic moisturizing solid scent and preparation method thereof |
| CN108926618A (en) * | 2018-08-16 | 2018-12-04 | 云南现代民族药工程技术研究中心 | A kind of plant aromatherapy essential oil of assisting sleep |
| CN108926618B (en) * | 2018-08-16 | 2021-04-20 | 云南现代民族药工程技术研究中心 | Plant aromatherapy essential oil for assisting sleep |
| CN110613805A (en) * | 2019-10-18 | 2019-12-27 | 成都瑞事吉事商贸有限公司 | Compound essential oil with calming and sleep-aiding effects and preparation method thereof |
| CN115572640A (en) * | 2022-10-22 | 2023-01-06 | 广州芬豪香精有限公司 | Sleep-aiding and nerve-calming essence and preparation method thereof |
| CN115572640B (en) * | 2022-10-22 | 2023-12-19 | 广州芬豪香精有限公司 | Sleep-aiding and nerve-soothing essence and preparation method thereof |
| CN116407591A (en) * | 2023-03-28 | 2023-07-11 | 科丽思化妆品（上海）有限公司 | Sleep-aiding compound essential oil composition, essential oil microcapsule and preparation method of essential oil microcapsule |
| CN116407591B (en) * | 2023-03-28 | 2024-04-05 | 科丽思化妆品（上海）有限公司 | Sleep-aiding compound essential oil composition, essential oil microcapsule and preparation method of essential oil microcapsule |
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